查询词典 sample method

The amount of H2 released from olivine increases rapidly with decreasing grain size of the crushed sample and orthopyroxene and clinopyroxene show the optimal grain size for H2 release with decreasing grain size of the crushed sample.

在幔源矿物的流体组分中含有一定数量的H2，这些H2在地球演化过程及地幔动力体系中起着十分重要的作用，其在幔源矿物中的赋存状态具重要的研究价值。

The synchronous sample reservation system designed for on-line monitoring of waster water system can sample and reserve the overproof waste water automatically,which was synchronous and consentaneous with the waster water.

废水污染源在线监测技术是近年来发展迅速的一种环境监测技术，对于提高污染物总量控制和环境管理能力具有重要的意义。

Results Crystallin could be well separated from 150 ig of total protein sample using 13% SDS-PAGE. High molecular weight proteins could be well separated from 1.2 mg sample using 10% SDS-PAGE.

结果 当上样量为150 μg，13%的分离胶对晶状休蛋白的分离效果较好，当上样量为1.2mg，10%的分离胶对高相对分子品质蛋白的分离效果较好。

Objective To determine the content of blood strontium for diagnosis of deathful causes of drowning and postmortem submergence. Methods The content of Sr content in the water sample of Nan Du River on Hainan Province, and in the left heart's blood sample of rabbits died of drowning, postmortem submergence were determined with ICP-XSP. The results were compared with that the controls.

目的 研究动物溺水死后不同时间血锶的变化方法以高频电感偶合等离子体光谱分析仪检测外样水体中锶离子含量，并分别测定家兔溺死与死后入水的左心血的锶含量。

Finally heat the starch to 80℃dextrinize 2h,keep warm 0.5h,then cooled to 40℃,add 2.8%CAN initiator,7.5%MMA monomer,sealed and stir 3.3hours of the nitrogen atmosphere,using the screw rod center distance is 32mm,expects the tube diameter phi300mm major axis compared to L/D is 12.5 double screw rods extruding machines,controls the screw rod rotational speed 100rpm sample water content when 20%squeezes out,and the results indictated that the sample may bear 302℃within the high temperature,the water resistance is 14.7%,buried in the simple earth passes through about 180 day to be allowed to achieve the nearly 60%weightlessness rate, and can be basically completely degrades.

因此将淀粉80℃糊化2h，保温0.5h，40℃添加2.8%引发剂，7.5%MMA单体，通氮气密封搅拌反应3.3小时后的接枝产物，利用螺杆中心距为32mm，料筒直径f300mm长径比L/D为12.5的双螺杆挤出机，控制螺杆转速100rpm样品含水量20%时挤出，测定知道样品可以耐302℃以内的高温，耐水性为14.7%，在简单土埋的情况下，经过180天左右可以达到近60%的失重率，可以说基本上完全降解。

Three components of peroxide in the activator amongwhich have the different decomposed temperatures made the Vinyl-ester resinsolidified heat discharge increased that gained a bigger solidified degree. Theactivator-adopted quantity can dramatically affect the casting samples performance:eg. When use 1.0-1.4 portions of activator, the casing sample can reach its maximumTensile strength and Bend strength; when use more activator, the polymeric meshworkcontracted which embrittle the casing sample and reduce the dynamic performance; Inthe Pultrusion processing, when CF composed of about 60vo1%, more demould agentcan bring the better processing but degrade the CFRP, normally use around 1.2 portion.

采用具有不同分解温度的三组分有机过氧化物引发剂，乙烯基酯树脂的固化反应放热量增加，固化程度提高；引发剂用量对浇注体的性能影响很大，在用量为 1.0~1.4 份时，浇注体拉伸强度剂弯曲强度达到最高，过多的引发剂使聚合网络减小，浇注体变脆，力学性能降低；在拉挤成型工艺中，碳纤维的体积含量一般为 60%左右，脱模剂增加使加工性能好转但会使复合材料性能下降，一般用量为 1.2 份。

The difference between the sample with high columnar crystal and the sample with high equiaxed crystal has been studied by using the two parameters.

本文应用上述参数对比研究了柱状晶发达与等轴晶发达样品的差异。

It was indicated by SEM spectra of ZnO thin films that the surface of the sample was leveled off, and the crystals were felsitic. It was found from the experiment that, with the increasing of substrate temperature, there were more oxygen vacancies in the films, which lead the conductance of the sample become larger , and the absorb edge of ZnO thin films shifted toward higher wavelength; with increasing of Ar:O2 ratio, there were lesser oxygen vacancies in the films, which lead the absorb edge of ZnO thin films shifted toward lower wavelength.

实验还发现，随着衬底温度的升高，薄膜中产生的氧空位将会增多，使得ZnO薄膜的电导逐渐增大，而且其紫外透射吸收截止边带向高波长方向漂移；随着氩氧比例的增加，薄膜中的氧缺陷相对减少，薄膜的透射吸收截止边向低波长方向漂移。

The Solidification temperature range was defined as 110-200℃ by DSC analysis. More accelerant used can increase the casing samples dynamic performance, but more than enough accelerant can induce a severe solidified reaction that result in a smaller polymeric meshwork and reducing the sample's performance. Normally the Accelerant dosage can be 2 portions; The Epoxy resin CFRP has a obvious better performances than the Vinyl-ester Resin CFRP, i.e. had a Bend Strength of 1516MPa, LSS of 85MPa, also Tg raised to 195~C~ When used the end-carboxyl polyether to reinforce the epoxy resin, the casing sample's SS, BS and Crack Elongation all increased geminately. The CFRP performance also increased a little, that is because the performance of the CFRP mainly contributed by the CF. The reinforced resin improved the interface between the CF and resin that contribute to the little increasing.

通过DSC分析确定了该环氧树脂的固化温度范围为110~200℃，促进剂增加会提高浇注体力学性能，但过多的促进剂会使固化反应剧烈，聚合网络减小，使浇注体性能下降，一般用量为2份左右；以环氧树脂为基体的复合材料性能明显比以乙烯基酯树脂的性能提高，弯曲强度达到1516MPa，层间剪切强度达到85MPa，同时Tg也上升到195℃；用端羧基聚醚增韧环氧树脂后，其浇注体的拉伸强度、弯曲强度及断裂伸长都成倍增加，复合材料的性能也有所提高，但提高幅度不大，因为复合材料的力学性能主要由碳纤维承担，树脂增韧后改善了复合材料的界面性能。

Degradation test in vitro was carried out in phosphate buffer solution (0.1M, pH7. 4) at 37 ℃. The buffer solution was changed daily. Degradation test in vivo was implanted the sample to subdermal in adult ICH rat in the scapular area lateral to the dorsal midline. At suitable time the samples were recovered. Molecular weight changes in surface layer and bulk of polymer sample were measured by GPC and weight loss was determined gravimetrically. It was found that the degradation behavior can be regulated by changing the composition of copolymers. The critical compositions from surface to bulk degradation behavior for PGCA, PLCA, PLMCA, PLDCA systems were 15-20, 20-30, 30- 40, 40 of mol percent GA or LA unit in copolymers, respectively. The degradation behavior of PGCA, PLCA, PLMCA, PLDCA systems were compared and analysed. Some factors influencing the degradation character, such as copolymer composition, hydrophobicity, crystallinity and enzyme affect etc. played important role.

体外实验中材料降解环境为37℃，0.1M，pH7.4磷酸缓冲溶液，每天换液，定期取样；体内实验中将聚合物试样埋置于ICH小白鼠背部肩胛骨皮下部位，定期处死小鼠，取样，将体内体外样品进行重量损失及试样内外层分子量变化测定，分析各聚合物试样降解行为特性，实验结果证明，改变共聚物组成，可以调节各聚合体系降解行为特性，对PGCA，PLCA，PLMCA，PLDCA共聚体系，交酯摩尔百分含量15-20％，20-30％，30-40％，40％分别为各体系内降解行为特性由表面降解型向本体降解型过渡的临界转折点，交酯含量较低的聚合物不同程度地表现表面降解行为特性，论文对各共聚体系体内外降解行为作了分析对照，例如共聚物组成对材料降解速度与降解行为的影响；生物体内酶对降解行为的影响；材料亲疏水性，聚合物链段结晶行为及碳酸酯结构对材料降解行为的影响等，得出交酯/环碳酸酯共聚体系降解行为一些共性和规律。

The dissecting of samples in group2 were difficult. The root of pulmonary artery and ascending aorta failed to be unfolded because fibrous tissue was tough, right and left fibrous trigone were too firm to be solved by hand. Cardiac muscle fibers couldn't be stripped along myofibrillar trajectory since they were prone to break because of their friability.

组2的心脏解剖困难，表现为纤维组织坚韧，游离肺动脉非常困难；徒手无法松解左、右纤维三角，肺动脉和主动脉根部的游离非常困难；心肌纤维坚硬、质脆，解剖时容易断离成碎块，无法沿纤维走行方向剥离。

We have battled against the odds in a province that has become increasingly violent.

我们对在一个争夺日益激烈省的可能性。