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Preparation of the cathode includes:shaping under the press of 40Mpa, sintering at 550℃for 1 hour and at 900℃for 8 hours and threading with molybdenum bar; Considering the literatures we choose CaCl2 as salt for preparation titanium. Pretreatment of salt is for 1 hour at 100℃and for 2 hours at 300℃. Partial pressure of oxygen which need lower than 5.11×10-7Pa to reduct titanium oxides and hygroscopic property of salt need a sealed equipment to electrolyse. And finally successfully designed a satisfied one and the results show that the equipment can be satisfied the requirment of the experiment. Flow of the inert gas is 1.5L/min, the voltage is 2.8 V, temperature is 850℃and time is 2 hours during pre-electrolysis. Flow of the inert gas is 0.2L/min, the voltage is 3.1 V, temperature is 900℃and time changes with the mass of TiO2 during electrolysis, namely the greater need the longer time; To eliminate influence of salt and other impurities, the products need to wash with distilled water and dilute chlorhydric acid , then wash with dilute hydrochloric acid under supersonic wave assistant. Finally, electrometical properties of the electrolysis of TiO2 is researched by cyclic voltammetry and chronoamperometry, and results show that there are two main reodox steps, namely from TiO2 to TiO and from TiO to Ti.

阴极制备主要包括40MPa压力下模压成型、两段式烧结(1小时内升至550℃保温1小时,再1小时升温至900℃保温8小时)及烧结后TiO2块打孔用钼棒串接三个主要环节;实验中选用CaCl2作为电解熔盐,并对其进行预处理(100℃,保温1小时; 300℃,保温2小时);经热力学计算,还原钛氧化物的氧分压至少要低于5.11×10-7Pa,结合电解过程中所用熔盐CaCl2有极强的吸水性的特点,电解装置应有较高的密封性,自行设计了一套密封性可靠的电解装置,便于实验过程中熔盐预处理和氧分压的控制;通过干燥处理预电解过程中Ar流量大约为1.5L/min、电压为2.8 V、温度为850℃、时间为2小时,电解过程中Ar流量大约为0.2L/min、电压为3.1V、温度为900℃,实验结果表明电解时间与TiO2质量密切相关,质量越大需要电解的时间越长;通过自来水冲洗—稀盐酸浸泡、洗涤—在超声波辅助作用下稀盐酸洗涤,可减少熔盐及其它杂质对电解产物检测结果的影响;最后,通过循环伏安法、计时电流法对电解机理的研究,确定电解还原TiO2制备金属钛主要经历了TiO2-TiO-Ti的过程。

Application of conductive polyaniline on the electronic related industry has become more and more interesting and popular. In this research, the chemical oxidization method was used to form emeraldine salt type PANi doped with HNO3 and dodecyl benzene sulfonic acid.

导电性聚苯胺(Polyaniline;PANi)应用在电子相关产业是目前相当热门的研究领域,本研究采用化学氧化合成法制备硝酸与十二烷基苯磺酸共掺杂之Emeraldine Salt型聚苯胺。

1The chemical oxidization method was used to prepare emeraldine salt type conductive polyaniline doped with hydrochloric acid by interfacial polymerization which employ immiscible interface formed via the water and organic solvent, and we discuss the influences of synthetic conditions on the conductivity of PANI-HCl.

1采用化学氧化合成法,以界面聚合方式,利用水与有机溶剂所形成的不相容界面,直接制备以盐酸掺杂Emeraldine Salt型导电性聚苯胺,探讨合成条件对PANI-HCl之导电度的影响。

Organic: dihydroxybenzene, oxalic acid, hydroquinone, fumaric acid, gulonic acid, o-dihydroxybenzne; m-dihydroxybenzene; coke powder, tartaric acid, cyanuric acid, G salt, R salt.

有机物:苯二酚、草酸、对苯二酚、富马酸、古龙酸、邻苯二酚、间苯二酚、焦炭粉、酒石酸、氰尿酸、 G 盐、 R 盐。

Image recording medium comprising a substrateand an imaging layer containing binder, developer, dye, stabilizer against oil exposure (e.g. Calcium salt of organic acid); method for preparing a recording medium comprising binder, radiation absorber, phenolic compound, calcium salt of organic acid, and leuco dye, said radiation absorber initiating reaction between phenolic compound, calcium salt of organic acid and leuco dye.

图像记录介质,其包含衬底和成像层,所述成像层包含粘合剂、显色剂、染料、抵抗油暴露的稳定剂;制备包含粘合剂、辐射吸收剂、酚类化合物、有机酸的钙盐和无色染料的记录介质的方法,所述辐射吸收剂引发酚类化合物、有机酸的钙盐和无色染料之间的反应。

The increase of salt content improved the production of palmitic acid and linoleic acid, but reduced that of oleic acid. The influence of salt content on stearic acid and linolenic acid was not singnificant.

土壤含盐量的增加,促进棕榈酸、亚油酸的生成,抑制油酸的生成,但硬脂酸、亚麻酸的变化受土壤盐含量的影响不明显。

Pristine Li-Al LDHs are synthesized by hydrothermal process in different reaction conditions by varying the aging time for 1 and 24 hours. Both the Li-Al layered double hydroxides (abbreviated as Li-Al LDH1 and Li-Al LDH24 for aging time 1 hour and 24 hours, respectively) were modified by using sulphanilic acid sodium salt hydrate, modified agent to form modified Li-Al LDH1-SAS and Li-Al LDH24-SAS. The morphology of the pristine layered double hydroxides are investigated by using wide angle X-rays diffraction, scanning electron microscopy and particle size analyzer which indicates that the crystallinity and aspect ratio is increased with increasing the aging time from 1 hour to 24 hours. The particle size of Li-Al LDH24 and Li-Al LDH1 are found to be ~1000 nm and ~250 nm, respectively. Both the pristine and modified LDHs are characterized by XRD, FTIR spectra and thermogravimetric analysis.

本研究目的在於改变长晶时间的长短,合成出同径大小的Li-Al LDHs,再经由改质剂sulphanilic acid sodium salt hydrate将Li-Al LDHs无机层材表面有机官能化制备出改质型Li-Al LDHs-SAS,於是进一步藉由扫描式电子显微镜、射径仪和穿透式电子显微镜等仪器分别观察LDHs改质前和改质后其主层结构型态上的变化;从中可以发现Li-Al LDHs随著长晶时间的增加其径有随之增大的趋势,但经有机化改质后其径会由於改质环境的影响明显低许多,针对此现象本实验将未改质和改质后之Li-Al人工无机层材制备成复材进一步探讨其在热性质和难燃特性上的为表现。

The technological processes of raw ore direct acid-leaching,raw ore salt roasting-water leching or acid leaching and raw ore salt roasting-acid pelletizing curing-acid leaching,etc.

原矿加盐焙烧水浸或酸浸;原矿加盐焙烧一拌酸制粒熟化酸浸等工艺过程。

The research activities were briefly highlighted as follows: They were yield nurseries, observational nurseries, tolerance/resistance screening nurseries (cold, drought, salt/acid, blast. bacterial leaf blight, rice tungro virus, brown planthopper and white-backed planthopper resistances). These studies with evolving technologies are aimed at improving crop production.

其研究活动着重于以下几方面:产量反应,生长观察,耐性/抗性筛选(抗冻、抗旱、抗盐/酸、抗稻瘟病、白叶枯病、水稻塘古罗病毒、褐稻虱和白背飞虱),其目的就是为了提高产量。

In litmus milk experiment, all of strains produced alkai expect for MZ02 and MZ04 produced acid reactions. At 30℃, all of strains grew best, and had a wide range in salt, acid and basic resistance. MZ04 was capable of good growth at salt density of 2.0%, MZ04 and MZ10 could still grew better at pH 9.0. All of the strains were not resistant to 250 μg /mL gentamicin(Sm3), and to other antibiotics, different resistances were presented by different strains, MZ02 had worst resistance to all antibiotics, while MZ04, MZ08,MZ09 had strong resistance.

所有供试菌株在温度30℃时生长最好,耐盐、耐酸碱范围较宽,MZ04在含盐浓度为2.0%环境还能生长良好,MZ04、MZ10在pH9.0环境仍能生长较好;所有菌株对250 μg /mL 庆大霉素(Sm3)均无抗性,不同菌株对其余供试抗菌素表现出不同的抗性,MZ02抗性最差,对所供试的抗生素均无抗性;MZ04、MZ08、MZ09抗性相对较强。

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在对危险的南部地区访问时,他斥责什叶派民兵领导人对中央集权的挑衅行为。

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