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A measuring system which mainly consists of a high precision motorized translation stage of one dimension, POINT GREY Flea2-14S3 CCD camera and LED light source was designed and constructed. Based on a detailed analysis for experiment results, the periodic changing law of system error of LED facula centroid location in this measuring system was found. The results indicate that based on Flea2-14S3 CCD camera, the random error of facula centroid location is about 0.018 pixels, the system error is about 0.06 pixels, and the total error is about 0.063 pixels (1/15 pixels).

利用高精度一维电动平移台、POINT GREY Flea2-14S3 CCD 相机和LED 光源构建了测试系统,对测试结果进行研究和讨论,发现了测试系统LED 光斑质心定位系统误差的周期性变化规律,计算得到了基于Flea2-14S3 CCD 相机的光斑质心定位随机误差为0.018 pixels,系统误差为0.06 pixels,总体误差为0.063 pixels(约1/15 pixels),能够应用于以光斑质心检测为手段的测量系统中。

A measuring system which mainly consists of a high precision motorized translation stage of one dimension, POINT GREY Flea2-14S3 CCD camera and LED light source was designed and constructed. Based on a detailed analysis for experiment results, the periodic changing law of system error of LED facula centroid location in this measuring system was found. The results indicate that based on Flea2-l4S3 CCD camera, the random error of facula centroid location is about 0.018 pixels, the system error is about 0.06 pixels, and the total error is about 0.063 pixels (1/15 pixels). According to the total error above, this CCD imager can be widely used in many measuring systems which count on facula centroid subpixel detection.

利用高精度一维电动平移台、POINT GREY Flea2-14S3 CCD相机和LED光源构建了测试系统,对测试结果进行研究和讨论,发现了测试系统LED光斑质心定位系统误差的周期性变化规律,计算得到了基于Flea2-14S3 CCD相机的光斑质心定位随机误差为0.018pixels,系统误差为0.06pixels,总体误差为0.063pixels(约1/15pixels),能够应用于以光斑质心检测为手段的测量系统中。

The results showed that the content of Se element in the Se-MT was 2.5 folds higher than that of Zn-MT, on the contrary the content of sulfur element in Se-MT was 2 folds lower then Zn-MT, C, H, N contents in MT were no significant differences in both groups. In terms of chemical property, the element of selenium is very similar to sulfur because they are in the same group in the periodic table. The above results illustrated that the Se could replace S from SH-sulfhydryl to SeH-selenihydryl in cysteine, which presents the existence of a novel Se-MT.

结果表明Se-MT中Se元素含量高于Zn-MTZ.5倍左右,而 S元素含量低于 ZnMT 2倍左右,C、H、N元素含量无明显差异,这说明了麦硒康诱导后Se仙T分子结构上的差异,由于Se元素与S元素同属氧族元素,在化学性质上极为相似,故Se元素极可能替代了MT的合成过程中所必需半味氨酸残基中的SH一基因上的S元素成为SeH一基团,这样我们就得到了一种含SeH一基团的新型Se-MT。

Visualization technology can realize interactive analysis of direct data input, results output and mining, and provide ways of data mining with the participation of people's perception, insight and perspicacity, as well as ways of visualized mining and the visualization of mining results.

可视化技术能为数据挖掘提供直观的数据输入、结果输出和挖掘过程的交互探索分析手段,可以在人的感知力、洞察力、判断力参与下提供数据挖掘手段,实现可视化辅助挖掘手段以及挖掘结果的可视化。

Results Cyclohexane, n-hexane, petroleum ether and chloroform had the same or better results in thin-layer chromatography.

结果 可获得等同效果或效果更好的薄层色谱。

Compared with the results of pharmacopeia methods, the results we obtained were satisfactory.

本方法已成功应用于3种含巯基药物制剂的含量测定,与药典方法比较,结果满意。

The results indicate that this method is robust to the noise in remote sensing dataset. Compared with other methods, time series of remote sensing data can be fitted to this model effectively, and realistic phenology results are detected.

结果表明,这种方法能够有效的消除遥感数据中的噪音对提取结果造成的影响,可以达到较以往的物候提取方法更满意的拟合效果和更符合实际的物候提取结果。

Therelationship of the amount of catalyst and the ee% of product was seen to be negative nonlin-ear. Catalyst 3 was used in the enantioselective addition of diethylzinc to aromatic aldehydesand gave good results. The configuration of products was determined by the configuration ofthe catalysts' chiral carbon linked with hydroxy group. Using β- amino alcohols bearing only one chiral center as catalysts for the enantiose-lective addition were studied. D-N, N-dialkyl-2-amino butanol gave poor catalytic effect be-cause of their structure. The configuration of the product is the same as the catalyst. Anotherkind of β- amino alcohols - phenylglycine derivatives and valine derivatives have chiralcenter on the carbon linked with amino group. Catalyzed by-phenylglycine derivatives 6,7, 9, 10, the reactions gave satisfied results. The optical yields exceeded 80%.

在探讨了含有两个手性中心的β-氨基醇之后,选择了只有一个手性中心的β-氨基醇,一是手性中心为连羟基的手性碳原子:D-N,N-二烷基-2-氨基丁醇;二是手性中心为连氨基的手性碳原子:D-苯基甘氨酸衍生物和L-缬氨酸衍生物。D-2-氨基丁醇的催化效果不太好,这与其结构的空间位阻较小有关系,反应产物与连羟基手性碳构型一致;由苯基甘氨酸和缬氨酸出发合成五种β-氨基醇6-10,研究了不同ee%的-6作用下的二乙基锌-苯甲醛加成反应,发现该催化剂具有不对称放大效应;-7,9,lO的催化效果也比较令人满意,光学产率80%以上,所得产物构型与催化剂构型一致。

Results: The determination results of calcium, phosphonium and uric acid in treated urine were all in linear ranger of biochemical analyzer.

结果:预处理后的尿液中三种物质的测定值均落在生化分析仪的线性范围以内,且均与比色法有显著的相关性。

Results: The determination results of calcium, phosphonium and uric acid in treated urine were all in linear ranger of biochemical analyzer. This method had a significant correlation with colorimetric method.

结果:预处理后的尿液中三种物质的测定值均落在生化分析仪的线性范围以内,且均与比色法有显著的相关性。

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