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The intermediates 2a～2f of cyclic (1-arylseleno)glycerol phosphate and tegafur conjugates were synthesized by one-pot reaction of hexaethyl phosphorous triamide, activated by a catalytic amount of iodine, with (N3-tegafur)alkanol, 1-arylselenoglycerol and sulphur successively in refluxing benzene.

以碘作催化剂，无水苯为溶剂，六乙基亚磷酰三胺依次与羟乙基替加氟、1-芳硒基甘油及硫反应，得中间体硒代环甘油磷脂替加氟缀合物2a～2f。

The factors,which infuences the decolorization effect of galactomannan extracted from the seeds of Trigonella Foenumgraecum were studied by ethanol refluxing.

采用乙醇回流法考察了影响由胡芦巴种子提取的半乳甘露聚糖脱色效果的因素，并应用L(9 34)正交实验设计优化脱色工艺条件。

MethodsSeveral extraction processes were used,such as decocting method,the refluxing method,leakaging method.

目的优选苦参中氧化苦参碱的提取工艺。方法比较多种提取工艺。

Compounds 3a-3d, 4a-4d, 5a-5d, 6a-6e and 7a-7e were prepared with a new efficient method, in which the aromatic amines were diazotized with isoamyl nitrite in EtONa/EtOH under refluxing condition, and mono -, bis -and tetrakis -substituted calix [4] arenes were obtained respectively as main product by diazo-coupling in different molar ratio to calix [4] arene.

一，提出了一个有效的新方法合成含有芳香偶氮基团的杯[4]芳烃衍生物3a-3d；4a-4d；5a-5d；6a-6e和7a-7e：即在非水溶剂乙醇中用亚硝酸异戊酯，在强碱乙醇钠存在下对芳香胺进行重氮化，得到芳香重氮酸盐沉淀，过滤，然后加入杯[4]芳烃的四氢呋喃溶液，通入CO〓气体调节溶液的pH值为7-9，使其发生偶联反应。

In contrast, the sulfated content of the catalyst was 1.45% after 24 h digestion refluxing.

而经水热回流处理24h制备的催化剂样品硫质量分数为1.45%，在正丁烷异构化反应中显示出优异的催化性能，250℃下的稳态转化率大于46%，接近该条件的平衡转化率。

Penicillin G sulphoxide is esterified by N,N′-bistrimethylsilyl urea under the temperature 55℃ with a molar ratio 2.5∶1 between BSU and sulphoxide,and the ester obtained is ring-enlarged in the toluene under refluxing with the exist of catalyst-pyridine acetyl bromide.

摘 要 本文在制得青霉素G亚砜的基础上，完成了重排酸的扩环反应，重点探讨了扩环反应的最优化条件。青霉素G亚砜与N，N′-双脲在55℃下反应，得到亚砜的酯化物。

And the best conditions were as following: alcohol as solvent, sodium carbonate as acid absorbing agent, refluxing for 8h.

通过因素分析确定了合成RNB的最优化条件为：以乙醇为溶剂，Na_2CO_3为缚酸剂回流反应8h。

The optimum conditions of synthesize RNB had been accomplished by the methods of factor analysis. And the best conditions were as following: alcohol as solvent, sodium carbonate as acid absorbing agent, refluxing for 8h.

通过因素分析确定了合成RNB的最优化条件为：以乙醇为溶剂，Na_2CO_3为缚酸剂回流反应8h。

QN 〓PHAL,〓PHAL and 〓PHAL were quaternized by refluxing with benzyl bromide to give ligands 8, 9 and 10 respectively. 2. The chiral ligands were applied to the AD reaction of olefins with NMO as co-oxidant and PEG (400 MW) or PF〓 as reaction media.

以奎宁和奎尼定为原料分别与1，4-二氯-2，3-二氮杂萘反应制备〓PHAL和〓PHAL，然后通过〓PHAL、〓PHAL及〓PHAL与苄基溴的季铵化反应制备单季铵盐手性配体8、9和10。

The effect of refluxing treatment of nitric acid and adding of nickel oxide to carbon nanotubes on the properties of supercapacitors was also studied.

分析了复合电极材料的结构和形貌，研究了碳纳米管与氧化镍复合、回流表面改性对超大容量离子电容器性能的影响。

Finally, according to market conditions and market products this article paper analyzes the trends in the development of camera technology, and designs a color night vision camera.

最后根据市场情况和市面上产品的情况分析了摄像机技术的发展趋势，并设计了一款彩色夜视摄像机。

Only person height weeds and the fierce looks stone idles were there.

只有半人深的荒草和龇牙咧嘴的神像。