查询词典 refluxing

The total flavonoids content of peanut hulls of different sources were evidently different,those peanut hulls contained more total flavonoids from Shandong province,higher maturity and raw. This suggested that attention should be paid to the choice of peanut hulls as medicine materials. 3.The optimized extraction technology conditions considering the two indices of total flavonoids andβ-sitosterol were: the peanut hulls were extracted by 95% acohole 6 times of the hulls weight refluxing for 2 hours first,and extracted by 70% acohole 4 times of the hulls weight refluxing for 2 hours at the temperature below 80℃successionally,then the concentrate was dried vacuumizedly with the additament of starch 2% of the concentrate weight after the extracts were fitrated,united and concentrated. 4.The dried extract powder possessed high hygroscopy and low fluidity,but the weight variation of capsule contents could comply with the requirement of CP if it was mixed with dextrin and granulated by sieving 40 meshes using 95% ethanol as the wetting agent,and filled into capsules after dried below 60℃.The critical relative humidity of the granules was about 63%.

不同来源的花生壳总黄酮含量有较大差异，山东产区、成熟度高的及未经炒制的花生壳总黄酮含量较高，提示作为药材时应注意选择； 3、兼顾总黄酮及β-谷甾醇的最佳提取工艺为：先以95%乙醇6倍量加热回流提取2小时，再以70%乙醇4倍量80℃以下回流提取2小时，提取液过滤、合并、浓缩，加2%淀粉60℃以下减压干燥； 4、浸膏粉吸湿性大，流动性差，但加糊精并以95%乙醇为润湿剂、过40目筛制粒，60℃以下烘干后填充胶囊，可保证装量差异符合要求；颗粒临界相对湿度约为63%。

The yield of the 3, 4-dihydropyrimidine-2(1H)-one was up to 95.4% under mole ratio of anisaldehyde, methyl acetoactate and urea is 1:2:5, ion-exchange membrane is 3 g, ethyl alcohol as solvent and refluxing for 2 h.

当对羟基苯甲醛、乙酰乙酸甲酯与脲的摩尔比为1：2：5，乙醇作溶剂，3 g离子交换膜，回流2 h，产物收率达95.4%。

Objective:To investigate the diagnosis and treatment of refluxing cholangitis.

目的探讨反流性胆管炎的诊断和治疗方法。

Methods:Clinical data of 60 patients with refluxing cholangitis treated by surgery in recent 7 years in our hospital were reviewed retrospectively.

方法回顾性分析7年间手术治疗反流性胆管炎60例患者的临床资料。

The diphenylamine was deuterated by refluxing with a mixture of heptane and ??

将二苯胺与正庚烷和？虻幕旌衔锛尤然亓？

The results of experiment show the optimal extraction condition of Gardenia Yellow: refluxing and extracting three times with 50 percent ethanol in 55℃, water-bath and extracting 4 to 5 hours, Gardenia Yellow extract solution is separated by X-5 absorption resin, and then with 30 percent ethanol, getting Geniposide white crystal, the determining purity by HPLC come to 99.1% and can be used as standard, the part doffing by 70% ethanol can be concentrated to get more pure Gardenia Yellow pigment.

实验证明了栀子黄的最佳提取条件：50%的乙醇回流提取3次，55℃水浴加热，提取时间为4-5个小时。栀子黄提取液经X-5大孔吸附树脂分离，用30%乙醇溶液洗脱，纯化得到栀子苷白色晶体，HPLC检测纯度达99.1%，可做标准品使用。70%乙醇洗脱部分浓缩可得栀子黄产品，精制后产品纯度有显著提高。

Methods 15 patients with different type and degree of cicatricial ectropion were repaired with the method of simple skin grafting, posterior auricular refluxing axial skin flap or anchyloblepharon.

对15例不同类型和不同程度的瘢痕性睑外翻，采用局部瘢痕松解睑缘粘连、耳后返流轴型皮瓣修复及瘢痕松解植皮修复。

Methods:The orthogonal design was used and menstruum capacity,extraction time and refluxing time were defined as factors of the design.

以多糖提取率、提取浸膏得率为指标，采用单因素考察提取溶媒，以溶媒量、提取次数和提取时间为考察因素，采用正交设计法优化提取工艺。

The method comprises following steps: taking diphenol and 3- trifluoromethyl- 4- chloronitrobenzene as raw material, salt precipitating for diphenol and potash, refluxing with water- containing toluene, reacting with 3- trifluoromethyl- 4- chloronitrobenzene and getting dinitro monomer; taking dinitro monomer, ferro powder and HCl as raw material, ethanol and water as disslovant for refluxing and ethanol recrystallization, getting fluorine- containing aromatic diamido monomer.

合成方法是以二酚与3-三氟甲基-4-氯硝基苯作原料，先将二酚与碳酸钾成盐，甲苯带水回流反应，然后与3-三氟甲基-4-氯硝基苯反应制得二硝基单体；再以二硝基单体，铁粉，HCl为原料，乙醇和水做溶剂，回流反应、乙醇重结晶，得到含氟芳香二胺基单体。

Results The optimum conditions for the extraction of Peucedanum praeruptorum Dunn was as follow: 80 % alcohol was used as solvent, and 8 times the amount of alcohol was added, the mixture was kept refluxing for 1.0 h for the first time; then 6 times the amount of alcohol was added and the mixture was kept refluxing for 0.5 h for the second time; Four times the amount of alcohol for 0.5 h for the last time.

结果 白花前胡的最佳提取工艺为用质量分数80 %的乙醇提取3次，提取时间分别为1.0、0.5、0.5 h，3次所用溶媒量分别为药材质量的8、6、4倍；按照筛选出的最佳工艺条件进行的3次重复性实验，测得浸膏中8-甲氧基补骨脂素含量质量分数为0.094 %，折合1 g生药中含量为0.171 2 mg，与预测值基本一致。

Plunder melds and run with this jewel!

掠夺melds和运行与此宝石！

My dream is to be a crazy growing tree and extend at the edge between the city and the forest.

此刻，也许正是在通往天国的路上，我体验着这白色的晕旋。