查询词典 redissolved

Objective To establish a HPLC method for the determination of aceclofenac in human plasma.Methods Acidified samples of plasma (500μL) were extracted with 4 mL of ethyl acetate. The organic phase was evaporated to dryness by nitrogen at 40℃ water bath. The residue was redissolved in mobile phase and then was determined.

醋氯芬酸是一种具有镇痛作用的非甾体类抗炎药物[1]，化学名为[邻-(2，6-二氯苯基)氨基]苯乙酰乙酸，l992年首先于西班牙上市，具有明显广泛的抗炎作用和强力的解热镇痛作用，其生物半衰期较双氯芬酸长，胃肠耐受性较双氯芬酸好，抗炎活性优于萘普生和保泰松[2]。

Brinkhous of the University of North Carolina at Chapel Hill and Edward Shanbrom of Hyland Laboratories produce a highly concentrated form of Factor VIII by pooling large quantities of plasma that generate vast amounts of cyro, which are then redissolved, treated, filtered, and centrifuged.

Brinkhous博士在查珀希尔和Edward Shanbrom的海兰实验室通过汇集许多能产生大量冷沉淀的血浆制造出富含Ⅷ因子的浓缩物，然后再融解、处理、过滤和离心。

The organic layer was evaporated and the residue was redissolved by mobile phase.The concentrations of propofol and lidocaine were assayed on a hypersil BDS C18 column with a mobile phase consisting of acetonitrile-methanol-water（10∶60∶30）（including 0.14%n-butyamine 0.1%acetic acid）at a flow rate of 1 mL*min-1 and detected at 220 nm during 1～7 min and at 273 nm during 7～16 min.

氮气吹干有机层，残留物用流动相重新溶解后，用Hypersil BDS C18柱分析，流动相为乙腈-甲醇-水(10∶60∶30)，内含正丁胺0.14%和冰醋酸0.1%，流速为1 mL*min-1，检测波长：1～7 min用220 nm，7～16 min用273 nm。

For Method Ⅰ, the residues were extracted from homogenized tissue with acetone-ethylacetate-n-hexane (1∶1∶1, v/v/v), and then were redissolved in acetonitrile; for Method Ⅱ, the residues were extracted from homogenized tissue with acetonitrile-water under ultrasonication, and then were separated by liquid-liquid partition.

在样品前处理方法Ⅰ中，样品经丙酮-乙酸乙酯-正己烷(体积比为1∶1∶1)混合溶剂提取，乙腈转溶；在样品前处理方法Ⅱ中，样品用乙腈-水溶液均质，超声波辅助提取，液-液分配。

DNA immunization with the Sj16 gene Plasmid DNA was prepared by QIAGEN plasmid mega kit and redissolved in NS at a final concentration of 1μg/μl.

Sj16基因DNA免疫研究用QIAGEN Plasmid mega大量质粒提试剂盒大量制备高纯度的pcDNA〓-Sj16、pcDNA〓和pUC19质粒DNA。

The sample was extracted by deionized water. The extract was cleaned up and concentrated on a SPE column, then eluted by methyl-tert-butyl ether. The elution was concentrated under nitrogen and redissolved to 1 mL.

样品中24种目标物用蒸馏水浸出后，经固相萃取小柱富集净化，再用叔丁基甲醚洗脱，洗脱液氮吹浓缩定容后用气相色谱－质谱法测定。

The eluent was evaporated to near-dry under nitrogen and then redissolved with methanol-0.1% formic acid(1∶1,by volume),finally determined by HPLC-MS/MS.The linear range of the calibration curve was 0-50 μg/L for all pyridine herbicides.

在大白菜和橙子2种基质中分别添加5.0、10.0和20.0μg/kg3个水平，玉米基质中添加5.0、10.0、20.0和40.0μg/kg 4个水平的4种吡啶类除草剂混合标准溶液，平均回收率为70%~117%，方法的相对标准偏差小于15%。

Results The clarity was good after roxithromycin redissolved in water; the preparation had no hemolysis phenomenon, no significant irritation effect on vessels and no allergic response. Conclusions The technics of preparing roxithromycin for injection is simple.

结果 罗红霉素与L-门冬氨酸成盐后溶解度大大提高，制备的冻干粉针复溶后澄明度良好；注射用罗红霉素无血管刺激性、无溶血现象、无过敏反应。

The combined extract was concentrated to dryness and redissolved in acetonitrile, then cleaned up by dispersive solid-phase extraction with sorbents of N-propyl ethylene diamine, graphited carbon black, and C18, and determined and confirmed by GC-NCI/MS.

样品经乙腈提取并浓缩后加入N-丙基乙二胺、石墨化碳黑和C183种填料进行分散固相萃取净化，气相色谱-负化学离子源质谱分时段选择离子监测技术测定与确证，外标法定量。

The sample was redissolved in the acetonitrilved in the acetonitrile-water (3:2, v/v), then analyzed using LC-MS/MS in multiple reaction monitoring mode via positive electrospray ionization with an Agilent ZORBAX SB-C18 column as the analytical column.

样品用1%醋酸乙腈溶液萃取，经Waters Sep-Pak Vac固相萃取柱净化，乙腈－甲苯（体积比为3：1）洗脱，旋转蒸发浓缩，用乙腈－水（体积比为3：2）溶解，以Agilent ZORBAX SB-C18色谱柱分离，以电喷雾电离串联质谱在正离子多反应监测模式下进行测定。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。