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Results the uncertainty from sampling,standard stock solution diluted, standard curve and recoveries are the key factors.conclusion the method of uncertaintuy for determination of manganese in air from workplace by faas can be used in quality control of determination process.

运用该不确定度评定方法对测定过程中关键环节的识别,将有助于检测人员重点关注关键环节的质量控制,以更为有效地提高检测工作的质量。

ConclusionThe GC-SIM-MS method developed in this study has been shown to be suitable with acceptable reproducibility and recoveries for simultaneous determination of putrescine,spermidine and spermine as N-HFB derivatives in hair samples.

该方法使我们能更快更正确地同时检测头发样品中的腐胺、精脒和精胺,能在临床早期诊断和癌症预防方面有一定帮助作用。

The relative standard deviation were less than 5%, and the recoveries were in the range of 97% to 103%.

测量结果的相对标准偏差小于5%,回收率在97%~103%。

Results:The recoveries for scopolamine and strychnine of the method are 100.5%(RSD 2.3%,n=5)and 97.5%(RSD 2.4%,n=5),respectively.

检测波长226 nm。结果:该方法回收率氢溴酸东莨菪碱为100.5%,RSD=2.3%(n=5);士的宁为97.5%,RSD=2.4%(n=5)。

The calibration curve of the SM2-Kit with standard SM2 inhibitor was typical sigmoid curve fitted to the four parameter logistic equation with the linear detection of 0.625 μg/L to 80.0 μg/L (R2=0.9911), the sensitivity of 0.9 μg/L, the IC50 of 5.82 μg/L and the detection limit of 1 μg/L. The recoveries of SM2 spiked in pig feed were 83.4 %, in pig urine were 89.5 %. The precision and accuracy of the assay as determined by inter-assay and intra-assay coefficient variation was both below 15 %. The SM2-Kit generally had 2.08 % cross-reactivity towards sulfamerazine and little or no cross-reactivity towards other sulfonamides. The dilution solution of SM2 had no effect on results of SM2-Kit. The validity of SM2-Kit in 4 ℃ was above six months.

研究结果表明,SM2-Kit的标准曲线呈典型的S型,相关系数R2=0.9911,符合4参数logit曲线拟合,线性检测范围为0.625 μg/L~80 μg/L,灵敏度为0.9 μg/L,半数抑制浓度(IC50)为5.82 μg/L,检测限为1 μg/L;饲料样、猪尿样的平均添加回收率分别为83.4 %、89.5 %,平均批内和批间变异系数均低于15 %;SM2-Kit与磺胺甲基嘧啶的交叉反应率为2.08 %,与其它磺胺类药几乎没有反应性;基质对SM2-Kit的检测结果影响不大;试剂盒在4 ℃可保存6个月。

With slower recoveries from Bell's palsy, synkinesis, hypertonic muscles and spasms become more likely.

贝氏面瘫缓慢的康复过程中,联带运动,cross-wiring,肌肉张力亢进和抽搐更易发生。

By studying the factors that affect the purities of products and recoveries of isoflavones, we got the optimum conditions for desorption: 70℃, eluting solvent sequence: water 3.0 BV, 75% ethanol 5.0 BV, flow-rate 2.5 mL·min~(-1). Under these conditions, the content of isoflavones in the product was 56.0% with the recovery of 89.3%. The content of isoflavones in the product was ten times larger than in the initial material.

异黄酮的解吸,以异黄酮产品的含量及异黄酮回收率为指标,对解吸溶剂浓度、温度等因素进行考察,确定采用水、体积分数75%乙醇溶液在70℃下依次洗脱,收集醇洗脱液可得到大豆异黄酮含量达56.0%的产品,含量比原料提高了十几倍,异黄酮回收率也较高,达到了89.3%。

The experimental conditions were optimized to produce following results: good linearity of sulfamethoxazole, norfloxacin, ciprofloxacin, ofloxacin and tetracycline in the range from 1.00 ng/L to 1 000 ng/L and the limits of quantification 1 ng/L, the good linearity of terramycin and aureomycin in the range from 10.0 ng/L to 2 000 ng/L and the LOQ 10 ng/L, the recoveries of deionized water and surface water from 72.1% to 112%, and the RSD from 0.6% to 9.2%.

摘要〗采用超高效液相色谱-电喷雾二级质谱联用技术同时测定水中7种抗生素,优化了试验条件。磺胺甲恶唑、诺氟沙星、环丙沙星、氧氟沙星、四环素在1.00 ng/L ~1 000 ng/L 范围内线性良好,定量下限为1 ng/L ,土霉素、金霉素在10.0 ng/L ~2 000 ng/L 范围内线性良好,定量下限为10 ng/L ,去离子水和地表水样加标回收率为72.1%~112%, RSD 为0.6%~9.2%。

The average recoveries were 60.2%~125% and 64.5%~126% for the drugs in plasma and urine except those of perphenazine, thioridazine and chloropromazine in plasma were 37.6%~57.5%, 36.3%~48.3%, 52.4%~67.4%, respectively; trazodone and diazepam in urine were 100%~142% and 108%~177%, respectively. The relative standard deviations of all the drugs in plasma and urine were within 0.8%~26% and 2.6%~18%(n=6), respectively. The detection limits of the 4 barbitals ranged from 20 to 100 mg/L and those of the other drugs ranged from 0.05 to 2.0 mg/L.

血浆样品中待测组分的加标回收率除了奋乃静、硫利哒嗪和氯丙嗪的分别为37.6%~57.5%, 36.3%~48.3%和52.4%~67.4%外,尿液样品中待测组分的加标回收率除了曲唑酮和地西泮的分别为100%~142%和108%~177%外,血浆和尿液中其余待测组分的加标回收率分别为60.2%~125%和64.5%~126%,相对标准偏差分别为0.8%~26%和2.6%~18%(n=6);除了巴比妥类药物的检出限为20~100 mg/L外,其余药物的检出限均为0.05~2.0 mg/L。

Under the optimum experimental conditions, copper, iron and zinc in traditional Chinese medicines such as radix angelicae sinensis, flos sophorae, herba taxilli, folium apocyni veneti and radix scutellarae were determined. The recoveries are between 90% and 110%, the relative standard deviation is less than 5%, and the experimental results are satisfactory. This method is rapid and reliable.

在选定的实验条件下,利用标准加入法分析测定了中药当归、槐花、桑寄生、罗布麻叶和黄芩等中药中的铜、铁和锌的含量,回收率为90%~110%,方法的相对标准偏差小于5%。

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