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In this thesis, the reaction of methanol conversion into hydrocarbons on HZSM-5 and SAPO molecular sieves, which is of great importance to industry, is selected as probe reaction to get deeper insights into the structure of solid catalysts and the interaction of reactants with catalysts during adsorption and catalytic reaction by solid state NMR.

本论文主要以固体NMR为研究手段，以甲醇制烃类作为探针反应，详细研究了催化剂的结构、吸附过程中反应物与催化剂的相互作用、反应过程中反应物与催化剂的相互作用，主要取得了如下结果： 1 原位MAS NMR实验结果表明，甲醇制烃类的过程是通过&碳池&机理来实现，&碳池&的组成随反应的进行而变化，在反应前期，&碳池&由饱和烃类构成，随着反应的进行，饱和烃类和不饱和烃类共同组成&碳池&。

In the interfacial layer near to SiC, elements Pd and Ni preferentially diffused to SiC and resulted in the reaction products of Pd-Si phase, Ni-Si phase and graphite. In the reaction zone further away from the SiC, mainly elements Cr and V in the brazing filler participated in the interface reaction, and formed Cr-C, Cr-Si, Cr5Si3C. In the central part of the joint, the matrix was composed of Pd-Si, Ni-Si and V-Si phases, on which some blocky carbides V2C, Cr23C6 distributed scatteringly.

MPa。微观分析表明，在靠近SiC的界面反应层中，主要是Pd和Ni优先与SiC反应生成相应的Pd-Si相，Ni-Si相和石墨；接头中在离SiC稍远的区域，主要是Cr和V与母材扩散进入钎缝且未与Pd和Ni反应的C和Si发生反应，生成Cr-C， Cr-Si， Cr5Si3C 等相；钎缝中心区的基体由Pd-Si，Ni-Si和V-Si相组成，其上弥散分布着块状碳化物V2C和Cr23C6。

A Bacteriocin-producing Lactic Acid Bacteria R260 strain was screened from plant-material. The morphological, physiological and biochemical features of R260 strain were as follows, the bacterial cell was gram-positive, straight rot-shaped, single or pairs and the spor wasn't found. VP reaction, nitrate reaction, gelatin liquefy and catalase reaction were negative. Glucose, fructose, sucrose and maltose were fermented to organic acids.

本实验从植物性材料中筛选到一株产细菌素的菌株 R260，菌株的形态观察和生理生化性质测定结果显示，菌体细胞呈杆状，单个或成对出现，革兰氏阳性，无芽孢；接触酶反应、硝酸盐还原实验、明胶液化实验、产氨实验、水解淀粉实验、硫化氢产生实验和 VP 实验均为阴性；发酵葡萄糖、蔗糖、麦芽糖、果糖和核糖。

The composition reaction of mullite 〓. Consumed Al〓O〓 and SiO〓 in this reaction were noncrystal shapless species got in the decomposition reaction of metakaolinite.

扫描电镜形貌分析表明，各焙烧制度下所得到的焙烧产品振磨后其形貌和颗粒大小都很接近，因而不会对溶出脱硅结果产生多大的影响。

The best reaction system for ISSR in our research followed as: the whole volume of the reaction is 20μL, and the mixture in this reaction included 50ng DNA, 2.0mmol/L MgCl_2, 0.2μmol/L primer, 200μmol/LdNTPs, 0.5U TaqDNA polymerise and 1×PCR buffer; and the PCR program was 94℃7min, 1 cycle; 94 ℃ 30s, specific temperature 45s, 72℃ 90s, 38 cycles; 72℃ 10min, 1cycle.

对两种标记的检测效果表明，ISSR和RAPD标记所得结果呈极显著相关，证明这两种标记技术均可用于樟科植物的遗传多样性和亲缘关系研究，但ISSR效果明显优于RAPD。

The pilot study shows that the ammonia dissociation/synthesis reaction is inherently free of any potential side reaction problems, and also offers phase separation of products. The carrier of heat store is liquid. and is very interesting for long-term storage as it can be carried out at room temperature with no energy losses, Its theoretics energy storage density reachs 66.5kJ/mol, which outclasses sensible or latent heat storage. In comparison to other thermochemical energy storage, ATCES needs lower temperature in endothermic reaction(only 650℃), but It can produce over 550℃ high temperature stream in exothermic synthesiser. Furthermore, the heat store/recovery can change with adapt to the heat source/load automatically, and offers coninuous(24 h) production of heat, These advantages will see a rapid increase in the adoption of large-scale concentrating solar thermal power generation.

初步研究表明：采用氨基储能体系，储/释过程无副反应，且储能介质能自然发生相分离；储热载体为流体，并可在室温下长期无热损储存，理论储能密度达66.5kJ/mol，远高于显热或相变蓄热；与其它热化学储能相比，吸热反应温度低，仅需650℃，而放热反应可产生500℃以上的高温，能量的储/释流量可随热源/负荷自适应变化，且可全天供热，更适合作为聚光式大规模太阳能热力发电中的能量储存系统。

The components of the catalyst are sulfurated more completely with a longer reaction time. But the catalyst congregates into a large volume ball with a low BET surface area after a certain reaction. So the best range of reaction time is from 60 to 90 minutes.

研究发现，虽然硫化时间的延长可提高催化剂中金属组分的硫化物含量，但超过一定反应时间可导致硫化物过度结晶聚集，颗粒度增大，比表面下降，较佳的反应时间为60～90 min。

Emulsification is the mainly reason to influence on the reaction, the influences of emulsifiers such as the concentration of emulsifies, the ratio of anionic to nonionic emulsifier on the polymerization stability were researched;The influences of concentration and feeding method of initiators on the reaction stability and the mechanical properties of coating film of acrylate polymerization stability were researched;The influences of reaction temperature, stirring speed and pH buffer agent on the polymerization stability and pH regulator on the storage stability of Acrylate emulsions were also researched.

乳化剂是影响乳液稳定性的主要因素，因此对乳化剂进行了全面的探讨，包括乳化剂的种类和用量、阴离子型与非离子型乳化剂的比例对乳液稳定性的影响；文中还研究了引发剂的用量、加入方式对聚合稳定性的影响，以及引发剂用量对聚丙烯酸酯涂膜力学性能的影响；此外，讨论了反应温度、搅拌速率、pH值缓冲剂对乳液聚合过程稳定性的影响及pH调节剂对乳液贮存稳定性的影响。

The influence factors include amount of esterifying agent, reaction temperature, reaction time, reaction pH and amount of urea.

实验表明干法制备高取代度木薯淀粉磷酸酯的适宜条件为：反应温度140℃～150℃，反应pH5.0，反应时间2h，尿素用量4～5%。

In this paper,NBR was modified by fluorinating with XeF2 and the reaction kinetics of fluorination was studied by FT-IR spectrometry.The apparent reaction order of 1.5 was suggested,which seemed to become less for long reaction time.

目前报道的高分子表面氟化改性的方法很多，主要的方式有：辐射接枝法、等离子体活化法[1，2]、静电喷涂法、离子注入法及氟化剂表面化学反应法[3—7]等。

But we don't care about Battlegrounds.

但我们并不在乎沙场中的显露。

Ah! don't mention it, the butcher's shop is a horror.

啊！不用提了。提到肉，真是糟透了。