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Methods:All patients with PTB were received PPD test,according to the outcome of test,The cases were divided into negative reaction group,positive reaction group and strong positive reaction group.All patients were received antituberculotic treatment.

将所有列入观察组的肺结核患者进行PPD试验,并根据皮试结果表现分为阴性反应组、阳性反应组以及强阳性反应组,分别给以抗结核治疗,观察不同PPD反应患者的痰菌转阴速度、空洞闭和速度以及疗程结束时病灶的吸收速度。

Results:according to the outcome of test,168 cases with new bacteriological positive ptb were divided into negative reaction group(group 1),positive reaction group (group 2)and strong positive reaction group(group 3).after antituberculotic treatment for 6 months.the rates of sputum coversion of group 1,group 2 and group 3 were 76.92%,94.79% and 100% respectively.the mean sputum coversion time of group 1,group 2 and group 3 were 12.46 weeks 5.0 weeks and 3.0 weeks respectively and the rates of focus absorption of group 1 ,group 2 and group 3 were 61.54%.

结果:168例痰菌阳性初治的结核病患者,根据ppd试验的结果分为阴性组,阳性组,强阳性组。经过6个月抗痨治疗后,ⅰ组痰菌转阴率为76.92%,平均转阴时间为12.46周,病人疗程结束时,肺内病灶x线吸收占61.54%;ⅱ组痰菌转阴率为94.79%,平均转阴时间为5.0周,病人疗程结束时,肺内病灶x线吸收占86.46%;ⅲ组痰菌转阴率为100%,平均转阴时间为3.0周,病人疗程结束时,肺内病灶x线吸收占100%。

To obtain antioxidative micrometer copper powder.Copper was plated with silver by substitutional reaction method. The effects of concentrations of argentamine,concentration of gelatin,and reaction temperature on reaction were studied.

为获得抗氧化微米级铜粉,采用置换反应法在铜粉表面镀银,研究了反应体系中明胶浓度、银氨浓度、反应温度对反应的影响。

We apply autocatalytic model to described the reaction of epoxy/amine systems. The parameters of the model can be obtained through DSC measurement and be used to adjust the curing time and temperature for the reaction. We have found the prediction of model is better fitting experimental results as the reaction temperature increases.

我们利用自催化模型来描述Epoxy/amine的反应过程,利用DSC得到此模型的四个反应参数,利用这些参数我们便可调控我们的交联温度与时间,在此研究中发现随著温度不断的提升,理论模型所预测的结果会与实验的结果越来越符合。

Six products were formed in the reaction between N-benzylideneaniline andethyl benzoate; two products were separated from the reaction between N- benzylidene-(4-chloro) aniline and acetonitrile; and three products were afforded in the reaction between N-benzylideneaniline and benzalazine.

亚胺和苯甲酸乙酯的反应得到六个产物,和乙腈的反应得到两个产物,和苯亚甲基联氮的反应得到三个产物。

The experiments also show that adding NaHSO3 into the reaction liquid of hydroxylation reaction can inhibit the catalytic effect of benzoquinone and residual catalyst on the phenolic tars formation caused by oxo-condensation of the diphenols and therefore reduce the tars formation of the diphenols in the reaction solution.

在羟基化反应液中加入亚硫酸氢钠可以抑制对苯醌和残留催化剂对苯二酚氧化缩合生成焦油的催化作用,从而减少了反应液中苯二酚的生焦反应。

The factors which affect the average molecular weight of the polymer of AM and DMDAAC were investigated. The optimal reaction conditions are as follows: the concentration of monomer AM was 30%, while DMDAAC was 5%; the reaction temperature was 30℃, the amount of initiators at the low temperature stage was 0.05‰(compared to the weight of the monomers joining the polymerization), while V-50 was 0.025‰, the weight ratio of potassium persulphate to sodium bisulphite is 1:1, the amount of carbamide was 40‰, and complexing agent was 0.05‰, besides, aerate nitrogen gas for 8min, then the high molecular weight polymer (M=1.217×10^7) could be got after 16h reaction.

研究了影响AM与DMDAAC共聚物的平均分子量的因素,得到了优化条件为:单体浓度为30%,DMDAAC与AM摩尔比为5:95,聚合温度为30℃,低温段引发剂用量为0.05‰,K2S2O8与NaHSO3质量比为1:1,偶氮二异丁基脒盐酸盐(V-50)用量为0.025‰,尿素用量为40‰,乙二胺四乙酸二钠(EDTA-2Na)用量为0.05‰,在此优化条件下聚合反应16h后得到分子量为1.217×10^7的阳离子型聚丙烯酰胺。

The optimal measuring conditions were investigated. The results indicated that the catalytic reaction to Pt and bromocresol purple was the first-order reaction. The apparent activation energy was 217.4kJ/mol and the maximum absorption wavelength of fading reaction was at 434 nm. The linear range of Pt was 0.16-4.0μg/L and the detection limit was 2.5×10^(-11)g/mL. Most of common ions had no interference with the determination, while ten multiples of Ru, Rh and Os had interference with the determination of Pt. Therefore.

选择了最佳测定条件,实验结果表明,催化反应对铂和溴甲酚紫为一级反应,反应的表观活化能为217.4kJ/mol,褪色反应的最大吸收波长为434nm,方法测定R哪的线性范围为0.16~4.0μg/L,检出限为2.5×10^(-11)g/mL,大多数常见离子不干扰测定,10倍以上的Ru,Rh和Os对测定有干扰,可在测定前分离除去。

The structural and photocatalytic properties of TiO〓 as well as surface acidity were greatly improved by sulfation. SO〓〓/TiO〓 solid superacid with Hammett constant Ho less than -12.14 was prepared by treating the TiO〓 with 1.0mol. L〓 sulfuric acid solution and then calcining at 450℃ for 3h. When compared to unmodified TiO〓, the SO〓〓/TiO〓 superacid catalyst exhibited higher anatase content, smaller crystal size, higher specific surface area, centralized pore size distribution, and the blue-shifted band edge of uv-vis adsorption spectra. Furthermore, the SO〓〓/TiO〓 superacid also showed excellent reaction activity and stability for CH〓Br photocatalytic decomposition even under the moist reaction conditions. The apparent quantum efficiency of SO〓〓/TiO〓 was 10 times of that of TiO〓 catalyst for the photocatalytic degradation of bromomethane. Therefore, the SO〓〓/TiO〓 superacid catalyst is promising for practical application in environmental remediation.It was found that both L and B acid sites exist on SO〓〓/TiO〓 photocatalyst while only L acid sites on TiO〓 photocatalyst. On the basis of experimental results, the synergistic model of superacidic centers was proposed for SO〓〓/TiO〓 photocatalyst to explain the photocatalytic behavior and the mechanism of superacidifing effects, assuming that the adjacent L and B acid sites induced by SO〓〓 comprise cooperatively the superacidic center on superacid photocatalyst. The group cooperation of the superacidic center could strengthen the surface acidity, increase surface acid sites and the adsorbtion of O〓, promote separation of photogenerated electron-hole pair, enhance the interfacial transfer of charges and reversibility of water adsorption. Consequently the excellent photocatalytic activity, reaction stability and resistibility to humidity of SO〓〓/TiO〓 superacid photocatalyst may attributed to the group cooperated effect of the superacidic center on the photocatalyst.

研究结果表明:SO〓〓与TiO〓表面的结合为螯合式双配位结构;TiO〓光催化剂表面经H〓SO〓浸渍处理后,提高了表面酸性,改善了催化剂结构和光催化性能,当H〓SO〓浸渍浓度为1.0mol.L〓、烧结温度为450℃时,可制得SO〓〓/TiO〓超强酸催化剂(H〓<-12.14),其结构和光催化活性得到明显改善,与TiO〓相比,SO〓〓/TiO〓光催化剂的锐钛矿含量高、晶粒小、BET比表面积大、孔径分布集中、光谱吸收边蓝移,具有优异的光催化氧化活性、稳定性及抗湿性能,光催化降解溴代甲烷的表观量子效率比TiO〓催化剂提高了一个数量级,是一种有实际应用前景的高效光催化剂;由此提出了SO〓〓/TiO〓超强酸催化剂表面集团协同作用的超强酸中心模型,认为在SO〓〓/TiO〓超强酸催化剂表面,由SO〓〓诱导的相邻L酸中心和B酸中心组成了集团协同作用的超强酸中心,其集团协同作用显著地增强了催化剂表面酸性、增大了表面酸量及O〓吸附量、促进了光生电子和空穴的分离及界面电荷转移,具有可逆吸附水的性能,是SO〓〓/TiO〓超强酸催化剂具有优异的光催化氧化活性、很好的活性稳定性及抗湿性能的重要原因。

In this paper isopropyl -γ- chlorobutyrate was prepared from γ- butyrolactone by one - step. The effects of molar ratio of reactants, reaction temperature, reaction time on the yield of product were discussed, the optimum reaction condition was obtained.

一氯代丁酸异雨酯是合成新型拟除虫菊酯中间体环丙烷较酸及高效抗菌新药丙氟见酸和环丙氟院酸中间体环丙胺的重要原料['']。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

The new PS20 solar power tower collected sunlight through mirrors known as "heliostats" to produce steam that is converted into electricity by a turbine in Sanlucar la Mayor, Spain, Wednesday.

聚光:照片上是建在西班牙桑路卡拉马尤城的一座新型PS20塔式太阳能电站。被称为&日光反射装置&的镜子将太阳光反射到主塔,然后用聚集的热量产生蒸汽进而通过涡轮机转化为电力