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It is the most important solid-liquid reaction that sulfuric acid decomposes phosphate rock in phosphate fertilizer production. By contrast with conventional reaction of acid decomposing phosphate rock, the effects of ultrasonic power, reaction time, and temperature are discussed.

硫酸分解磷酸是磷肥工业中最重要的液固分解反应,本研究从磷矿酸解液—固反应着手,通过对比的方法,探讨常规的液—固反应体系施加超声波后,超声的声强、时间、温度对磷矿酸解的影响。

This article analyzed the method of calcify reaction on oxalic acid process and put forward the conditions of calcify reaction and acidify reaction.

根据钙化法草酸生产工艺的研究,提出了钙化反应、酸化反应的工艺条

Effect of diamond grits as an additive on Ni-Al SHS reaction process was studied. The morphology of reaction products as well as the surface morphologies and the compressive strength of diamond after reaction were investigated.

本研究主要针对Ni-Al自蔓延反应燃烧过程和加入金刚石磨料后的变化,其反应产物的微观形貌,以及SHS反应后金刚石的表面特征及强度的变化进行的探讨。

Therefrom; heating said waste edible oil from which solid materials have been removed to a predetermined temperature, thereby removing moisture and materials of odor contained in the waste edible oil therefrom by evaporation; dissolving in alcohol a catalyst containing at least one type or more types of alkaline material selected from a group comprised of at least potassium hydroxide, potassium carbonate and potassium alcoholate, thereby preparing an alcoholic solution containing the catalyst; mixing said waste edible oil from which said solid materials, moisture and materials of odor have been removed with said alcoholic solution containing the catalyst and stirring the waste edible oil and alcoholic solution, thereby accelerating a catalytic reaction between the waste edible oil and the alcohol and obtaining a reaction product between the waste edible oil and the alcohol; separating said reaction product into a light solution and a heavy solution; mixing the light solution obtained in the separation step with a solid absorbent, thereby impurities such as residual catalyst, odor material, moisture contained in the light solution being absorbed by the solid absorbent; and separating and removing said solid absorbent from a mixture of the solid absorbent having absorbed the impurities and the light solution.

完成前述对象,根据这项发明的特点是获得的柴油燃油从废油脂透过几个步骤:去除固体材料包含在一个废油脂倾倒,从餐厅,食品厂,民政等因此;暖气说,废油脂从哪个固体材料已被调离到一个预定的温度,从而消除了水分和材料的气味,载于废油脂因此由蒸发;溶解在酒精的催化剂至少含有一种或更多类型的碱性材料选定由一组组成的至少氢氧化钾,碳酸钾和钾,醇,从而准备一醇溶液中含有催化剂;混合说,废油脂从哪个说,固体材料,含水率和材料的气味已被剔除与说,酒精性解决方案载有催化剂和搅拌废物食用油及含酒精的解决办法,从而加速催化反应之间的废油脂及酒精和获得反应产物之间的废油脂及酒精;分开说,反应产物成为一个轻型的解决方案和沉重的解决方案;混合轻解决方案,获得了在分离一步一个坚实的吸水性,从而杂质,如残留的催化剂,气味的物质,水分,载于轻解决方案,被吸收的固体吸收剂;分离和消除说,固体吸附剂从混合物对固体吸收剂吸收了杂质和轻便的解决办法。

The results show that the initial phase is non-homogeneous reaction,solid-liquid mass transfer coefficient is the main factor on the reaction rate,N-methyl-2-pyrrolidone can accelerate the dissolution of polyester film and prompte the alcoholysis reaction into homogeneous process.

结果表明,反应初始阶段为非均相阶段,固-液间传质系数是影响反应速率的主要因素,加入NMP可以加速PET的溶解,促使醇解反应快速进入均相阶段。

The effect to rate of production of the reaction active of different alkaline earth, the reaction efficiency of different low-carbon alcohols and reaction time were investigated.

考察了不同碱土金属、不同低碳醇及反应时间对醇盐产率的影响。

Alkylamine reaction with dialkyl cyanodithioiminocarbonate was catalyzed by quaternary ammonium salts at room temperature to yield 3-alkylamine-5-amino-1,2,4-triazole in good quality and high yields. After imidization and reaction with an α,β-unsaturated acid derivative, the reaction intermediate was hydrolyzed in the presence of a Lewis acid to obtain the target product.

烷基胺与氰基亚胺硫代二甲酯在季氨盐催化作用下得到质量好、收率高的3-烷氨基-5-氨基-1,2,4-三氮唑,进一步经过亚胺中间体并与α,β-不饱和酸酯作用后,中间产物在Lewis酸催化作用下水解得到三唑嘧啶酮。

2Obtained alkylate reaction technical parameter :reaction time of alkylate of rapeseed oil phospholipid was 2 hours . after 2 hours the reaction almost cease

2确定烷基化反应的工艺参数:菜油磷脂的烷基化反应所用的时间为2小时,在2小时之后反应基本停止

Then Doripenem came into the market in the July ,2005. We studied the synthesis of Doripemen.Firstly, we synthesized the chemical 2 from the starting material------o-hydroxylphenylacylamine through Reformastky reaction, alkylation, Diekmann reaction, enolization, esterification and etc. Secondly, we synthesized the chemical 3 from L — hydroxylproline through the protection of carboxyl, amidogen and hydroxyl group, reduction by NaBr, SN_2 substitution and Mitsumobu reaction.

我们以水杨酰胺为起始原料,经Reformatsky反应、烷基化、Diekmann环合、烯醇化、酯化等反应合成双环母核2;再从L-羟基脯氨酸出发,经酯化保护羧基、保护氨基、保护羟基、硼氢化还原酯得醇、Sn2取代和Mitsumobu反应等合成巯基侧链3;最后由化合物3经脱保护、水解得硫醇,和化合物2在二异丙基乙基胺的作用下缩合,最后Pd/C催化脱保护,历经16步反应最终得到产物多尼培南。

The result was showed that the optimal process conditions were presented as follows: molar ratio of methyl glucose amine to oleic acid 2.5, reaction time 8h, reaction temperature 90℃, and the catalyst dosage 1.5% to the oleic acid reaction.

结果表明,最佳工艺条件为:甲基葡萄糖酰胺和油酸的摩尔比为2.5,反应时间为8 h,反应温度为90℃,催化剂用量占油酸用量的摩尔分数为1.5%。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

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