查询词典 reaction rate

The studies showed that the optimum conditions of the reaction were the amount of the 75% gathers the phosphoric acid 30 mL,the mole ratio ofhexamethylene tetramine to nitrophenol was 2∶1,the reaction time was about 3.0 hours,the reaction temperature was about 105℃.

结果表明较佳反应条件是：在对硝基苯酚为3.5 g的情况下，75%的多聚磷酸用量为30 mL，n∶n=2∶1，反应时间为3.0 h，反应温度105℃，5-硝基水杨醛的产率可达68.1%。

The reaction of disproportionation of gum rosin catalyzed by AH nonnoble metal catalyst was studied, and the effects of reaction temperature, reaction time, particle size of catalyst, and stir speed were investigated.

用AH型非贵金属催化剂催化松香歧化反应，考察了搅拌速率，催化剂粒度，反应温度，反应时间对反应的影响，建立了动力学方程。

In the hydroxylation of phenol with H〓O〓 in the presence of Ti-ZSM-5, water is best solvent. It produces catechol and hydroquinone simultaneously, and catechol/hydroquinone ratio is approximately 0.85. The results show H〓O〓 utilization ratio increase 14%, when nonoxidizable weak acid HAc is added into the reaction system. Under the conditions of Ti-ZSM-5 as catalyst, phenol/H〓O〓 ratio being 10, a little HAc, temperature 75℃, reaction time 6h, H〓O〓 utilization ratio reaches 74. 6mo1% in the reaction.

对Ti-ZSM-5催化苯酚羟基化的研究结果表明，水是最好的溶剂，羟基化有邻、对苯二酚两种产物，并且邻苯二酚/对苯二酚摩尔比可维持在～0.85左右；向反应体系中加入非氧化性弱酸性助剂HAc时，H〓O〓有效利用率较未加入助剂时可提高14mol%；当催化剂用量为8g/100g苯酚、苯酚/H〓O〓比为10、反应温度75℃、添加少量HAc的条件下，反应6h后，H〓O〓有效利用率可达74.6mol%。

The resules show that the optimal reaction conditions are as follows: tin octoate is used as catalyst; w(SnOct2)lw and w(nano-SiO2)/w is 1:400 and 1:20, respectively; the reaction temperature is 140 CC and the reaction time is 72 h. Under this conditions, composite withM of 1.5091×10^5 was obtained.

结果表明，最优的反应条件为：采用辛酸亚锡为催化剂，催化剂用量和二氧化硅用量分别为丙交酯用量的0.25%和5%，在140℃油浴中，氮气保护下反应72h，可得到重均分子量为1.5091×10^5的聚乳酸纳米二氧化硅复合材料。

In order to solve the problems such as multiple components in products, long time of rectification, high energy consumption, low yield and purity of product occurring during the production of p - octyl phenol, the effects of reaction conditions including reaction temperature, reaction time, the molar ratio of phenol to diisobutene on the conversion and yield of the product were examined.

为解决对辛基酚生产过程中精馏时存在组分多、精馏时间长、能耗高、产品收率和纯度低等问题，用正交实验探讨反应温度、反应时间、苯酚与二异丁烯原料摩尔比3因素对原料转化率和产品对辛基酚收率的影响。

Thus, in order to attain acetal can be used as precursor of its matrix olefine aldehyde, 2-undecental glycol acetal was synthesized, and the corresponding optimum reaction conditions as: 2-undecental 0.2mol, glycol 0.3mol, cyclohexane as solvent, catalysed by vitamin C, the optium reaction time was 6h, its reaction yield could reach over 77.25%.

为了进一步探求效果更理想的前体化合物，本文继续合成了2-十一烯醛乙二醇缩醛，通过单因素优化实验得到最佳反应条件为：环己烷作溶剂，VC作催化剂，用量0.42%，醛醇物质的量之比0.2：0.3，反应时间6h，此条件下产品收率达77.25%。

The reaction has been drawing increased attention in that the reaction permit the use of organoboron compounds that are thermally stable and inert to water and oxygen.In this section microwave promoted Suzuki reaction of Sodium tetraphenylborate (NaBPh4) with carboxylic anhydrides catalyzed by Pd(PPh3)2Cl2 in THF was first reported.

第二章：微波辐射下Pd配合物催化NaBPh_4与羧酸酐的偶联反应研究本章中我们在微波辐射条件下，研究了PdCl_2(PPh_3)_2催化NaBPh_4与羧酸酐偶联反应，合成出了十种不对称芳酮，并分别考察了微波辐射功率、辐射时间、溶剂和原料配比等因素对反应的影响，优选出了较佳的反应条件，并根据文献及实验结果，讨论了可能的反应机理。

Meantime, we further studied this reaction under microwave irradiation conditions and first introduced the concept of the solvent-free and no-catalyst in this reaction, expanded the olefination of organozinc halides reagents with aldehydes, enlarged the application scopes of this reaction.

同时在微波辐射条件下进一步研究了该类反应，并在该类反应中初步引进无溶剂、非催化的概念，扩展和完善了有机卤化锌试剂与醛的烯基化反应，扩大了其应用范围。

Products have good thermal stability anddecomposition temperature above 200℃; Selected lauryl amine as a case, then optimizedthe synthesis conditions by orthometric trial, and obtained the best synthesis technichs: themolar ratio of 1: 2.1, the reaction temperature was controlled at 80℃and the reaction timeof 16 h, reaction to the solvent n-propanol.

并对其热稳定性进行了分析，合成产物具有较好的热稳定性，分解温度都在200℃以上；以十二胺为例，用正交实验法优化合成条件，获得最佳合成工艺为：摩尔配比为1：2.1，反应温度控制在80℃，反应时间为16h，反应所用的溶剂为正丙醇。

Reaction of 9-bromofluorenewith diethyl malonate and sodium carbonate gives diethyl 2-(9-Fluorenyl)malonate.Aminolysis of diethyl 2-(9-Fluorenyl)malonate in ethylenediamine and propylene diamine give〓 and 〓, respectively.〓 and 〓 were synthesized by the reaction of 9-bromofluorene with oxalyl bisethylenediamine. Copper and nickel complexes of 〓 and 〓 were obtained by the reaction of 〓 and 〓 with copper and nickel salt, respectively, in aqueoussolution and extrusion of two hydrogen ions from the amide groups.

使9-溴芴与丙二酸二乙酯在无水碳酸钠存在下反应合成出2-(9-芴基)丙二酸二乙酯。2-(9-芴基)丙二酸二乙酯在乙二胺中胺解得到配体〓，2-(9-芴基)丙二酸二乙酯在1，2-丙二胺中胺解得到配体〓，使9-溴芴与草酰二乙二胺作用得到配体〓和〓与相应的金属盐作用分别得到它们的铜、镍配合物。

As of Tuesday, Google's results were still censored in China.

截至周二，谷歌的搜索结果仍受中国审查。

In order to make the positive action increase and negative one decrease, the sub-forces of the social factors must be adjusted to form a centripetal force.

在这一过程中，人的主体性发挥是社会有机体健康发展的灵魂。