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The results indicated the order of factors that influence the oil transesterification ratio within the experimental range was as follows: the rate of rotation r>catalyst dosage>mole ratio of methanol to Kosteletzkya virginica oil >reaction time>reaction temperature.

结果表明,在试验范围内各影响因素对酯交换率作用的大小依次为:搅拌强度>催化剂用量>醇油摩尔比>反应时间>反应温度。

The optimal technological parameters of oil transesterification from Kosteletzkya virginica oil should be as follows: the rate of rotation 1800r.min-1, catalyst dosage 0.6%, mole ratio of methanol to Kosteletzkya virginica oil 6/1,reaction time 60min and reaction temperature 65℃, and under such conditions, the total oil transesterification ratio after transesterification three times is 97.8%.

海滨锦葵油制备生物柴油的最佳工艺参数为:搅拌强度为1800r.min-1,催化剂KOH用量为海滨锦葵油质量的1%,醇油摩尔比6/1,反应时间60min,反应温度65℃,在该工艺条件下,酯交换反应三次,酯交换率达到97.8%。

During preparation, mercapto ethanol isooctanoate, alkyl or ester tin chloride and organic solvent are first heated and refluxed while adding catalyst; organic layer is then obtained through separating liquid and decompression distilled; and through further steps, the compound is obtained. The synthesis process of the present invention is simple, and has conversion rate higher than 95 %, normal pressure and low reaction temperature, low power consumption and less pollution, and the prepared compound has high reaction activity and low toxicity.

制备时,将异辛酸巯基乙醇酯、烷基或酯基氯化锡和有机溶剂加热回流,同时加入催化剂,然后通过分液,保留有机层,再对有机层进行减压蒸等步骤制得所述化合物;本发明合成工艺简单,转化率大于95%,反应在常压条件下,反应温度低,从而降低了能耗,减少了污染,所制备的化合物具有反应活性高和毒性小的特点,使用安全。

Compared with oxygen as an oxygenant, the advantages of this method are that reaction time is shorten to half, reaction temperature is lowed about 40℃ and utilization rate of ammonia is increased.

与用氧气作氧化剂相比具有不需耐压设备,反应时间缩短一半,反应温度降低40℃左右,氨利用率提高的优点。

Study the bioactivity of the n-HA/PA66 composite and the effects it would be to body's metabolism of calcium and phosphorus ion in vivo.(3) Study the osteo-conductivity and the ability to repair bone defect of the porous n-HA/PA66 composite and the feasibility use it as the scaffold of bone tissue engineering. Objects and Methods as follows: 1.To evaluate the biocompatability of nano-hydroxyapatite crystals and polyamide composite (n-HA/PA66) with the L929 cells.To proceed the morphological observation and take pictures of L929 cells after 1d,2d,4d,and 7d of co-cultured with extract of n-HA/PA66 ,and direct contact with n-HA/PA66.To determine light absorbtion value of every hole under 500 nm with enzyme linked immunity instrument after 1 d,2 d,4 d,and 7 d of contact of n-HA/PA66 extract with L929 cells,and direct contact with n-HA/PA66.In the meanwhile calculate the relative multiplication rate of cells,and evaluate them by six degree tests for cytotoxicity. To investigate the acute and chronic toxic reaction on the whole body induced by the new nano-hydroapatite crystals and polyamide composite(n-HA/PA66)after implanting in vivo and its effects on partial constitution of animal organs after implanting in vivo,and evaluate the potential and degree of subcuticular stimulation reaction.

本实验主要由以下三部分组成:一、n-HA/PA66 复合材料在动物体内、体外的生物相容性及生物安全性评价二、n-HA/PA66 复合材料植入动物体内的生物活性及近期对机体钙、磷代谢影响的实验研究三、网孔 n-HA/PA66 复合材料作为支架修复兔桡骨节段缺损的动物实验研究主要研究目标及方法如下:参照 GB/T16886.5-1997-ISO 10993-5:1992《医疗器械生物学评价细胞毒性试验体外法》之评价标准和要求,采用规定的 L929 细胞(小鼠结缔组织成纤维细胞),分别经直接接触和材料浸提液与细胞共培养等方式对 n-HA/PA66 复合材料进行细胞毒性测试,采用细胞形态观察法观察两种细胞各组在 24h、48h、72h、5 天后各时相点的细胞形态学变化,并在显微镜下照相,从而对细胞与材料的生物相容性进行定性评价;同时采用细胞生长抑制法,以酶标仪定量测定评价各组 1,2,4,7 天 L929 细胞的相对增殖率,以定量测定并判别材料对细胞的毒性程度。

Sulfuric acid was sulphonation reagent, add the sulfuric acidquantity was 8%, reaction temperature was 60~65℃.The reaction occursbetween the feed oil and sulfuric acid,then add 30% of sodium hydroxidesolution conducted neutralization in the Pyrex standard react kettle,when the reactionfinished ,draw out the products by funnel,then the products react with 8%clay to refine received the sulphonation refining oil so as to review property andreceive rate of the shallow sulphonation refining oil .By the using the sulphonationrefining oil to blend lubricant,its quality is on-specification .

为验证其可行性,首先在实验室进行浅度磺化小试,原料油采用新疆原油经常压蒸馏、减压蒸馏、溶剂精制、溶剂脱蜡后的减压二、三线脱蜡油,发烟硫酸作为磺化剂,发烟硫酸加入量8%,反应温度60~65℃,用三口圆底耐热玻璃标准反应釜对原料进行发烟硫酸磺化,加入量30%氢氧化钠中和,分液漏斗抽提,在烧杯内加入量8%白土进行精制得到磺化抽余油,考察浅度磺化抽余油性质和收率,用磺化抽余油调合润滑油质量合格。

Studies on the trinitration of toluene showed that, the trinitration temperatures were high enough to intensify oxidation, and the two thermal hazard evaluation methods mentioned above couldn\'t evaluate the situation well. Results were found from the reaction calorimeter experiments that lower reaction temperature and decelerating dosing rate could prevent thermal accumulation and decrease thermal hazard efficiently.

在对三段硝化反应进行热危险性评估时发现,三段硝化反应的温度很高,氧化副反应随温度升高而加剧,风险矩阵法和失控情景分析方法难以准确评估该情况下的热失控危险,但实验结果表明降低反应温度,减缓加料速率能有效地防止热积累,减小反应过程中的热危险性。

MAP is a kind of fertilizers which can be sold for reducing the expense of chemical precipitation method running. Though large numbers of experiments some kinetic parameters, including the value of pH, the relationship between the rate of ammonia-nitrogen removal and the ratio of reagents selected in reaction, reaction time and speed of whisking and so on were obtained.

在大量实验的基础上,通过对反应的几个动力学参数的详细研究,总结出了pH 值、反应药剂配比等与氨氮去除率的关系,并通过正交试验设计与单因素分析得出该方法在处理高浓度氨氮废水中最佳的工艺条件。

The ISSR fingerprinting of 18 Japanese plum cultivars and 12 plum species or variety were established by using optimum system with primer 5"-9T-3"and 5"-9C-3", respectively. The identification rate of plum cultivars and species or variety was 100%. The effects of five important components on reaction of SSR were studied with Prunus salicina cv. Meilili. The results showed that the optimum concentration of five important components i.e. Tag DNA polymerase, Mg +, single primer, template DNA and dNTPs in 25 μL reaction system of SSR were 1.5u, 2.0mM, 0.8 μ M, 30~40ng and 0.16~0.24mM, respectively. The dendrograms of these cultivars was contructed according the Jaccard coefficient of similarity.

利用该优化体系,以5′-_9T-3′为引物,构建了中国李18个品种的ISSR指纹图谱,该引物可将这些品种完全区别开来;以5′-_9C-3′为引物,构建了李属6类种质资源的ISSR指纹图谱,该引物区分率为100%。4、中国李品种适宜的SSR反应分析体系是:25μL SSR反应体系中,Taq DNA聚合酶、Mg~(2+)、每个引物、模板DNA和dNTPs等5种成分的适宜浓度分别是:1.5u、2.0mmol·L~(-1)、0.8μmol·L~(-1)、30~40ng和0.16~0.24mmol·L~(-1)。5、采用RAPD、ISSR和SSR等三种分子标记技术对中国李品种资源54份和2个欧洲李品种进行了遗传多样性分析,并以品种间的遗传相似系数构建了Jaccard聚类树状图。

In this paper, the principle of membrane humidification is analyzed, and the effects of humidifying temperature, reaction gas pressure, reaction gas flow rate and power of hot water pump on humidification function are studied systematically.

初步分析了膜加湿的原理,并在不同操作条件下,定量地对膜透过水量与反应气体的润湿程度进行了测量,得到了Nafion115膜加湿器对电堆的润湿性能。

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呼气,收缩臀部肌肉;拱起身体,尽量抬起头来,右腿伸直朝向天花板(膝微屈,以避免肌肉紧张)。

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然而,要让一个真正的引用,你需要提供详细的个人和财务信息。