查询词典 pyridine

The thesis consists of two main sections. The synthesis of 1,3,4-thiadiazoles,triazolotriazines and dioxapyrrolinopyrazoles containing chiral pyrazolyl moietyfrom D-glucose is described in the first part and the section one is about theDiels-Alder reactions between dienophile enaminones and diene 1,2,4-triazines,which provides a new methodology to construct the pyridine compounds. A total of37 new compounds were synthesized.

本论文包含两部分内容，一是以D-葡萄糖为原料合成含手性吡唑基的1，3，4-噁二唑、三唑并三嗪及二氧代吡咯啉并吡唑类化合物；二是将烯胺酮作为亲双烯体，与双烯体1，2，4-三嗪类化合物发生Diels-Alder反应，发现了一令人意外的构建吡啶类化合物的新方法。

With sodium acetate as catalyst, inosine was esterified with acetic anhydride in the yield of 92% to give 2',3',5'-triacetyl inosine, which was treated with pyridine and phosphorus oxychloride to form a pyridinium solution, followed by performing an amination at 40℃ and 0.25~0.30 MPa to achieve adenosine in the yield of 67%.

肌苷在醋酸钠存在下与醋酸酐发生酯化反应以92%的收率得到2'，3'，5'-三乙酰肌苷，其化合物经吡啶和三氯氧磷处理形成吡啶盐溶液，未分离直接在40℃、0.25~0.30 MPa压力下进行氨解反应以67%产率制得腺苷。

The nitrogen in the coal exists in the forms of pyridine (N-6), pyrrolic and pyridone (N-5), quaternary nitrogen and nitrogen oxides. The N-Q near 401.5eV is assigned to a protonated or oxide form of pyridinic nitrogen. On this basis, the nitrogen in six-membered rings is the dominant in Yibin coal.

研究结果表明，宜宾煤中氮的官能团有4种，即吡啶(N-6)、吡啶(N-5)、质子化吡啶和氮氧化物，其中吡咯含量最大，煤中的N-X就是N-O，是煤中吡啶结构氮与氧直接结合的结果。

Macrocycle with two pyridyl unitsZ-protected groups in the di-ester formed from esterification of Z-Glycine with 2,6-bishydroxymethyl pyridine was removed and thenconverted into Ts-protected group.

本论文以天然氨基酸为手性源，以芳杂环为大环分子的刚性因素，研究它们的环合反应和分子结构，为此设计了下列三种结构类型的大环分子：一。

A liquid crystal with pyridine group was synthesized from reactants of pyrogallic acid and isonicotinato by esterification reaction.

以焦性没食子酸和异烟酸为原料合成了带吡啶官能团的液晶配体。

This study discussed the composition of coal pyridine soluble from column-chromatography and the Soxhlet extraction method.

本研究以吡啶为溶剂，对准葛尔黑岱沟、平朔、潞安常村3种不同变质程度的煤样进行了柱色谱分离和索氏抽提。

It is found that when the molar ratio of sulphoxide,pyridine and acetyl bromide is 1∶0.6∶0.4,the catalytic effect on the ring-enlargment is the best,and the yield and purity of the final product can reach 76% and 97% respectively at a pH of 1.8 in toluene under refluxing for about 3.5h.

通过正交实验可得出以下结论：当N，N′-双脲-亚砜为2.5∶1，乙酰溴-亚砜为0.4∶1，吡啶-乙酰溴为1.5∶1，回流时间为3.5h，酸化pH值为1.8时，扩环反应结果最好，总收率可达76%，纯度97%以上。

To economize cost of S03H-functionalized ionic liquids,extend their range of application in chemistry reaction,fifteen of ionic liquids have been synthesized by using methylimidazole,tri-alkylamine,pyridine with industrial materials 1,4-butane-sultone and 1,3-propane sultone as source in this paper.The ionic liquids were synthesized by tri-alkylamine have not been reported and yields are higher than 98%.

为了降低SO_3H-功能化离子液体的成本，使其应用范围更加广泛，本论文利用N-甲基咪唑、三烷基胺、吡啶和廉价工业级原料1，3-丙烷磺内酯、1，4-丁烷磺内酯为原料来源，合成十五种SO_3H-功能化离子液体，三甲胺为原料合成的SO_3H-功能化离子液体还未见文献报道，收率大于98%。

A gelator (G2) synthesized from 1,2,4,5-benzene tetracarboxylic acid and 4-hydroxy pyridine at molar ratio of 1:4 was characterized by 1H-NMR and FT-IR.

采用1H-NMR和FT-IR表征了在摩尔比1：4条件下，由均苯四甲酸和对羟基吡啶合成的一种凝胶因子(G2)。

Compared with G1 synthesized from 1,2,4,5-benzene tetracarboxylic acid and 4hydroxy pyridine at molar ratio of 1:2,G2 gelled water at higher minimum gelator concentration and gave the gel with lower gel-to-sol dissociation temperature at the same concentration.

相对于在摩尔比1：2条件下，由均苯四甲酸和对羟基吡啶合成的凝胶因子G1，在相同浓度下，G2在更高的最低凝胶因子浓度使水凝胶，并且得到的凝胶具有更低的凝胶-溶胶破坏温度。

Fancy gold-plated dangling earrings with facetted White Opal crystals.

花式镀金悬垂耳环与facetted白欧泊水晶。

This essay chooses the study aim from biology teachers in middle school in Shi Jiazhuang which tells us that most of the middle school biology teachers in Shi Jiazhuang have the"burnout", lower successfulness, individualize.

本文选取石家庄市初中生物教师作为研究对象，运用问卷调查的方法对石家庄市初中生物教师职业倦怠的现状进行调查，调查结果发现，石家庄市初中生物教师这一群体普遍存在职业倦怠，情感枯竭程度偏高，成就感偏低，去个性化程度最为严重。