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The invention relates to a method for preparing dimeric acid methyl ester and dimer acid thereof.

本发明是一种制备二聚酸甲酯及其二聚酸的制备方法,以不饱和脂肪酸甲酯含量较高的混合脂肪酸甲酯或混合脂肪酸为原料,浓硫酸为助催化剂,无水氯化铝或无水氯化锌为催化剂,采用两步催化法进行二聚化反应。

On the basis of the study of the low heating solid state reaction of the above mentioned inorganic compounds with NaOH, a method of preparing nanometer NiO through discomposing the precursor at higher temperature is built, the main factors of influencing the size of product are discussed, and the nanometer NiO particles whose average diameter are 5nm and 25nm are prepared respectively.

以无机化合物与NaOH的低热固相化学反应的研究为基础,建立了低热固相反应—高温分解法制备纳米NiO的工艺,研究了影响粒子粒径大小的主要因素,制得了平均粒径分别为5nm和25nm的纳米NiO产品。

for preparing n-boc or n-cbz derivatives of chiral alpha,alpha'-disubstituted pyrrolidines containing olefinic bond and acetylene bond

一种制备含烯键和炔键取代基的手性α,α'-二取代吡咯烷的n-boc或n-cbz衍生物的方法

The new process for preparing 4,4"-Diaminostilbene-2,2"-disulfonic acid was characterized by carrying out the catalytic hydrogenation of 4,4"-dinitrostilbene-2,2"-disulfonic acid or its alkali salts in presence of both Pd/C and OVN in water, the amount of OVN ranging from 0.1 to 0.2% by weight of 4,4"-dinitrostilbene-2,2"-disulfonic acid or its alkali salts, yielding 98.7% of desired product with 99.3% purity.

确定了氧化缩合反应的较佳工艺条件,DNS收率达95.2%,纯度达到了99.1%。而在本论文所确定的还原反应最佳条件下,DSD酸的收率可达98.7%,纯度高达99.5%。

Mathematician, biologist, chemist and computer expert get edificatory from which, preparing tomorrow in collaboration...

数学家、生物学家、化学家以及计算机专家从中得到启迪,正在合作研制未来。。。

To study the law of preparing paraffin which be used in the phase-change thermostatic vavle, The samples were made by mixtures of eicosane and octadecane with different proportion. The samples were investigated by DTA analysis and measurement of melting point.

为研究应用在蜡式温阀中的感温石蜡的调配规律,使用十八烷与二十烷以不同比例进行混合,测量每组样品的熔点,再对样品进行DTA差热分析。

Subsequently, the methods for preparing electrochemical sensors and immobilizing bioactive molecules and their application in electroanalytical chemistry were also summarized.

全文共分五章: 1、绪论首先评述了各种类型模拟酶的研究、应用及发展,然后评述了电化学传感器的制备方法、生物活性分子的固载方法及在电分析化学中的应用。

The invention relates to an electrochemical method for preparing ultra-fine tantalum powder, wherein it uses the mixture slat flux with CaCl2 or CaCl2 as electrolyte; composites Ta2O5 powder/block with metal collector as solid cathode; uses graphite or inertia anode as anode; uses reference polar to control the electrolysis level, under inertia gas to electrolyze at 500-1000Deg. C; and the electrolysis time should make electrolysis electricity reach needed amount; reduces Ta2O5 into ultra-fine metal tantalum powder.

本发明涉及一种超细钽粉的电化学制备方法,以CaCl2或者含有CaCl2的混盐熔体为电解质,将Ta2O5粉末或块与金属集流体复合作为固态阴极,以石墨或惰性阳极作为阳极,用参比电极控制电解电位在惰性气氛保护下进行电解,电解温度控制在500-1000℃,控制电解时间使电解电量到达到理论所需电量及以上,将五氧化二钽电化学还原为超细金属钽粉。

It is necessary for preparing the Y-Ba-Cu-O superconducting ceramic with high quality that the equilibrious liquid phase in the sintering should be prevented by selecting ceramic composition or sintering temperature.

在此基础上,独创了银套Bi-Pb-Sr-Ca-Cu-O超导带的升温处理新工艺,试验了Y-Ba-Cu-O超导陶瓷变氧压处理作低温织构生长的可能性。

This experiment uses lime carbonate, kaolin clay and starch as filler, uses sorbitol, ethanediol and chitosan as hygroscopic agent, under without foaming and foaming systems conditions, study filler and hygroscopic agent affect on tear strength, tensile strength, moisture coefficient and gas permeability of this film, and research mechanics of ventilation and moisture-penetrability of experiment preparing PE film by SEM.

本实验以碳酸钙、高岭土和淀粉为填料,山梨醇、乙二醇和壳聚糖为吸湿剂,分别在无发泡体系和有发泡体系的PE薄膜中,研究填料和吸湿剂对聚乙烯微孔薄膜的撕裂强度、拉伸强度、透湿系数和透气性能的影响。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。

There is no differences of cell proliferation vitality between labeled and unlabeled NSCs.

双标记神经干细胞的增殖、分化活力与未标记神经干细胞相比无改变。