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The results show that the SAPO–5 has a pillar-like morphology with the size of about 20 μm×5 μm×5 μm.The ratio of P:Al:Si is 1:1.19:0.67 in its crystal structure, the content of Si is high. The total acidimety fo the SAPO–5 is 578.0 μmol/g , hihger than that of prepared by one step crystalline hydrothermal method.And its initial catalysis character performance on normal butane isomerization reaction reach 24.8 %, higher than that of prepared by one step crystalline hydrothermal method.

实验结果表明：产物为柱状的磷酸硅铝分子筛，其晶粒尺寸大约为20 μm×5 μm×5 μm，其晶体结构中P：Al：Si＝1：1.19：0.67，硅含量较高；采用分段晶化方式制备的SAPO-5分子筛的总酸量为578.0 μmol/g高于一段晶化方式制备的SAPO-5分子筛的总酸量；采用分段晶化生成的SAPO-5分子筛的催化正丁烷异构化反应初始活性可达到24.8 %，远高于一段晶化制备的SAPO-5分子筛的初始活性14.1 %。

The phosphotungstic acid and the silicotungstic acid are prepared firstly, and the Keggin structure of them is also confirmed by IR spectrum. Then the HPWA/SiO2 and HSiWA/SiO2 are prepared by impregnation, and IR spectrum and UV spectrum are used to characterize the Keggin structure of them.

通过经典酸化－乙醚萃取法制备了钨磷酸和钨硅酸，并用红外光谱证明其具有Keggin结构；再用传统浸渍法对制备的钨磷酸和钨硅酸进行SiO2固载化，然后重点对杂多酸在固载化后Keggin结构是否依然保持进行了研究。

The design, synthesis of crosslinked poly-salenCo complexes and their application in the HKR of terminal epoxides Di-salicylaldehydcs and tri-salicylaldchydes S-3, S-4, S-5 were synthesized from some easily prepared acids. The crosslinked polymeric ligands could be prepared by condensation of -1, 2-cyclohexanediamine stoichiometrically with a mixture of S-3 and S-4 in different proportions, polymeric catalysts were obtained by inserting the Co atoms to the ligands.

四 交联poly-salenCo络合物的设计合成及其在末端环氧化合物的HKR中的应用以几种易得的羧酸为骨架，设计合成出了相应的双水杨醛和三水杨醛S-3、S-4、S-5，将双水杨醛S-3和三水杨醛S-4按不同比例混合后再与手性环己二胺缩合制备出交联聚合物配体，该配体与Co络合后得到交联聚合物催化剂。

A kind of BaTiO3/epoxy composite material with high dielectric constant and low dielectric dissipation was prepared by mixing method. The composite was prepared with BaTiO3, epoxy resin CYD128, 4, 4-diaminodiphenyl sulphone and nitrile-butadiene rubber.

以BaTiO3、CYD128型环氧树脂、丁腈橡胶和4，4-二氨基二苯基砜为原料，采用共混法制备了具有高介电常数和低介电损耗性能的BaTiO3/环氧复合材料。

And the healing agent containing both multiply vinyl group and double SiH bonds was prepared by reducing the oligomer by lithium aluminum tetrahydride.,dichloropolymethylvinylsiloxane was prepared by hydrolyzing partially of MeViSiCl2 under nitrogen protected in ether.

甲基乙烯基二氯硅烷在氮气保护下，以乙醚为溶剂进行非充分水解，得到，二氯聚甲基乙烯基硅氧烷，再经过LiAlH4还原可得兼有多个乙烯基和两个SiH键的自修复单体。

The results showed the masterbatch prepared from EVOH/compatibilizer,HDPE and EVOH/compatibilizer(4:1)was used as barrier masterbatch,the prepared material had an obvious and homogeneous toothlike structure,having good barrier property.

结果表明采用EVOH／相容剂和HDPE、EVOH制备的母粒能明显改变材料的流变性能，当采用EVOH／增容剂为4／1的阻隔母粒，所得材料的结构为大而均匀的片状形态，具有优异的阻隔性。

Aim to the application purpose of all-solid state electrochromic device and electronic link materials, which are prepared on flexible substrate. The tungstenic acid sols doped with PEO, MoO_3 and the PEO6000 nano-sized composite Ni_2 sols were prepared by ionic- changing and alcohol salt hydrolyzing technology of sol-gel method.

本论文以全固态的电致变色显示器件和柔性基板电子墨水显示材料为应用目标，采用溶胶-凝胶技术中的离子交换法和醇盐水解法分别制备了PEO、MoO_3掺杂的钨酸溶胶和PEO掺杂Ni_2的复合溶胶体系。

The reaction results show that the catalytic activity and selectivity of W-HMS prepared with tungstic acid is better than that prepared with sodium tungstate. And the consumption of t-BuOH also is successfully reduced.

实验结果表明：钨酸是制备W-HMS催化剂很好的钨源，以钨酸为原料制备的催化剂具有很高的催化活性和选择性，使溶剂叔丁醇用量大为减少。

Compared with the unactivated P polyelectrolyte film, the activated form P/PMMA polyelectrolyte film obtained by adopting the technology of the invention has better absorbency, room-temperature conductivity, electrochemical stability and the interface stability of electrolyte and lithium electrode; the performance of a lithium secondary battery prepared by using activated electrolyte is obviously better than the performance of the lithium secondary battery prepared by using the unactivated polyelectrolyte; the invention has simple technology, short reaction time, and convenient and easy condition for technologized production.

采用本发明技术获得的活化型P/PMMA聚合物电解质薄膜相比未活化的P聚合物电解质膜，有更好的吸液性和室温电导率，更好的电化学稳定性及电解质和锂电极的界面稳定性；用活化后的电解质制备的锂二次电池性能明显好于未活化聚合物电解质制备的锂二次电池；本发明工艺简单，反应时间短，为工艺化生产提供了简便易行的条件。

Ceramic-veneer Composites is a three-layers plywood prepared by heat pressing, which composes of ceramic-veneer on the surface and unworked veneer inside. Ceramic-veneer is a material prepared by Sol-Gel method and Vacuum-Pressure method, and constitutes with veneer and ceramic emulsion.

摘 要：陶瓷化单板表层复合材料是以陶瓷化单板为表层材料，未处理木材单板为芯材，经热压工艺制备而成的三层胶合板；陶瓷化单板是以木材单板为基材，陶瓷前驱液为浸注剂，采用溶胶-凝胶法经真空加压浸渍处理而成。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。