查询词典 phase

Onsidering the crystallographic and the phase stability information, a new model,〓, was used to describe the NiTa phase.

ALPHAD技术是目前最为成熟而且用途最为广泛相图评估和预测手段，它不仅是材料动力学及由此产生的组织演变的计算机模拟的理想的热力学平台，而且在新材料的设计与研制中有着更为直接而广泛的应用。

The effects of the reaction temperature, the ratio of fluorous phase and organic phase and the water in the reaction system on the nitration were investigated.

考察了反应温度、氟相和有机相的体积比与体系中的含水量对氟两相硝化区域选择性的影响。

The conclusions were as follows: theνO-H andνC=O IR absorption maxima shifted towards higher wave numbers after imprinting 17β-estradiol on TFMAA-co-TRIM copolymer with the red shift of theνO-H groups being apparent after precipitation polymerization for 16h while that forνC=O groups being observed after polymerization for 24h. A strong interaction between TFMAA and 17β-estradiol was confirmed by the high selectivity for 17β-estradiol, as indicted by the values of the separation factor of isomers of 17β-estradiol/17α-estradiol (2.28) and the imprinted factor (3.01). Particle diameter of TFMAA-co-TRIM polymer was between 300 nm and 1.5μm, which suited well for solid phase sorbent throughout at low column pressure. The recognition of imprinting TFMAA-co-TRIM polymer for sterol molecules was driven by enthalpy eluted with acetronitile, and low temperature was in favor of the separation of sterol structure analogues on imprinting column. TFMAA-co-TRIM polymer possessed of determinate anti-heat stability, with melting point beginning at 255.84℃, Tp=257.40℃, control TFMAA-co-TRIM polymer and imprinting TFMAA-co-TRIM polymer were respectively decompounded at 267.79℃and 343.11℃, and solid micro-extraction noddle prepared by the special polymerization also showed definite recognition for 17β-estradiol by GC/MS detecting at 270℃. By selection of various washing and elution solvents, elution reagents of close polymerization system were of more advantage in template molecules retention and recognition on molecularly imprinted solid phase extraction column. At a certain extent, progesterone, 17α-estradiol, 17β-estradiol and 4-androstene-3, 17-dione could be intercepted on the MISPE column. Especially, MISPE had high selectivity for progesterone, and imprinting TFMAA-co-TRIM polymer could achieve adsorption balance within 50 min by absorption kinetics test for 17β-estradiol. However, MISPE column showed better selectivity and enrichment property for 17β-estradiol than C18 and CSPE columns according to the data from HPLC and GC/MS analyses. Recovery of 17β-estradiol on MISPE column was up to 85.5% while when prime extracting solution of milk powder was sampled, the recovery of CSPE and C18 columns were 43.7% and 30.7%, respectively.

通过研究阐明：紫外聚合产物TFMAA-co-TRIM中的νO-H振动吸收峰在聚合16h后红移，νC=O振动吸收峰在聚合24h后红移；TFMAA-co-TRIM对雌二醇异构体的印迹因子达到了3.01，α为2.28，优于其它功能单体参与得到的聚合物识别特性；TFMAA-co-TRIM聚合物粒径介于300 nm至1.5μm之间，作为色谱固定相具有良好的通量和低的柱压；在乙腈流动相中，TFMAA-co-TRIM分子印迹固定相的分离过程主要被焓驱动，低温有利于分子印迹固定相分离甾醇结构类似物；TFMAA-co-TRIM分子印迹聚合物在255.84℃时开始熔融，Tp=257.40℃，聚合物CP的降解温度在267.79℃，MIP降解温度在343.11℃，制备的固相微萃取头初步经GC/MS 270℃的耐热性测定；不同的洗提溶剂筛选证明了选择接近聚合溶剂的洗脱体系更有利于MISPE发挥识别效应；分子印迹固相萃取柱对孕酮、17α-雌二醇、17β-雌二醇和雄烯二酮都具有不同程度的保留特性，可作为此类化合物的吸附材料，特别对孕酮强保留的富集特性，可作为孕酮的选择性识别吸附剂，其分子印迹聚合物对17β-雌二醇的吸附动力学测定显示在50 min内基本达到吸附平衡，具有作为传感器核心敏感材料的潜力；对比萃取奶粉中17β-雌二醇性能，MISPE柱比非分子印迹固相萃取柱和C18柱具有更高的保留，回收率依次为85.5%，43.7%和30.7%。

Accurate and efficient phase decoding algorithms play an important role in noncontact optical phase-measurement.

精确高效的相位解码在非接触光学测量中有着重要的作用，在总结传统算法的基础上，提出一种新的相移光解码算法。

The sample of nonleaded freeutting brass containing silicon is observed with electron microscope, we find that there is a clearance in the boundary between basal part?P phase and second phase particle?

将合硅的无铅易切削黄铜试样置于电子显微镜下观察，发现第二相质点γ相与基体β相的交界处有一间隙，说明基体与第二相质点间并未紧密结合。

While, for a higher polymer concentration, due to its high viscosity, the infiltration rate of nonsolvent is reduced and the phase separation occurs by the mechanism of nucleation-and-growth of polymer-poor phase.

然而高浓度之高分子溶液，因黏度高，故而减缓非溶剂渗入之速率，导致相分离机制系以高分子贫相成核成长之方式进行。

The effects of nonsolventγ-butyrolactoneon the behavior of phase separation of PC casting solution were studied at different operating temperature according to the LCP correlation.It was found that the phase separation behavior of PC/NMP/γ-GBL also exhibited well agreement with the LCP correlation.Therefore,the maximum content ofγ-GBL in casting solution could be obtained according to the binodal line of the system,which provided scientific basis for the composition of casting solution.

实验进一步考察了不同温度下非溶剂γ-丁内酯对PC铸膜体系相分离的影响，并依据LCP线性回归结果外推计算三元体系的双节线，由此得到了铸膜液体系中非溶剂添加剂的上限含量，为铸膜液体系的构建提供了可靠的依据。

The system at higher temperature becomes thermodynamically more stable, and raises the diffusion exchange rate of solvent and nonsolvent at the interface according to the diffusion kinetics. For the PANCMA/DMSO/ system, with the addition of DMSO to nonsolvent, the cloud point curves shifts to the polymer-nonsolvent axis, and the homogeneous phase region is broadened, system becomes thermodynamically more stable and needs more nonsolvent mixture to induce liquid-liquid phase separation.

通过浊点滴定，结合LCP半经验关系，可以得到制膜体系PANCMA/溶剂/非溶剂的三元相图浊点线，考察其相分离过程中的热力学性质，同时考察了溶剂和非溶剂双向扩散传质动力学，从体系热力学和动力学性质出发为PANCMA中空纤维膜的制备以及解释最终的膜结构和性能提供理论依据。

based on the analysis of the traditional gnss carrier phase measurement model and the rule of the integer ambiguity estimation,the quality of normal integer mapping is gained,then,the theory of rough integer mapping is proposed,the question of gnss integer ambiguity estimation is solved,the searching efficiency of integer ambiguity is improved,the problem of gnss carrier phase measurement in a certain extent is solved.

摘 要：在分析传统的基于gnss载波相位测量模型对整周模糊度解算的一般规律后，得出一般归整映射的性质，进而提出粗糙归整映射理论，用来解决整周模糊度浮点解归整问题，提高了整周模糊度的搜索效率，一定程度上解决了载波相位实时测量的技术难题。

There were two or more nucleole in the nuclei of the apicalmeristem cell when the plant went into reproductive phase from vegetative phase.

植株由营养生长转入生殖生长时，茎端细胞的核内有2个或多个核仁。

"Yes, now you can give yourself airs," she said, you have got what you wanted.

"对了，您现在高兴了，"她说道，这是您所期待的。

Then the LORD said to me: Rebel Israel is inwardly more just than traitorous Judah.

上主于是对我说：＂失节的以色列比失信的犹大，更显得正义。