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Objective To establish a HPLC method for the determination of aceclofenac in human plasma.Methods Acidified samples of plasma (500μL) were extracted with 4 mL of ethyl acetate. The organic phase was evaporated to dryness by nitrogen at 40℃ water bath. The residue was redissolved in mobile phase and then was determined.

醋氯芬酸是一种具有镇痛作用的非甾体类抗炎药物[1],化学名为[邻-(2,6-二氯苯基)氨基]苯乙酰乙酸,l992年首先于西班牙上市,具有明显广泛的抗炎作用和强力的解热镇痛作用,其生物半衰期较双氯芬酸长,胃肠耐受性较双氯芬酸好,抗炎活性优于萘普生和保泰松[2]。

The paper also places emphasis on a novel method called the phase alignment algorithm for subaperture reference signals.The algorithm adjusts phases of respective subaperture reference signals in order to make them in phase and constructs a new spotlighting window function for SAR imaging.

子孔径参考信号相位对齐算法本质是将各个子孔径参考信号的相位调整为同相,并构造新的聚束窗函数进行SAR成像。

A.The inverter part is made of MOSFET single-phase inverter bridges connected in CFI. The power of single-phase bridge is 60kW; the inverter bridge adopts the building block method to realize power superposition. Every piece of bridge plate is designed in the shape of a drawer, which is very easy to install and repair

逆变部分由 MOSFET 单相逆变桥并联组成,单桥功率设计为 60kW ,逆变桥采用积木式方式完成功率叠加,每块桥板均设计为由滑道组成的抽屉式结构,方便安装与维修

Two new methods about preparation of nano-inorganic coated polymer microsphere have been found. The research mainly focused on controlled precipitation of inorganic precurdors onto the polymer microspheres, technique of preparation and size distribution of transition metal oxides and sulfides emulsion particles, nano-paticles''surface modification and the HLB values adjustment, emulsification of oil-soluble monomer in inorganic colloid and emulsion stability, emulsion polymerization that inorganic particles act as medi-phase, the preparation of inorganic nano-particle/polymer hybrid microspheres, preparation of hybrid materials in inverse emulsion, inverse emulsion polymerization of acrylamide and its phase behavior. Inorganic nano-particles we studied concerning TiO2、SiO2、Fe3O4、ZnO、ZnS、Ag and black carbon. Also we studied the morphology and capability of the hybrid materials.

主要内容有:无机物在高分子乳胶模板体系的界面定位沉积研究;过渡金属氧化物、硫化物纳米胶体粒子的制备工艺与胶粒尺寸分布研究;纳米粒子的表面修饰及其亲水亲油平衡值的调制;油溶性单体在无机胶体中的乳化行为与乳液稳定性研究;以无机纳米粒子做中介相的乳液聚合与无机纳米粒子/高分子复合微球制备研究;反相体系中杂化材料的制备;丙烯酰胺水溶液反相乳液聚合、相行为与稳定性;丙烯酰胺反相体系中无机粒子的制备研究;涉及到TiO2、SiO2、Fe3O4、ZnO、ZnS、Ag、碳黑等纳米无机物,系统考察了相关材料的形态与性能,为其应用开发奠定了基础。

The study and comprehensive analysis of static high-pressure quenching experiments and laboratory dynamic high-pressure experiments on chondrites,as well as the study of shock-induced phase transition of minerals in the Suizhou meteorite revealed that the P-T conditions for phase transition of minerals during natural impact events,such as collision of cosmic bodies or impact of meteorites on the Earth′s surface,are not consistent with those obtained by shock experiments on chondrites or rocks in laboratory,...

通过对球粒陨石的静态高压淬火实验和人工动态高压实验的研究和综合分析,以及对在太空中经受过撞击的随州陨石中矿物发生高压相变的研究,查明了自然界的冲击事件,如星体的相互碰撞和陨石对地球表面的撞击中,矿物发生相变的P-T条件与人工冲击波实验的结果并不一致,而与静态高压淬火实验的结果相似,即前者类似静态高压淬火实验,保压时间较长,能产生高压矿物,后者保压时间极短,无高压矿物形成。

The fire fault tree of public building in the construction phase is set up,and carries out qualitative analysisBased part of the construction site for the fires accidents occurred in 2007,the paper introduces the current construction phase of our public buildings and characteristics of the status of the fire.

建立了公共建筑施工阶段火灾事故树,并进行了定性分析以2007年发生在施工现场的部分火灾事故为引,介绍了目前我国公共建筑施工阶段火灾的现状和特点。

Result: The knee joint angle of affected-side and unaffected-side of hemiplegic gait showed significant differences on knee flexions at heel-ground (4.49±6.16,14.02±8.49), Max. extension in stand phase (-0.89±3.86, 3.18±5.47), Max. flexion in swing phase (23.11±10.54, 30.28±10.52) and total excursion on sagittal plane (27.94±8.06, 28.94±10.10) comparing with healthy subject.

结果:偏瘫患者患侧和健侧膝关节初始着地时刻(4.49±6.16, 14.02±8.49)、站立相最大伸展角度(-0.89±3.86, 3.18±5.47)、摆动相最大屈曲角度(23.11±10.54, 30.28±10.52)、矢状面膝关节角度范围(27.94±8.06, 28.94±10.10)均与正常人存在显著差异。

In order to achieve good control effect in the research of special electronic power transformer,we employed Park transformation to implement the transfer from the double closed-loop decoupled control of three-phase to four-phase EPT s primary side.

在特种电子电力变压器的研究中,为了达到良好的控制效果,采用Park变换来实现三相变换到四相电子电力变压器高压侧的双闭环解耦控制。

The advantages of catalytic synthesis of oxalate ester in gaseous phase by carbon monoxide are summarized. The five important characterization of our patent technology invented for the use of industrial raw material and the potential good economic value of the process are presented. It indicates that study and development of catalytic synthesis of oxalate ester .oxalic acid as well as glycols by natural gas in gaseous phase have a great advantage for full utilization of natural gas....

概述了&CO气相催化合成草酸酯&技术的先进性,介绍用工业性原料为主要内容的专利技术:&气相催化合成草酸酯连续工艺&的五个主要特点及其潜在的经济效益,并指出,用天然气经合成气进行气相催化合成草酸酯和草酸、乙二醇的研究与开发,可使天然气得到充分的利用,具有很好的经济效益,是天然气化工综合利用的一条有效途经,也是当代C1化学的重要发展方向。

1 The expression of Bax began in the late proliferative phase, the highest level in the involuting phase.

TGFβ1在增生期血管瘤组织中表达较弱,阳性表达率43.75%,退化期血管瘤组织中表达强,阳性表达率83.33%,两组比较有显著性差异,p<0.01。

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书,王祥生,李德昌。安徽省首次发现嗜群血蜱。

Chapter Three: Type classification of DE structure in Sino-Tibetan languages.

第三章汉藏语&的&字结构的类型划分。