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In this thesis, the tripeptide GHK has been synthesized by liquid-phase method and octpeptide Eptifibatide by solid-phase method. Coupling agents and purification problem have been studied in the process of peptide synthesis.

本论文分别采用液相法和固相法合成了具有药用价值的三肽GHK及八肽Eptifibatide,研究了多肽合成过程中缩合剂及纯化等问题。

The method comprises the following steps of: preparing and scraping polymer casting solution on the surface of clutch gold; conducting humidification treatment on the polymer casting solution by a humidifier or conducting phase inversion in non-solvent until phase inversion occurs in the polymer casting solution and micro porous membrane is formed; making use of the electrodeposition technology to allow tin or tutania to deposit on the surface of the clutch gold; conducting thermal treatment on the clutch gold with the protection of idle gas to obtain a Li-ion battery composite cathode electrode tab.

该方法包括如下步骤:配制聚合物铸膜液,并将聚合物铸膜液刮涂在铜箔表面;利用加湿器对铜箔上的聚合物铸膜液进行加湿处理,或在非溶剂中进行聚合物的相转化,直到聚合物铸膜液发生相转移形成微孔膜;通过电沉积工艺,使锡或锡合金通过微孔膜膜孔沉积在铜箔表面;铜箔在惰性气体的保护下进行热处理,得到锂离子电池复合物负极电极片。

The subject of the article is three-phase unsignalized intersection control in highway system. The correlation analysis and AIC principle analysis are applied to building the crash prediction model of three-phase unsignalized intersection in the plain based on the probability model.

以三路无信号交叉口为研究对象,采用相关分析与AIC原则分析方法,建立基于概率模型的平原区无信号三路交叉口事故预测模型。

Phase unwrapping is one of the most key steps in magnetic resonance imaging applications in which accurate phase is required.

相位展开是磁共振成像技术应用中最关键的环节之一,可以为磁共振的某些重要临床应用提供精确的相位信息。

Besides, owing to considerable difference in voluminal heat capacity between gaseous phase and solid phase, the reactor has high stability even the feed composition and gas velocity fluctuate frequently in a certain range.

而且由于气固两相的体积热容量相差很大,使这一过程的抗干扰能力较强,反应器具有比定态操作更大的操作弹性,即使原料气浓度和流量在一定范围内频繁波动,系统也能维持正常操作。

The result showed that Wote and PAM increased the average temperature of the earth's surface, temperatures of 10cm soil, 20cm soil and the lowest temperature of the earth's surface, but reduced the highest temperature of the earth's surface in reviving phase. Soil moisture was increased by using Wote and PAM, and the soil moisture of 0-30cm soil in florescence and fruiting phase was also increased.

结果表明,施用沃特和FAM降低了西瓜缓苗期的地表最高温度,提高了地表的平均温度、最低温度及10cm土层和20cm土层的土壤温度,增加了土壤的含水量,特别是开花坐瓜期0~30cm土层的土壤含水量。

This is the first report of pectenolone and pectenoxanthin, two types of carotenoid, in the muscle of the Yesso scallop.3 Roles of the carotenoids composition and accumulation in Yesso scallopThe method for detecting carotenoids using reverse phase high performance liquid chromatography was developed. The conditions of RP-HPLC analysis were an analytical scale (200×4.6 mm, inner diameter 5μm) Eclipse XDB-C18 column of Agilent corporation; 10μl injection volume; 25°C column temperature; acetonitrile, methanol and methylene dichloride mobile phase (40:56:4, V/VV) with 0.1% BHT; 1.0 ml per minute flow rate; 450 nm UV-VIS detector; 8 minutes elution.The carotenoids from orange muscle of Yesso scallop of 7, 10, 12, 15, 18, 22 months old was detected using the method refered above.

通过柱层析、高效液相等手段对橘红色闭壳肌中的主要类胡萝卜素进行了提取分离,分离提纯得到两种类胡萝卜素,并通过MS、~1H-NMR和~(13)C-NMR对其进行结构鉴定,结果表明(3S,3\'R)-3,3\'-dihydroxy-7\',8\'-didehydro-β,β-Caroten-4-one和(3S,3\'S)-7,7\',8,8\'-tetradehydro-β,β-Carotene-3,3\'-diol,俗称pectenolone和pectenoxanthin是橘红色闭壳肌中的主要类胡萝卜素,这是国内外首次对虾夷扇贝闭壳肌中的类胡萝卜素进行提纯及结构鉴定。3虾夷扇贝类胡萝卜素的种类组成和累积变化规律建立了橘红色闭壳肌中类胡萝卜素的HPLC分析定量检测技术:色普柱为Agilent公司的Eclipse XDB-C18柱200mm×4.6mm,i.d.5μm进样体积,5μl ;流速1ml/min;检测波长450nm;柱温25℃;流动相为乙腈:甲醇:二氯甲烷(V/V/V=40:56:4并加入0.1%的BHT;分离时间为8min。

At first, Oil phase conductivity change tendency is texted in this article, after mixed solution of Benzene,Tetrabutylammonium Bromid,cosurfatant which is added in KBr aqueous solution with different concentration, migration process of TBAB to the aqueous phase is studied.

本文首先通过电导率法测定了苯、四丁基溴化铵、助表面活性剂混合溶液中加入不同浓度的KBr水溶液震荡后油相电导率变化趋势,研究TBAB向水相迁移的过程。

However, fully consideration of special structure and physiological function of CRP is critical to investigate whether CRP provide protect effect or pathogenic effect in the progression of atherosclerosis. CRP is a member of pentrxins family, which consists of five identical, noncovalently associated 23-kDa protomers arranged symmetrically around a central pore with a 102 A external diameter. Each protomer has a recognition face with a phosphocholine binding site consisting of two coordinated calcium ions adjacent to a hydrophobic pocket. The opposite face of the pentamer is the effector face, where complement Clq binds and Fc receptors are presumed to bind. A cleft extends from the center of the protomer to the central pore of the pentamer. Both faces ofpentamer form a special bi-phase structure: one face is the ligand recognition phase, which can recognize apoptosis cells and enzyme modified low density lipoprotein in which PCh is exposed.

CRP是一种五聚体蛋白,外径为102 A,由5个相同的单体以非共价键结合,形成双面的环形结构,每个单体的配体识别位点或受体结合位点分别位于五聚体两个平面上,分别组成配体识别相和效应器相,从而构成特殊的二相性结构:一面为配体识别相,含有磷酸胆碱(phosphorycholine,PCh)结合位点,能够使CRP识别在病理条件下暴露出PCh的凋亡细胞、酶修饰低密度脂蛋白(enzyme modified low density lipoprotein,E-LDL)等。E-LDL是天然低密度脂蛋白(native Low density lipoprotein,N-LDL)在多种蛋白酶,如胰蛋白酶、神经氨酸酶、胆固醇酯酶等作用下的代谢产物,其主要特点是结构发生改变(N-LDL大小均匀,平均直径250±30 A,E-LDL大小差异极大,直径为100-2000 A),暴露磷酸胆碱位点,能够被CRP识别;另一面为效应器相,能够与巨噬细胞、单核细胞表面受体FcγRⅡa结合,介导巨噬细胞、单核细胞识别及吞噬凋亡、坏死细胞作用。

BY modifying phase mask UV exposure system and inserting a circumvolved device which making optical fiber rotation in back of the phase mask, the PMD in fiber Bragg gratings is compensated.

改变光纤光栅紫外曝光系统,在相位掩模板后插入一个旋转装置,使得光纤在制作过程中可以进行某种旋转。

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书,王祥生,李德昌。安徽省首次发现嗜群血蜱。

Chapter Three: Type classification of DE structure in Sino-Tibetan languages.

第三章汉藏语&的&字结构的类型划分。