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A preparation method of the visible-light photocatalyst Bi2WO6 nano-powder is characterized by comprising the steps as follows:(1) the selection of raw materials;(2) bismuth nitrate Bi(NO33 question mark 5H2O is added into a citric acid solution to obtain the citric acid solution containing white sediment;(3) EDTA is added into ammonia water which is then added dropwise with the citric acid solution containing the Bi(NO3)3 question mark 5H2O so to obtain a solution of bismuth;(4) the solution of bismuth is added with (NH4)6W7O24 question mark 6H2O solution to form a precursor solution which is then stirred, dried, coked, cooled and ground to obtain decarburized powder;(5) the decarburized powder is roasted for 2h to 4h under 450 DEG C to 550 DEG C to obtain the visible-light photocatalyst Bi2WO6 nano-powder.
可见光催化剂Bi 2 WO 6 纳米粉体的制备方法,其特征在于它包括如下步骤:1原料的选取;2将Bi(NO 3 ) 3 5H 2 O加到柠檬酸溶液中,得到含有白色沉淀的柠檬酸溶液;3将乙二胺四乙酸加到氨水中,并缓慢滴加入含有Bi(NO 3 ) 3 5H 2 O的柠檬酸溶液中,得铋的溶液;4将(NH 4 ) 6 W 7 O 24 6H 2 O溶液加入上述铋的溶液中,组成前驱液;搅拌,干燥,焦化,冷却后,研磨,得去碳的粉体;5将去碳的粉体在450~550℃下焙烧2~4h后,得到可见光催化剂Bi 2 WO 6 纳米粉体。
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The general form of solution for the non symmetric matrix A is given, the expression of optimal approximation solution is presented, and an algorithm for solving the problem is described. The total least squares problem with symmetric and bisymmetry constraints is discussed respectively. A sufficient condition for existence of solution is derived by use of the theory of matrix Ricaati equation. The general form of solution is given if the problem has a solution, and the expression of optimal approximation solution is presented. Some numerical examples are given.
对矩阵A是非对称情形,给出了解的一般表达式,证明了最佳逼近问题解的存在唯一性,并给出了其解的表达式,描述了求解问题的算法;讨论了带对称和双对称约束的总体最小二乘问题,利用Ricaati矩阵方程的理论得到了解存在的一个充分条件,分别对对称矩阵和双对称矩阵两种情形,给出了解的一般表达式,证明了最佳逼近问题解的存在唯一性,给出了其解的表达式,提出了求解这些问题的算法,并给出了数值例子。
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Material and MethodsRA Rabbit Model group: 15 early RA rabbits of the same weight and variety Control group:10 normal rabbits of the same weight and varietyMethods of making RA rabbit model:elect 15 normal rabbits of the same weight and variety, dissolve Ovalbumin in 0.9% sodium chloride solution, to make the solution of 20mg/ml concengtration, blend the same quantity of complete Freund′s Adjuvant equably ,inject the mixed solution into endermic tissue of the rabbit′s scapular section, making the rabbits allergic, inject 1 ml of the mixed solution to one rabbit every time, inject 1 ml of the mixed solution in 5 different places of the rabbit′s scapular section, inject the rabbit one time every week,inject 3 weeks continuously,it turned out to be that the rabbits will be allergic, inject Ovalbumin blent with the 0.9% sodium chloride solution into the knee joint cavity of the rabbits in the fourth week, 5 mg Ovalbumin every knee joint cavity,two knees of every rabbit of the 15 rabbits are both injected,the arthrosis diameter and the exterior temperature of the knees will be added obviously in 24 hours,and they will drop gradually,at the time of the 14th or 21th day, the arthrosis diameter and the exterior temperature of the knees will get to the balance time,the incidence rate of RA is 100%.after the RA model succeeds,it is the early time of RA from the first week to the fourth week,after the fourth week,it is the late time of RA, the cartilage of the femoral condyle and the subchondral bone cortices will be changed unrecoverily.
资料与方法RA模型组:早期RA家兔模型15只,品种及体重接近。对照组:正常家兔10只,品种及体重接近。RA家兔模型制作方法:选取15只成年家兔,体重、品种接近,将卵蛋白溶解于生理盐水,配成浓度为20mg/ml的溶液,与等量完全弗氏佐剂混匀,注入家兔肩胛区皮下致敏,每只家兔每次注射1ml,于肩胛区5个不同区域注射,每周一次,连续注射3周而致敏,第4周向膝关节腔注射卵蛋白生理盐水溶液,每只关节腔注射5mg卵蛋白,15只家兔膝关节全部注射,24h内此关节直径和表面温度大幅度上升,以后缓慢下降,至14~21d达到平台期,发病率达100%。造模成功后第1~4周为早期改变,第4周以后出现不可逆的关节软骨及骨破坏。采用高频超声对RA模型组与对照组的膝关节髌上囊液体厚度、滑膜及股骨髁软骨厚度及软骨下骨皮质的回声情况进行对比观察。结果RA组模型组膝关节髌上囊积液及滑膜的厚度明显厚于对照组,其股骨髁软骨的厚度与对照组相比无明显差异,其软骨下骨皮质与对照组相比无明显改变。
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In chapter two, under non-Lipschitz condition, the existence and uniqueness of the solution of the second kind of BSDE is researched, based on it, the stability of the solution is proved; In chapter three, under non-Lipschitz condition, the comparison theorem of the solution of the second kind of BSDE is proved and using the monotone iterative technique , the existence of minimal and maximal solution is constructively proved; in chapter four, on the base of above results, we get some results of the second kind of BSDE which partly decouple with SDE, which include that the solution of the BSDE is continuous in the initial value of SDE and the application to optimal control and dynamic programming. At the end of this section, the character of the corresponding utility function has been discussed, e.g monotonicity, concavity and risk aversion; in chapter 5, for the first land of BSDE ,using the monotone iterative technique , the existence of minimal and maximal solution is proved and other characters and applications to utility function are studied.
首先,第二章在非Lipschitz条件下,研究了第二类方程的解的存在唯一性问题,在此基础上,又证明了解的稳定性;第三章在非Lipschitz条件下,证明了第二类BSDE解的比较定理,并在此基础上,利用单调迭代的方法,构造性证明了最大、最小解的存在性;第四章在以上的一些理论基础之上,得到了相应的与第二类倒向随机微分方程耦合的正倒向随机微分方程系统的一些结果,主要包括倒向随机微分方程的解关于正向随机微分方程的初值是具有连续性的,得到了最优控制和动态规划的一些结果,在这一章的最后还讨论了相应的效用函数的性质,如,效用函数的单调性、凹性以及风险规避性等;第五章,针对第一类倒向随机微分方程,运用单调迭代方法,证明了最大和最小解的存在性,并研究了解的其它性质及在效用函数上的应用。
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The polymeric sol is obtained by process of preparing a calcium salt solution, containing calcium ethoxide dissolved in organic acid, and a phosphate solution, containing triethyl phosphite or triethyl phosphate dissolved in the organic acid, mixing the calcium salt solution with the phosphate solution to produce a mixed solution, and aging the mixed solution.
本发明的磷酸钙化合物的聚合物溶胶是通过如下步骤制备的:制备含有溶解在有机酸中的乙醇钙的钙盐溶液和含有溶解在该有机酸中的亚磷酸三乙酯或磷酸三乙酯的磷酸盐溶液;及将该钙盐溶液和该磷酸盐溶液混和制得混合溶液,并老化该混合溶液。
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An alkaline solution containing mercaptides is regenerated in an improved process wherein the alkaline solution to be regenerated containing a suitable oxidation catalyst is contacted with an oxygen-containing solvent which is immiscible with said alkaline solution in a reaction zone comprising a plurality of fibers positioned longitudinally within a conduit, whereby the two liquids are in contact while concurrently flowing through said reaction zone during which the mercaptides contained in the alkaline solution are oxidized to disulfides and are simultaneously extracted from the alkaline solution into the solvent solution.
包含 mercaptides 的碱解决在一个改良的程序被再产生在何处碱的解决被再产生包含一个适当的氧化催化剂与被说反应的碱的解决组成一个纤维的多数地域纵观地放置在一个导管里面的对一个包含氧的溶剂感到不能相混合的一起连络,那里当协同地流动过说的反应地域的时候,这二种液体保持接触在哪一个期间包含在碱的解决 mercaptides 被使氧化到 disulfides 而且同时地从碱的解决到有偿付能力的解决被吸取。
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The oil shale ash is disintegrated into fine powder less than 150 eye to be calcined at a certain temperature, then sulfuric acid solution is added for performing acid dipping, after solid-liquid separation and solid residue removal, aluminum sulfate solution is obtained and is then filtered after sodium hydroxide solution is added in, further metallic ions as Ca2 , Mg2 , Fe3 , Fe2 and the like are filtered from the solution, thereby sodium aluminate solution is obtained, gas of carbon dioxide is communicated into the sodium aluminate solution to obtain aluminum hydroxide sediment, and after drying and calcining aluminum hydroxide powder is obtained.
将油页岩灰渣粉碎至<150目的细粉,在一定温度下煅烧,加入硫酸溶液进行酸浸,固液分离,去除固体残渣,得硫酸铝滤液,加氢氧化钠溶液后过滤,滤除溶液中的Ca 2 、Mg 2 、Fe 3 、Fe 2 等金属离子,得偏铝酸钠溶液,向偏铝酸钠溶液通入二氧化碳气体,得到氢氧化铝沉淀,经烘干、煅烧得到氢氧化铝粉末。
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One kind is using the particular solution of the indefinite equation, which can be obtained by the property of the prime number , and the foundation system of solution of its corresponding homogeneous equation ,obtains its solution formula. Another kind is under the foundation of the matrix primary line transformation, and with the aid of some knowledge of numeral theory, obtains its solution formula.
一种是利用该不定方程的一个特解和其相对应的齐次方程的一个基础解系,得出该不定方程的求解公式,而这个特解可以由素数性质得到;另一种是在矩阵的初等行变换基础上,借助一些数论知识,得出该不定方程的求解公式。
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Secondly, by linearizing the system at the unique positive equilibrium solution and analyzing the associated characteristic equation, it is found that the positive equilibrium solution is asymptotically stable when the delay equals to zero and when it is increased to certain critical value, the positive equilibrium solution will loss the stability and a spatially heterohomogeneous periodic solution will bifurcate from this positive equilibrium solution.
通过在系统唯一的正平衡解处线性化系统和分析相应的特征方程,发现在时滞等于零时该正平衡解是渐近稳定的,当时滞逐渐增大到某个临界值时该正平衡解将失去稳定性而且在该平衡解处分支出空间非齐次的周期解。
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Huang and Lin proposed the weak solution concept for Backward Stochastic Differential Equation This paper based on the predecessor's work , gives the weak solution concept for Backward Stochastic Differential Equation with continuous martingale,uses the Girsanov transformation, obtains its weak solution of the existence of a necessary and sufficient conditions, and on this basis obtains its weak solution of the existence of sufficient conditions,these sufficient conditions weakened the drifting coefficient which requested in the existence uniqueness of strong solution to satisfy the Lipschitz condition the request.
本文在前人研究的基础上,给出由连续鞅驱动的倒向随机微分方程弱解的概念,利用Girsanov变换,得到其弱解存在的存在的一个充分必要条件,并在此基础上得到了其弱解存在的一些充分条件,这些充分条件减弱了在强解的存在唯一性中要求的漂移系数满足Lipschitz条件的要求。
- 相关中文对照歌词
- Love Solution
- Second Solution
- That Particular Time
- Nothing In Particular
- The Song We Were Singing
- Ain't No Particular Way
- The Solution
- Bite Your Rhymes
- Revolution
- 推荐网络例句
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The shaping method of noncircular part and the tool holder's radial motion characters in noncircular turning process are discussed in detail in the thesis.
论文详细研究了非圆零件的成型方法和加工过程中刀架的径向运动规律。
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I have not really liked him,I do not like his this kind of disposition.
我没有真的喜欢他,我不喜欢他的这种性格。
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As we know the price of traditional product is composed of the cost and the profit of the company involving market competition, monopolizes and many other factors.
我们知道作为传统的商品,定价的模式往往是在成本的基础上增加厂商的预计利润而形成其价格,当然也要考虑到市场竞争、垄断等其他方面的因素。