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Investigating the influences of processing parameters on the C/Si molar ratio of resulted nanosized SiC powders indicated that there was a direct pyrolytic reaction from DMS to SiC as well as the previous proposed two-step reaction. Under the optimized processing conditions, the silicon carbide powders of homogeneous particle size distribution, spherical shape and stoichiometrical C/Si molar ratio are obtained. The silicon carbide particle consists of β-SiC crystallite arranged randomly.

论文系统研究了工艺条件对产物粉体C/Si摩尔比、粉体颗粒尺寸和组成粉体的SiC微晶尺寸的影响;研究了粉体制备过程中可能发生的化学反应,提出了反应过程中除了分步进行的生成SiC的反应外,同时在高温区还存在一步完成的生成SiC的化学反应的观点;通过调整工艺参数,制备得到了粉体尺寸分布均匀、呈均匀球状、C/Si摩尔比符合化学计量比的颗粒尺寸为40nm的纳米SiC粉体。

Pristine Li-Al LDHs are synthesized by hydrothermal process in different reaction conditions by varying the aging time for 1 and 24 hours. Both the Li-Al layered double hydroxides (abbreviated as Li-Al LDH1 and Li-Al LDH24 for aging time 1 hour and 24 hours, respectively) were modified by using sulphanilic acid sodium salt hydrate, modified agent to form modified Li-Al LDH1-SAS and Li-Al LDH24-SAS. The morphology of the pristine layered double hydroxides are investigated by using wide angle X-rays diffraction, scanning electron microscopy and particle size analyzer which indicates that the crystallinity and aspect ratio is increased with increasing the aging time from 1 hour to 24 hours. The particle size of Li-Al LDH24 and Li-Al LDH1 are found to be ~1000 nm and ~250 nm, respectively. Both the pristine and modified LDHs are characterized by XRD, FTIR spectra and thermogravimetric analysis.

本研究目的在於改变长晶时间的长短,合成出同径大小的Li-Al LDHs,再经由改质剂sulphanilic acid sodium salt hydrate将Li-Al LDHs无机层材表面有机官能化制备出改质型Li-Al LDHs-SAS,於是进一步藉由扫描式电子显微镜、射径仪和穿透式电子显微镜等仪器分别观察LDHs改质前和改质后其主层结构型态上的变化;从中可以发现Li-Al LDHs随著长晶时间的增加其径有随之增大的趋势,但经有机化改质后其径会由於改质环境的影响明显低许多,针对此现象本实验将未改质和改质后之Li-Al人工无机层材制备成复材进一步探讨其在热性质和难燃特性上的为表现。

Sodium allyl hydroxyalkyl sulphonate was used as reactive surfactant to modify the polymerization ofelastic acrylic emulsion. Influence of SAHS on minimum content of surfactants and particle size of emulsion was studied andmechanism of change of particle size discussed.

使用烯丙基羟烷基磺酸钠作为可聚合乳化剂,改性合成了弹性丙烯酸酯乳液,研究了它对乳化剂的最低用量和乳胶粒粒径的影响,探讨了乳胶粒粒径变化的机理。

Grasp sulphonation mechanism of aromatics, including the process of producing electrophilic particle, the process of electrophilic particle attacking aromatics, reaction dynamics and influence factor.

掌握芳香族磺化反应历程,包括产生亲电质点的过程和亲电质点进攻芳环进行磺化反应的过程、反应动力学及影响因素。

The experiment result : In some constant flow ,the unequality degree of particle decreases while concentration of particle increases.

实验结果表明:当液体流量一定时,颗粒的不均匀度随浓度增加而减小。

In order to elucidate the effect of the texture, structure and particle size of aggregate on determining its ASR reactivity, the texture, structure and ASR features of zeolitic pearlite and siliceous gravel were examined by optical microscope, XRD and SEM/EDS. It has been found that in addition to the type and amount of reactive constituents in aggregate, the physical structure has also strong influences on the process and expansion behavior of ASR, and the influences of physical structure may be various with particle size of aggregate.

为进一步研究集料结构构造和集料尺寸对鉴定集料ASR活性的影响,用光学显微镜、XRD和SEM/EDS等方法研究了集料的岩石学、矿物学特征及其ASR反应特征,发现除集料中活性组分的类型和数量外,集料的物理构造特征对ASR过程和膨胀行为有显著影响,而且集料的尺寸不同,物理构造的影响程度有差异。

The invention discloses an electrochemical method for preparing a hydroxylapatite particle thin coating on the surface of a metal implant, which comprises the following steps: electrolyte is put into a container equipped with a constant temperature heating system and heated to be 30 DEG C to 95 DEG C, and then the temperature is kept; platinum is taken as the anode and evenly distributed around the container, and the metal implant is taken as the cathode, put in the middle of the container and totally soaked in the electrolyte; DC voltage of 2V to 4V is added between the anode and the cathode, the surface of the metal implant has cathode reduction reaction, the pH value is increased and the supersaturation degree of the hydroxylapatite is also increased, so as to crystalize on the surface of titanium; after 0.5h to 5h of deposition, a layer of hydroxylapatite particle thin coating which can be excellently adhered to the matrix metal is formed on the surface of the implant.

本发明公开了一种在金属植入体表面制备羟基磷灰石颗粒薄涂层的电化学方法,在装备了恒温加热系统的容器中装入电解液,并将电解液加热到30~95℃恒温;将铂作为阳极均匀分布在容器四周,金属植入体作为阴极置于容器中间,完全浸没在电解液中,两极之间加直流电压2~4V,金属植入体表面发生阴极还原反应,pH值升高,羟基磷灰石过饱和度增加,从而结晶在钛金属表面;经过0.5~5小时沉积后,在植入体表面即可形成一层与基体金属结合优良的、薄的羟基磷灰石颗粒薄涂层。

During powder injection in the bottom-blown ladle, forces acting on particle were analyzed in consideration of the interaction between gas and particle.

在底喷粉条件下,通过考虑颗粒与气体之间相互作用,对气固两相流中的颗粒进行受力分析。

Only average percentage of Al in episode days is high than that in nonepisode days.The A/C ratio of the cation or anion in PM10 is greater than 1 for every sampling situation. It was highly correlate between NH4+ and NO3-, NH4+ and SO4-2 of PM10 particle among four sites. The NR of each site was all 1. It means that the PM10 particle is acidulated during the sampling period and that phenomenon worth to be researched further in the future.

无论污染事件日、非污染事件日或日、夜间,各测站PM10上阴、阳离子当量比之比值均大於1;各测站PM10微粒中NH4+与NO3-间及NH4+与SO4-2间均呈高度之相关性,其PM10微粒之中和比值(neutralization ratio;简称NR)均小於1,表示各测站在本研究之采样期间,其PM10微粒均偏酸性,其原因未来值得深入加以探讨。

The coupling admixes the particle and collective degrees of freedom in such a manner as to partially transfer the one-particle transition strength onto the collective modes.

耦合使粒子和集体自由度按这样的方式混合,即使单粒子跃迁强度部分地转变到集体模式中。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。