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When comparing USFA concentration, it tended to be higher in female. Breast meat contained significantly higher saturated fatty acid (P.001) and leaf fat contained significantly higher USFA (P.001). C18:2 content from birds kept in wet pad type housing increased significantly between 10-11-wk old; at 10-12-wk old, the increment in male was significant while gradient increment was noted in female between 11-12-wk old. The content of USFA in breast meat tended to increase gradually with age and vice versa for SFA after 12-wk old. The trend for SFA and USFA content in thigh meat were gradual after 7-wk old while no considerable change was noted for the SFA and USFA content in the leaf fat.

胸肉含有显著较高之总饱和脂肪酸(P.001),腹脂含有显著较高之USFA(P.001)。C18:2含量在水帘式畜舍在10到11周龄之间有一明显的增加,开放式畜舍则在11到12周龄之间有一明显的增加;公鸡部分在10到12周龄之间有一明显的增加,母鸡部分则在11到12周龄之间有逐渐增加之趋势;不同部位的部分则可以发现,胸肉中USFA含量,会随著周龄的增加而有逐渐增加的趋势,SFA则反之,且皆在12周龄以后趋於平缓,腿肉中之SFA及USFA含量,皆在7周龄以后趋於平缓,腹脂中之SFA及USFA含量,在全期则变化不大。

The SOD and the LDH-1 activities and EST (R_f=0.17 and R_f=0.72) at 1℃weresignificantly higher than the values of the room temperature(P<0.05), but the total enzymeactivities of LDH, G6PDH and EST at room temperature and 1℃were similar(P>0.05).This showed well-developed anoxia tolerance of the Heilongjiang wood frog to maintainplasma viability when low temperature interrupts the delivery of oxygen and substrates. LDH-1rose significantly avoided the liver lactic acid accumulation that may created the liver to bewearied. EST (R_f=0.17 and R_f=0.72) rose may enhance the ester metabolism to offer muchenergy. These showed steady metabolic rate and relative stable organism environment of theHeilongjiang wood frog to survive under low temperature.Native PAGE separated proteins of liver tissue successfully on the better condition is 6%final gel concentration and there were 15~19 bands identified on this condition.

同功酶电泳图谱显示,1℃组与室温组黑龙江林蛙肝脏LDH酶活性差异不显著,均以LDH-5为主,但1℃组LDH-1显著高于室温组(P<0.05),推测黑龙江林蛙为适应低温低氧环境,增强LDH-1酶活性以较好的利用乳酸,避免因大量乳酸形成造成肝脏疲劳;而1℃组肝脏G6PDH酶活性无显著变化,进一步说明低温条件下葡萄糖戊糖途径和糖酵解作用的互相协调,维持机体代谢的稳定;1℃组和室温组EST总酶比活力无显著变化,但1℃组中R_f=0.17和R_f=0.72的EST同工酶显著升高(P<0.05),推测在低温条件下黑龙江林蛙可能通过选择性增强部分酯酶同功酶活性,增加肝脏酯类物质代谢,为机体提供维持生命必需的最低能量。

RESULTS: Sixteen compounds, ursolic acid (1), indole-3-carboxaldehyde (2), indole-3-carboxylic acid (3), p-coumaric acid (4), azelaic acid (5), N-trans-feruloyl tyramine (6), blumenol A (7), 2-hydroxy-3-methylanthraquinone (8), rubiadin l-methyl ether (9), rubiadin (10), quercetin (11), luteolin (12), chrysoeriol 6-C-β-boivinopyranosyl-7-O-β-glucopyranoside (13), alternanthin (14), stigmasta-5, 22-dien-3β-ol (15), and α-spinasterol (16) were obtained from the EtOAc extract of Alternanthera philoxeroides.

结果:得到并鉴定了16个化合物,分别为乌苏酸(1)、吲哚-3-甲醛(2)、吲哚-3-甲酸(3)、对-香豆酸(4)、壬二酸(5)、N-反式阿魏酰基酪胺(6)、布卢姆醇A(7)、2-羟基-3-甲基蒽醌(8)、甲基异茜草素-1-甲醚(9)、甲基异茜草素(10)、槲皮素(11)、木犀草素(12)、柯伊利素-6-C-β-波伊文糖基-7-O-β-吡喃葡萄糖苷(13)、莲子草素(14)、豆甾醇(15)和α-菠甾醇(16)。

Ni-P-mCMC/mCS bipolar membrane was prepared from carboxymethyl cellulose modified with phosphorylated agent as a cation exchange layer and chitosan modified with glutaraldehyde as an anion exchange layer. The electrolysis cell was constituted by Ni-P-mCMC/mCS BPM as a septum for electrogenerating furfural alcohol and furoic acid.

以磷酸化试剂改性羧甲基纤维素钠制备了阳膜层,以戊二醛改性壳聚糖制备了阴膜层溶胶,将阴膜层溶胶流延于阳膜层上,制备了P-mCMC/mCS双极膜,而后以化学镀方法在阳膜层表面镀镍,制备了Ni-P-mCMC/mCS双极膜,并应用于成对电合成糠醇、糠酸。

These compounds were identified as follows:chrysophanol (FP-1),physcion(FP-2),eriosematin(FP-3),scoparone(FP-4),lupeol(FP-5),betulinic acid(FP-6),3\',4\'-Dihydroxy-trans-cinamic acid octacosyl ester(FP-7),β-sitosterol (FP-8),flemiphilippinone A(FP-9),monopalmitin(FP-10),emodin(FP-11),islandicin (FP-12),salicylic acid(FP-13),p-methoxyphenylpropionic acid(FP-14),trideca-1, 3-diene(FP-15),lupinifolin(FP-16),flemichin D(FP-17),flemiphilippinin A(FP-18), auriculasin(FP-19),erythrinin B(FP-20),6-C-prenylluteolin(FP-21), 8-(1,1-dimethylallyl) genistein(FP-22),flemiphilippinin E(FP-23),flemiphilippinin F (FP-24),5,7,3\',4\'-tetrahydroxy-6,8-diprenylisoflavone(FP-25),flemiphilippinin D (FP-26),dorsmaninsⅠ(FP-27),osajin(FP-28),6,8-diprenyleriodictyol(FP-29), lupinalbin A(FP-30),genistein(FP-31),3\'-O-methylorobol(FP-32),orobol(FP-33), 5,7,2\',3\',4\'-pentahrdroxyflavone(FP-34),the mixture of biochanin A and prunetin (FP-35 and 36),genistin(FP-37),sophororicoside(FP-38),3\'-O-methylorobol-7-glucoside(FP-39),the mixture of sissotrin and prunetin 4\'-O-β-D-glucoside(FP-40 and 41),adenosine(FP-42) and luteoloside(FP-43,mixture).

这些化合物分别为大黄酚(FP-1)、大黄素甲醚(FP-2)、eriosematin(FP-3)、滨蒿内酯(FP-4)、羽扇豆醇(FP-5)、白桦酸(FP-6)、咖啡酸二十八烷酯(FP-7)、β-谷甾醇(FP-8)、蔓性千斤拔酮A(FP-9)、单棕榈酸甘油酯(FP-10)、大黄素(FP-11)、islandicin(FP-12)、水杨酸(FP-13)、对甲氧基苯丙酸(FP-14)、十三烷-1,4-二烯烃(FP-15)、lupinifolin(FP-16)、千斤拔素D(FP-17)、蔓性千斤拔素A(FP-18)、auriculasin(FP-19)、erythrinin B(FP-20)、6-C-异戊烯基木犀草素(FP-21)、8-(1,1-二甲烯丙基)-染料木黄酮(FP-22)、蔓性千斤拔素E(FP-23)、蔓性千斤拔素F(FP-24)、5,7,3′,4′-四羟基-6,8-双异戊烯基异黄酮(FP-25)、蔓性千斤拔素D(FP-26)、dorsmaninsⅠ(FP-27)、osajin(FP-28)、6,8-双异戊烯基圣草素(FP-29)、lupinalbin A(FP-30)、染料木黄酮(FP-31)、3\'-O-甲基香豌豆苷元(FP-32)、奥洛醇(FP-33)、5,7,2′,3′,4′-五羟基黄酮(FP-34)、鹰嘴豆素甲和樱黄素的混合物(FP-35和FP-36)、染料木苷(FP-37)、槐属苷(FP-38)、7-葡萄糖基-3\'-O-甲基香豌豆苷(FP-39)、印度黄檀苷和樱黄素4′-O-β-D-葡萄糖苷的混合物(FP-40和FP-41)、腺嘌呤核苷(FP-42)和木犀草苷(FP-43,混合物)。

The content of ferulaic acid is least, its range is 0.496~12.566μg·g~(-1), the content in old-growth Chinese fir soil is more than 5μg·g~(-1), and others are less than 5μg·g~(-1). The content of three phenylic acids in 0~20cm depth soil is larger than 20~40cm. Along the ecosystem conversion direction, in 0~20cm and 20~40cm depth soil, the laws of P-hydroxybenzoic acid, ferulic acid and vanillic acid content are complex, does not exist apparent refularity.

其中对羟基苯甲酸含量最大,大小范围为2.233~19.589μg·g~(-1),其中只有二代杉木人工林的20~40cm层土壤的酚含量小于5,其他的都大于5;香草酸次之,大小范围为0.912~5.683μg·g~(-1),其中只有天然更新常绿阔叶林的酚含量大于5,其他的都小于5;阿魏酸含量最小,大小范围为0.496~12.566μg·g~(-1),其中老龄杉木林的0~20cm和20~40cm层土壤的酚含量大于5,其他的都小于5。

NM taurocholic acid at pH 5.5. The LES activity became sustained increase in basal tone withcaotic response after continuous perfusion of 20 nM taurocholic acid longer than1 hour, andfinally loss of response.

动脉注射substance P 抑制剂,可小幅减低下食道括约肌收缩。4nM 和20 nM 的taurocholic acid at pH 5.5 胆酸灌注会使氧化自由基产生些微增加。20 nM taurocholic acid at pH 5.5 约一小时后,基础食道压力上升且型态混乱不规则,对刺激反应呈疲乏。

Results:(1)Plasma FC concentration in undialyzed patients with CRF was significantly higher than that in normal subjects(P.05),and it was closely correlated with blood urea nitrogen(r=0.666 0) and uric acid(r=0.642 0,P.05),not correlated with serum creatinine.

结果:(1)慢性肾衰保守治疗患者血浆FC浓度明显高于正常人(P.05),并与血清尿素氮、尿酸显著相关(r=0.666 0,r=0.642 1,P.05),与血清肌酸酐无关。

Among them, p-coumaric acid, cis-aconitic acid, vanillic acid, citric acid were well known antiinflammation active components.

已知对羟基桂皮酸、顺式乌头酸、对羟基苯甲酸、香草酸、柠檬酸具有抗炎活性。

The third category is planted second-generation Chinese fir, the soil phenol content is highest. It shows that along the ecosystem conversion, or as the increase of Chinese fir planted generation, the phenols in soil are accumulated to a certain extent.(6) Detecting the soil of four systems and found that there exist p-hydroxybenzoic acid, vanillic acid and ferulaic acid, but not exist cinnamic acid.

根据主成分分析结果,大致可以把4种系统分成3类,第一类为天然更新常绿阔(来源:ABC论文8f网www.abclunwen.com)叶林,其土壤酚含量低;第二类为老龄杉木林和二代杉木萌芽天然更新林,其土壤酚含量较高;第三类为二代杉木人工林,其土壤酚含量最高。

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