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This process utilizing modern efficient wire gauze wave-like packings sepa-rates three isomers of MNT(ortho-.meta- or para-), then the O-MNT or P-MNTis nitrated to produce military TNT by a mixture of nitric and sulfuric acid.

本工艺利用近代高效的金属丝网波纹填料分离MNT的三种异构体,然后用硝硫混酸把邻一或对一MNT硝化成军品TNT,这样可避免亚硫酸钠溶液精制TNT的工序。

The mouse serum uric acid level and liver xanthine oxidase activity were used to evaluate anti-gout effects of raw and processing P.

以小鼠血清尿酸水平和肝脏黄嘌呤氧化酶活性为指标,评价黄柏生品和盐制品抗痛风作用。

Their structures were elucidated on the basis of chemical and spectral analysis. RESULTS: Twelve compounds were isolated from the 95% ethanol extract of the aerial parts of L.rotata. Their structures were identified as luteolin (1), luteolin 7-O-β-D-glucopyranoside (2), apigenin (3), apigenin 7-O-β-D-glucopyranoside (4), apigenin7-O-6-(E-p-coumaroyl-β-D-galactopyranoside (5), tricin (6), acacetin (7), genkwanin (8), lamiophlomiol A (9), lamiophlomiol B (10), shanzhiside methyl ester(11)and syringic acid (12), respectively.

结果:从独一味地上部分的乙醇提取物中分离得到了12个化合物,分别鉴定为木犀草素(1)、木犀草素7-O-β-D-吡喃葡萄糖苷(2)、芹菜素(3)、芹菜素7-O-β-D-吡喃葡萄糖苷(4)、芹菜素7-O-(6-反式-对-香豆酰基)-β-D-半乳糖苷(5)、小麦黄素(6)、刺槐素(7)、芜花素(8)、独一味素A(9)、独一味素B(10)、山桅苷甲酯(11)及丁香酸(12)。

N-substituted pyrroles are synthesized by reacting acetonylacetone with carbamic ester , catalysted by p-toluenyl sulfonic acid, heated at reflux temperature for 6h, collecting evolved water, giving to 75% yields, which is 26% more than the literature value.

以对甲苯磺酸为催化剂,用甲苯作溶剂,使2,5-己二酮与氨基甲酸酯在110℃反应6h,合成了5种氮取代吡咯衍生物,其中两种未见文献报道,反应产率均达到75%以上,比文献值高出了26%。

It was found that all these compounds are hydrolyzed in different degrees;among which N-(p-chlorophenyl)amidophosphoric acid is the most stable.

而对于不同底物的水解速度与亲和力都不相同,显示磷酸氨基酶活力与底物的结构有密切关系。

The non-volatile taste components in these mushrooms included soluble sugars, free amino acid and flavor 5'-nucleotides. Soluble sugars included arabitol, mannitol, glucose and trehalose and were found in the highest amount in P.

酸。经分析后发现,此四种菇类子实体所含的可溶性糖,包含有阿拉伯糖、甘露糖醇、葡萄糖、肌醇和蕈糖,而可溶性总糖含量则以日本蚝菇所含者(138.75 mg/g)较高。

Rhodamine B, Malachite green, Auramine O, Bismark Brown,Methyl Violet 5BN, Basic Magenta, Acid Orange II, Chrysophenine GX, Direct Fast Black G, Indigo, Sulphur Black, Solvent Red 24, Solvent Red 49, Solvent Brown 41, Solvent Orange 3,Pigment Yellow 154,155, Pigment Red 188,208, Meta-Diethyiaminophenol, M-Amino acetanilide , P-Amino acetanilide, etc.

主要产品:碱性玫瑰精,碱性品绿,碱性嫩黄O,碱性品红,碱性紫5BN,碱性红6DDN,酸性橙II,靛蓝,硫化黑,直接冻黄,直接黑G,溶剂红24,溶剂红49,溶剂棕41,溶剂橙3,溶剂橙62,颜料黄154,155,颜料红188,208,间羟基-N,N-二乙基苯胺,间氨基乙酰苯胺,对氨基乙酰苯胺。

P-π conjugated polyamic acid was synthesized by the poly-condensation of benzoguanamine and pyromellitic dianhydride under microwave irradiation. Then PAA was grafted with different side-chain containing azobenzol groups through azo coupling reaction.

选取苯代三聚氰胺和均苯四酸二酐为单体进行微波辐射溶液聚合反应,所得的聚酰胺酸与对位取代基不同的苯胺重氮盐偶合接枝,从而合成了一系列新的具有三阶非线性光学活性的侧链型聚合物。

For the saturated aromatic aldehydes with malononitrile and barbituric acidit, the reaction was found to proceed very efficiently at room temperature giving excellent yields under ultrasonic irradiation, while for α,β-unsaturated aldehydes as well as p-phthalaldehyde with malononitrile and barbituric acid the reaction also proceeded smoothly at room temperature with good yields.

在超声波辐射下,不仅饱和芳香醛与丙二腈、巴比妥酸的一锅反应在室温下能高收率地进行,而对于α,β-不饱和醛以及二元醛与丙二腈、巴比妥酸的一锅反应也能在室温下顺利进行,获得较高的收率。

Of water (Note 1) and 100 g.(0.44 mole) of benzilic acid (p. 89) are added.

水(注1 )和100克( 0.44摩尔)的benzilic酸(第89页)的补充。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。

There is no differences of cell proliferation vitality between labeled and unlabeled NSCs.

双标记神经干细胞的增殖、分化活力与未标记神经干细胞相比无改变。