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My company can provide pesticide, medicine, veterinary medicine intermediates, have 48 kinds of products (p-Bromo-p-Bromotoluene bromoform 1 - bromo-heptane Triethyl Citrate 1,2,3 - three Bromopropane 3 - Chlorine -4 - fluoro bromobenzene Bromotoluene ethylbenzene 4 - bromo -2 - bromo-ethyl-Chloroaniline 2 - bromo--5 - chloro-toluene 3 - bromo-C methyl 1,6 - dibromo-hexane 1 - bromo --4 - p-methoxy benzaldehyde o-bromo-acetic acid propyl bromide p-fluorotoluene dodecane four bromoethane of iodine bromide toluene tert-butane Tributyl Citrate 2 - bromo-p inter - Hydroxybenzaldehyde bromine butane 2 - bromo-propionic acid bromide veratryl aldehyde inter-bromo-trifluoro-n-hexane of toluene on Bromoxynil Bromotoluene toluene ethylbenzene o-bromophenol bromide Cyclohexane Cyclopentane bran bromate bromide Malay Dibutyl Ethyl Lactate Propylene between bromine bromine bromine between aniline o-anisidine o-fluorophenol difluorobenzonitrile to aminobenzaldehyde Bromotoluene aniline on Bromobenzaldehyde Bromotoluene acid) expressed the hope that customers contact us!

我公司可提供农药,医药,兽药中间体,有四十八种产品(对溴苯酚对溴甲苯溴仿 1-溴庚烷柠檬酸三乙酯 1,2,3-三溴丙烷 3-氯-4-氟溴苯对溴乙苯 4-溴-2-氯苯胺溴乙酸乙酯 2-溴-5-氯甲苯 3-溴丙酸甲酯 1,6-二溴己烷 1-溴-4-硝基苯邻甲氧基苯甲醛溴乙酸丙酯对氟甲苯溴代十二烷对碘甲苯四溴乙烷溴代叔丁烷柠檬酸三丁酯 2-溴氯苯间羟基苯甲醛溴丁烷 2-溴丙酸黎芦醛溴已烷间溴三氟甲苯对溴苯腈对溴乙苯邻溴甲苯溴代环已烷溴代环戊烷糠溴酸马来酸二丁酯溴丙烯乳酸乙酯间溴苯胺间溴苯甲醚邻氟苯酚邻氟苯腈对氨基苯甲醛对溴苯胺对溴苯甲醛对溴苯甲酸)希望广大客户与我司联系!

The main products are: HH-01 fungicides HH-02 organic dispersant HH-03 cationic starch Wood HH-04 cationic starch Department HH-05 modified starch warp sizing agents also sell German Baker Chemical Co., Ltd. Main Products Defoamer series product: E640, T50 Surface Sizing Agent: A281, A288, K532, pesticides / medicine / veterinary medicine a variety of intermediate products (p-Bromo-p-Bromotoluene bromoform 1 - bromo-heptane triethyl citrate 1,2, 3 - Three Bromopropane 3 - chloro -4 - fluoro bromobenzene Bromotoluene ethylbenzene 4 - bromo -2 - bromo-ethyl-Chloroaniline 2 - bromo--5 - chloro-toluene 3 - bromo-methyl 1,6 C - Dibromo Hexane 1 - bromo -4 - nitrobenzene o-methoxy benzaldehyde acid propyl bromide p-fluorotoluene bromo dodecane toluene four of iodine bromide bromoethane three citric acid tert-butane n-butyl 2 - bromo-p-bromo-butane Hydroxybenzaldehyde between 2 - bromo-propionic acid bromide veratryl aldehyde inter-bromo-trifluoro-n-hexane of toluene on Bromoxynil Bromotoluene toluene ethylbenzene o-bromophenol bromide bromide Cyclohexane Cyclopentane bran acid dibutyl maleate Ethyl Lactate Propylene between bromine bromine bromine between aniline o-anisidine o-fluorophenol difluorobenzonitrile to aminobenzaldehyde Bromotoluene aniline on Bromobenzaldehyde Bromotoluene acid) and other relevant units have been in substantial promotion, and client set up a good relationship of cooperation has been the user's praise.

现主要产品:HH—01杀菌剂 HH—02有机分散剂HH—03阳离子淀粉 HH—04木署阳离子淀粉 HH—05 经纱上浆变性淀粉同时还代理销售德国贝克化学公司系列产品主要产品消泡剂:E640 、T50 表面施胶剂:A281、A288 、K532,农药/医药/兽药中间体多种产品(对溴苯酚对溴甲苯溴仿 1-溴庚烷柠檬酸三乙酯 1,2,3-三溴丙烷 3-氯-4-氟溴苯对溴乙苯 4-溴-2-氯苯胺溴乙酸乙酯 2-溴-5-氯甲苯 3-溴丙酸甲酯 1,6-二溴己烷 1-溴-4-硝基苯邻甲氧基苯甲醛溴乙酸丙酯对氟甲苯溴代十二烷对碘甲苯四溴乙烷溴代叔丁烷柠檬酸三丁酯 2-溴氯苯间羟基苯甲醛溴丁烷 2-溴丙酸黎芦醛溴已烷间溴三氟甲苯对溴苯腈对溴乙苯邻溴甲苯溴代环已烷溴代环戊烷糠溴酸马来酸二丁酯溴丙烯乳酸乙酯间溴苯胺间溴苯甲醚邻氟苯酚邻氟苯腈对氨基苯甲醛对溴苯胺对溴苯甲醛对溴苯甲酸)等在相关单位得到了大量推广,与客户建立了良好的合作关系,得到了用户的赞誉。

1 At a reaction temperature of 100 ℃ and a reaction time of 30 min to give 2,which was then subjected to condensation reaction with p-propoxy mandelic acid in the presence of phosphoric acid at a molar ratio of m(2)∶m( p-propoxy mandelic acid )∶m=1∶1∶1 at a reaction temperature of 60 ℃ for 3 h to yield 3,which was further oxidized by chloranil to give t.

对现有分散红356合成工艺进行了优化,以n∶n=1.2∶1投料,100℃反应30 min得缩合物2,再在等质量磷酸催化下与分批加入的等质量对丙氧基扁桃酸60℃缩合3 h得缩合物3,经温和氧化剂四氯苯醌氧化得标题化合物,总收率55%。

The constituents were extracted by some solvents. 18 constituents were isolated from Chloroform fraction by different chromatography. 15 constituents were identified by IR ,MS and NMR as follows: 3-sitosterol, P-sitosterylpalm itate,succinate acids, 1, 4-benzenediol, 1, 2-benzenediol, p-hydroxybenzaldehyde, syringaresinol, oleanolic acid, usolic acid, ethyl caffeate , Rosmarinic acid ethylster and etc. In such constituents ,nine compounds were isolated for first time from Origanum vulgare L..

牛至药材经水煮醇沉法所得浸膏,利用溶剂法和色谱法从中分离得到18个单体成分,通过IR、MS、NMR等波谱技术鉴定了其中的15个化合物,分别为β-谷甾醇(1)、β-胡萝卜苷(2)、琥珀酸(3)、对-二苯酚(4)、邻-二苯酚(5)、对羟基苯甲醛(6)、1.2-二羟基-4-异丙基-5-甲基苯(7)、新木脂素(8)、丁香脂素(9)、齐墩果酸(10)、乌苏酸(11)、4-二十六烯(12)、正二十六醇(13)、咖啡酸乙酯(14)、迷迭香酸乙酯(15)等,其中化合物3、4、5、6、7、8、9、14、15等9种化合物均为首次从该属植物中分离得到。

The contents of organic matter, total nitrogen, phosphorus, iron, manganese, copper, zinc can be increased, and the contents of hydrolizable nitrogen and their forms , Fe-P, Al-P, Ca〓-P, all organic P forms, exchangeable and organic iron, manganese, copper, zinc are increased obviously in long-term application organic manure soil. Not only the contents of soil readily oxidizable carbon, humic acid, fuluic acid, and HA/FA value are increased and Kos value decreased but also the available nitrogen, phosphorus, iron, manganese, copper, zinc are kept more high level in the organic manure soils. Long-term mulching straw has similar role with organic manure for soil nutrient except for decreasing total phosphorus, available P, N and Ca〓-P, but its fertilizer efficiency is not better than organic manure.

有机肥还具有提高土壤易氧化碳和松结态腐殖质含量,降低kos值,提高土壤HA、FA含量及其比值的作用,使土壤中有效态氮、磷、铁、锰、铜和锌含量处于中上等水平;长期秸秆还田除了不增加土壤全磷、有效氮和磷等外,对其他养分的作用效果与有机肥相似,但其肥效不如有机肥;长期氮磷化肥单施,土壤全氮和磷增加,有机质、铁、锰、铜和锌含量下降,易氧化碳、松结态腐殖质、HA和FA含量、kos和HA/FA值下降;长期不施肥土壤有机质、全氮等养分处于消耗状态。

The purification-pretreatment technique of 8 kinds of solid phase extracting column stuffing (silica gel, acid silica gel, Florisil, siliceous magnesium sorbent, Al2O3, celite 545, acid celite, Al2O3+silica gel) for the prepared polluted soil containing 13 kinds of organochlorine pesticides (α-HCH,β-HCH,γ-HCH,δ-HCH, o,p'-DDT, o,p'-DDE, p,p'-DDT, p,p'-DDD, p,p'-DDE, a-endosulfan, dieldrin, endrin, hexachlorobenzene) was screened prior.

用製备的8种固相萃取柱填料(硅胶,酸化硅胶,氟罗里硅土,硅镁型载体,Al2O3,硅藻土载体545,酸性硅藻土,Al2O3+硅胶)对含有13种有机氯农药的污染土壤的纯化预处理技术进行了优化筛选。

In the recent years, the company has developed series of the down-stream derivatives of P/O-Chlorotoluene, i.e. 3,000 t/a O- Chlorobenzaldehyde and O-Chlorobenzyl Chloride, 3,000 t/a P- Chlorobenzaldehyde and P-Chlorobenzyl Chloride, 1,500 t/a 2.4- Di chlorotoluene etc. In addition, there is the by-product of 30,000t/a of chlorhydric acid (31-33%). In 2008, the company invested 80 mln yuan, to build the project with 25,000t/a of Maleic Acid by adopting the up-to-date in China technology, thus to improve the product range to a greater extent, and hence to sharpen its competitive edge.

近年来又发展了对、邻氯甲苯的下游衍生系列产品:3000t/a邻氯苯甲醛、邻氯氯苄,3000t/a对氯苯甲醛、对氯氯苄,1500t/a2,4-二氯甲苯等,另有副产盐酸(31~33%)30000t/a.2008年,公司投资8000万元,采用国内最先进的技术建成了25000t/a顺丁烯二酸酐项目,大大改善了公司的产品结构,提高了企业的竞争能力。

To evaluate the potential of several biodiesels, which had different content of fatty acid methyl ester, as substitute solvent for quizalofop-p-ethyl emulsifiable concentrate, the type and content of fatty acid methyl esters in tested biodiesels were analyzed by gas chromatography, and 5% quizalofop-p-ethyl ECs were prepared with different biodiesels, respectively. The control test against gramineous weeds by the 5% quizalofop-p-ethyl ECs were carried out in greenhouse.

为评价不同来源生物柴油作为溶剂配制精喹禾灵乳油的效果,采用气相色谱法测定了几种生物柴油中脂肪酸甲酯的种类及含量,利用相应制备的5%精喹禾灵乳油进行了防治禾本科杂草的盆栽试验,同时比较了不同生物柴油对药剂稀释液表面张力、干燥时间和在叶片表面沉积量等药液物理性状的影响。

The chemical analysis of N, P and K in organic fertilizer is presented: sample is decomposed by sulfuric acid-hydrogen peroxide and prepared to be a solution. N can be determined by NC-2 model quick N analysis set, P by chinoline molybdic acid method and K by tetraphenylboron potassium, needless of spectral photometer and flame photometer, the method is available when the content of N, P or K is over 0.1% with desired accuracy and precision.

介绍用化学分析方法测定有机肥料氮、磷、钾的含量,即样品经硫酸-过氧化氢消化后,制备待测溶液,分取待测溶液用NC-2型快速定氮仪测定氮,用磷钼酸喹啉重量法测定磷,用四苯硼酸钾重量法测定钾,不需使用分光光度计和火焰光度计,适宜一般复混肥料厂采用,对含氮、磷、钾分别达0.1%以上的样品均可用本法测定,方法的准确度和精密度能满足生产的要求。

Oxalic acid loading substantially stimulated soil P release from A1 horizon, showing a linear relationship; but its effect on B horizon soil was relatively negligible, especially at low oxalic acid concentrations mmol L^(-1. Oxalate solutions 0.5~20.0 mmol L^(-1 oxalic acid adjusted to pH 5.16 with 10.0 mmol L^(-1) NaOH had a much higher (1.51~2.98 times) soil-P-release effect than oxalic acid solution the same in oxalate concentration. Therefore, the mechanism of oxalic acid/oxalate triggering release of soil phosphorus is assumed to be dominated by ligand-exchange or complexing reactions of oxalate anionC2O(superscript 2- subscript 4 but not simply acid-dissolving effect. The effect of oxalate anion on soil phosphorus release was found to be somewhat cumulative, i.e. the amount of P released was primarily controlled by the cumulative oxalate loading rate, relatively independent of the manner of oxalate addition (one-time or sequential).

结果表明,草酸能显著促进暗棕壤A层磷的释放,土壤磷溶出量随草酸溶液浓度升高而线性增加;但对B层土壤磷的释放效应相对较弱,草酸浓度低於5mmolL^(-1)时B层磷的释放不明显。pH5.16草酸钠溶液比相同浓度的草酸溶液具有更高的解磷效率,在设置二者浓度为0.5~20.0mmolL^(-1)时,前者的解磷量是后者的1.51~2.98倍,推断草酸盐溶液或凋落物淋洗液中草酸类物质促进暗棕壤磷释放的主要机理在於草酸阴离子C2O(上标 2-下标 4配位反应。

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