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The main object of this research is to investigate synthesis of Cu23Cl Cu and CuO nanoparticles through electrospinning and heat-treated method The research is mainly focused on preparative parameter and the change of heat-treated temperature to form the nanoparticles inlaid in silicon fibers the shape and color change are dicussed First of all to prepare the Polyvinyl butyral and silica dioxide complex nanofiber by electrospinning and then to investigate different heat-treated temperature and reactive time to being an influence on the products The results detected by SEM XRD TEM EDS FTIR combined sol-gel process and electrospinning can prepare Polyvinyl butyral and silica complex nanofiber The experimental result is found when heat-treated temperature is 100~4750C it can produce Cu23Cl nanoparticles; Above 4750C~ 4900C it can produce Cu nanoparticles; Above 450~7000C it can produce CuO nanoparticles And the viscosity is lain between 20~40cp and the sol-gel process time is 3hr it can produce the thinner fibers The average diameter of the fibers are 107 88±21 01nm;Due to the nanoparticles inlaid in the silica fibers the thinner fibers can be inlaid the smaller nanoparticles so this is the result that the experiment is expected To calcine the complex fibers is to produce surface silica fibers contain Cu23Cl Cu and CuO nanoparticles due to surface plasma resonance it make the color of the fibers become yellowish green from light white green turn into the red nuclear finally As the experimental result to utilize sol-gel process combine electrospinning can produce porous silica fibers contain Cu23Cl Cu and CuO nanoparticles
本研究旨在探讨「利用放电纺丝和热处理法来合成Cu23Cl、Cu和CuO奈米粒」之研究,实验著重在制备参数与热处理温度变化对所形成的奈米粒镶嵌在二氧化矽纤维中的形态与颜色变化探讨。首先,利用放电纺丝法制备出聚乙烯醇缩丁醛及二氧化矽之奈米纤维,比较不同的热处理温度与反应时间的改变对产物生成产生影响,进而研究不同热处理温度和时间对生成奈米粒的影响。产物经由SEM、XRD、TEM、EDS和FTIR等仪器分析结果显示,结合溶胶-凝胶法(sol-gel process)和放电纺丝法可产生聚乙烯醇缩丁醛及二氧化矽复合奈米纤维。实验结果发现,若热处理温度在100~4750C下可得到Cu23Cl奈米粒,475~4900C 可得Cu奈米粒,450~7000C以上可得 CuO奈米粒。而黏度介於20~40cp间和溶胶-凝胶时间为3hr时,可产生直径比较细的纤维,纤维直径为107 88±21 01nm;且由於奈米金属颗粒镶嵌在二氧化矽纤维中,直径比较细的纤维,可以得到比较小的奈米金属颗粒,这与实验预期相符。而锻烧此复合物产生多孔的二氧化矽纤维并包含Cu23Cl、Cu和CuO奈米微粒时,由於表面电浆子共震关系,而使纤维颜色由淡白黄绿色变成黄绿色,再变红褐色。由实验结果得知,利用溶胶-凝胶法(sol-gel process)结合放电纺丝法和不同热处理温度,可产生Cu23Cl、Cu和CuO奈米粒镶嵌在二氧化矽纤维。
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The findings knew that the ships collision is a type of an act of tort , its liability asks to recompense is looks carefully the state of fault to decide , generally may divide into the force majeure or the unknown cause collision , the mutual fault of both sides collision and so on , because if the force majeure or the unknown cause collision , undertake voluntarily by the victim , if an error of the side undertakes the damage compensate responsibility by the inflicter , when if both sides have mutually to cause its faults , basically it depends on the fault to share , but if it's unable to judge the proportion then the average to share is necessary.
研究结果得知,船舶碰撞为一典型之侵权行为,其责任求偿乃端视过失型态而定,一般可分为不可抗力或不明原因之碰撞、单方过失碰撞及双方互有过失碰撞等,而若因不可抗力或不明原因之碰撞者,由受害人自行承担,若纯为一方之过失者则由加害者承担损害赔偿责任,若因双方互有过失所造成时,原则上依过失程度分担,但若无法判定比例时则平均分担。
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This thesis analyzes the types and art trait of solar-assisted heat pump water heater, the development trend of direct expansion solar-assisted heat pump water heater, makes a summary of these research results from six aspects. On the basis of these works and from the point of view of receiving optimum solar radiation , the thesis develops a novel design model of direct expansion solar-assisted heat pump water heater with a truncated cone collector/evaporator, theoretically analyzes the heat that the system can absorb, compares its ability with other two types of cylinder and flat plate ones, and calculates COP and EER with computer aids. The results show that a truncated cone direct expansion solar-assisted heat pump water heater can absorb not only more solar energy but heat energy in air. It takes on favorable thermal performance. Under the average day in February which is of the worst weather throughout the year in Kunming, the COP is about 4. 2, EER is about 2.9 . The heat absorbed by the system are more than those of the other systems. The system is very great in terms of saving
本文分析研究了太阳能热泵热水系统的分类及技术特点,直膨式太阳能热泵技术国内外发展趋势,从六个方面对直膨式太阳能热泵热水系统的研究进行了归纳总结;在此基础之上,从太阳辐射的最佳接收考虑,提出了集热器/蒸发器为圆台侧面的圆台型直膨式太阳能热泵热水器的设计模型,理论上分析了这种热水系统所接收的太阳辐射和得热量,并与圆柱型、平板型的直膨式太阳能热泵热水系统进行对比分析,通过计算机辅助模拟计算出:系统不但可以有效地吸收太阳能,还能有效地吸收空气中的热量,具有良好的热性能;在昆明,以2月为代表的冬季,其太阳辐照较低,系统的制热系数COP值也能达到4.2,效能比EER值为2.9;系统的得热量高出圆柱型、平板型的直膨式太阳能热泵热水系统,节能效果明显。
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Research makes clear as a result: TC measure has apparent seasonal change feature, average scale is in the biggest April, achieve 230.4km, the smallest Feburary, for 69.5km;TC measure apparent area distributings inhomogenous sex, the area of TC measure occurrence maximum is located in 28.6 ~ 29.5 ° N, 133 ° of 131.1 ~ on the offing of E, and it is to the south of 123 ° E with 12 ° N with south area, TC measure often is under 200km; the TC to different intensity, its measure and intensity luffing have apparent difference, tropical storm (the 24h measure luffing of TS) is the biggest, and typhoon (the dependency of measure of the biggest;TC and intensity is in the 24h intensity luffing of TY) is discrepant below different method, on northwest travel, westing, north model TC measure and intensity show remarkable positive to close, both correlation coefficient achieved 0.93 above, northeast travel and whirly model the correlation coefficient of TC measure and intensity is adjacent 0.6, change direction model the correlation coefficient of TC is in 0.85 or so; in addition, the dependency of TC measure and intensity in its the different level of life history also is put in notable difference, sending exhibition period, the dependency of measure and intensity is best, its correlation coefficient...
探究结果表明:TC尺度有明显的季节变化特征,平均尺度在4月份最大,达到230.4km,2月份最小,为69.5km;TC尺度有明显的区域分布不均匀性,TC尺度出现最大值的区域位于28.6~29.5°N,131.1~133.0°E的海面上,而在123°E以东和12°N以南地区,TC尺度往往都在200km以下;对于不同强度的TC,其尺度和强度变幅有明显差异,热带风暴的24h尺度变幅最大,而台风的24h强度变幅最大;TC尺度和强度的相关性在不同路径下是有差异的,西北行、西行、北上型的TC尺度和强度呈显著的正相关,两者的相关系数达到了0.93以上,东北行和回旋型的TC尺度和强度的相关系数接近0.6,转向型TC的相关系数在0.85左右;此外,TC尺度和强度的相关性在其生命史的不同阶段也存在显著差异,在发展期,尺度和强度的相关性最好,其相关系数。。。
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The periostea of both experimental and control side of the mandibular ramus were taken and prepared, 2 of each 5 rabbits in a group were prepared for HE stain detection and 3 for proliferating cell nuclear antigen immunohistochemical detection.Results:1, The newly formed bone was detected on the lateral aspect of mandibular ramus after periosteal distraction. The bone was shaped like a hill. It looked very low and was full of holes at postoperative day 28. With the time of consolidation period lengthened, the newly formed bone matured gradually. X-ray examination showed the new bone shaped like a hill. The average values of new bone height at postoperative days 28,35,42 and 56 were 1.86 + 0.15mm, 2.29 + 0.29mm,3.19 + 0.13mm and 4.70 + 0.45mm. Histological examination of both HE stain and picricacid-fuchsin stain showed the increase in the number of osteoblasts and the change in the orientation of collagen fibers and bone trabecula. There were no significant differences between newly formed bone and original bone on the lateral aspect of mandibular ramus at postoperative day 56 histologically.2 Compared with the control side, the distracted periostea proliferated obviously under the microscope, and the number of periostealcells increased with satiation of cellular nuclear per unit area. The images of PCNA immunohistochemical stain of periosteum showed that the experimental periosteum proliferated obviously after distraction compared with the control side.
结果:骨膜牵张成骨的实验研究南京医科大学硕{学位论文l、骨膜牵张后,可见下领升支外侧的骨皮质上有新骨形成,新骨呈山峰状凸起,术后第28天的新生骨较低平,多孔隙,随着固定时间的延长,新骨逐渐成熟;下领升支前后向切线位X线投照显示新骨呈山峰样隆起;经测量,术后第28、35、42和56天组平均新生骨厚度分别为x.86士0.15mm、2.29士0.29mm、3.19士0.13mm和4.70 土0.45mm;脱钙骨组织的HE染色和不脱钙骨组织的苦味酸一品红染色的组织学观察均显示了新生骨在成骨细胞数量上的增长,以及胶原纤维和骨小梁排列方向上的变化,术后第56天的新生骨在组织学上与原升支骨组织已无明显区别。2、HE染色显示,与对照组相比较,实验侧骨膜增生明显,细胞间排列紧密,单位面积内骨膜细胞数增多,细胞核饱满;骨膜PCNA 免疫组化染色显示,与对照侧相比较,实验侧骨膜在牵张后出现了明显的增生迹象,PCNA阳性细胞分布紧密,单位面积内阳性细胞数较对照组多,靠近骨表面的骨膜中的阳性细胞数更多而且分布更为紧密。
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The results show that concentration of ownership has a significant impact on risk-taking. The higher the largest shareholder's shareholding percentage, the higher the risk-taking is; the higher the top five shareholders' shareholding percentage, the lower the risk-taking is. The percentage of untradeable shares, the size of the board of directors, the proportion of independent directors and the average remuneration of top 3 senior executives with the highest remuneration are negatively correlated to the risk-taking. However, the situation that the chairman or vice chairman concurrently holds the post of president or CEO increases the bank's risk exposures to a certain extent. Proportion of state-owned shares, the nature of the largest shareholder and the executives' shareholding have no significant impact on risk-taking.
结果表明,股权集中度对风险承担产生了显著的影响,其中第一大股东持股比例越高风险承担越高,而前五大股东持股比例越高风险承担越低;非上市流通股比例、董事会规模、独立董事比例以及薪酬最高的前三名高管的平均薪酬均与银行风险承担负相关;银行董事长同时兼任行长在一定程度上倾向于增加银行的风险承担;国有股比例、第一大股东性质和高管持股状况没有对风险承担产生显著影响。
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The players in different positions have different action combinations in the match. The action combination group is made of different action combination. The players, body action in the match is mostly reflected by action combinations.3. The setter has the most average HR among the match in our excellent men volleyball players. The HR is 143 times every minutes; the assistant spikier,s HR is 136.5 times every minutes; the spikier,s HR is 127 times every minutes; the assistant setters HR is 121.5 times every minutes; and the libero,s HR is 136.5 times every minutes.4. There are some questions in the exercise on specialized physical constitution of our men and women volleyball players. The questions are: the principle about the wholly exercise is not clearly bodied; the exercises are not perfectly coincided the position distinguishing; the exercises of specialized physical constitution are not prominent; the content about the exercises of specialized physical constitution is not like the match.5. The excellent volleyball players in different positions have the different demands on the specialized physical constitution.
不同位置运动员在比赛中表现出的动作组合形式不同,不同的动作组合之间相结合又形成了不同的动作组合集,运动员在比赛中的身体活动主要是以动作组合集的形式表现出来的。3我国优秀男子排球运动员,在一场比赛中,二传的平均心率最高,为143次/分;副攻平均心率为136.5次/分;主攻的平均心率为127次/分;接应二传的平均心率为121.5次/分;自由人的平均心率为109.5次/分。4目前我国国家男排和女排运动员专项身体素质训练还存在一些问题,主要体现在四个方面:1、专项身体素质训练整体性原则体现不足2、没有很好地结合排球运动员专项身体素质的位置特征3、专项身体素质训练重点不突出4、专项身体素质训练内容不贴近比赛实际。5不同位置优秀排球运动员对专项身体素质的发展要求不同,或者说排球运动员专项身体素质具有位置特征。
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On the termination date, the cultured explants were all examined by Western blot, HE and transmission electron microscope. Our results showed that after 12-days in culture, the cultivation treated with AS-ODN reduced the synthesis of AMBN and had a deformed dental cusp with thinner enamel matrix. Ultrastructure analyses showed that there was hardly any cisternae of the rough endoplasmic reticulum in the ameloblasts at the tip of the cusp of AS-ODN treatedexplants. However, on average the enamel matrix was thinner compared with that in the control group. Furthermore, the collagen fibers in extracellular matrix were found disorganized. These findings seemed to provide a direct experimental evidence that tended to indicate that the arrested AMBN translation in cultured tooth germs might result in the delay of the tooth development.
经用Western蛋白印迹检测表明,所设计的反义核酸对AMBN InRNA具有良好的封闭效果并成功阻断了牙胚对AMBN的表达;在缺乏AMBN情况下,与对照组相比,实验组牙胚在体外可以继续生长发育至钟状晚期,出现成釉细胞和成牙本质细胞的分化,成釉细胞可以分化成为分泌期型成釉细胞,胞浆中缺少合成蛋白质所必需的粗面内质网和高尔基氏体,缺乏溶酶体,表明对蛋白合成和脚的能力降低;实验组牙胚有牙尖形成和基质分泌,但牙尖形态异常,基质形成减少,牙尖周围基质最厚处为O.6卜m,明显薄于对照组的5.spin,基质中胶原纤维粗细不等,排列稀疏, 3 第四军医大学硕士学位论文未见钙化现象,充分证明了AMBN在牙胚发育中参与釉质基质形成和矿化过程,影响胶原纤维和牙本质基质的合成,促进成釉细胞对蛋白质的合成和釉质基质蛋白降解。
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For each strategy, a corresponding exploitation plan of groundwater was designed. Then each designed exploitation plan (except scheme 3) was put into the model for calculation and simulation. The analysis on the forecasting results every plan indicates that:(1) Shuting down the self-provided wells is the most direct and effective method, playing an important role in the land subsidence prevention.(2) The resumption of compressed soil by groundwater artificial recharge is limited. So the artificial recharge can\'t provide essential effect for the resumption of land subsidence, unless the artificial recharge is much more than the groundwater withdrawal.(3) The method of "adjusting the exploitation stratum of groundwater to the shallow" has an obvious effect on the land subsidence prevention.(4)"Sand wells" can increase the leakage recharge for confined aquifer, and thus can slow and prevent the development of the land subsidence.(5) For the groundwater exploitation in Xi\'an, emergency self-provided wells should be managed according to the well spacing of 1600m, 2000m and 1600m, respectively, in the river terrace area, alluvial-proluvial fan area and loess tableland area to exploit the first confined groundwater. Corresponding individual well yield can be set as 2500m~3/d, 1500 m~3/d and 200 m~3/d. Make emergency self-provided wells pump in the dry year and stop pumping groundwater to restore and conserve underground water sources in average years and wet years. In this way, groundwater withdrawal of 162000m~3/d can be obtained to provide for the supplement of water supply in Xi\'an. As a result, the water supply stress can be released in dry years. The groundwater depression formed in the exploiting year can resume in 3-4 years. At the same time, this exploitation manner will not lead to obvious land subsidence.
本文利用所建的模型预测了现状开采条件下未来20年的地下水位和地面沉降的变化,在此基础上,提出了防治西安市地面沉降的五个地下水开采方案,利用所建的地面沉降模型对各个设计方案其进行了模拟和预报,对预测结果的分析表明:①封停自备井是防治地面沉降最为直接和最有效的对策,对防治地面沉降起着最为积极的作用;②采用人工回灌方法使被压缩的土层得到的恢复是非常有限的,对地面沉降不能起到根治作用,只有回灌量明显大于开采量时才能有一定的效果;③&调整开采层次,在浅层取水&对防治地面沉降的效果十分明显;④布设&砂井&可以增加对承压含水层的越流补给量,从而可以有效地缓解和控制地面沉降的发生和发展;⑤对西安市的地下水开采,可在河流阶地区、冲洪积扇区和黄土塬区分别采用1600m、2000m、1600m的井间距布置应急自备井,分别采用2500m~3/d、1500 m~3/d和200 m~3/d的单井开采量,开采第一承压水,在平水年或者丰水年不开采,涵养地下水源,在枯水年启动这些应急自备井开采,在输出分析范围内共可获得162000 m~3/d(5913万m~3/a)开采量,可以有效地补充西安市的供水水源,缓解供水紧张局面,开采年开采导致的下降的水位可在停采3~4年后得到基本恢复,同时,这种开采方式不会造成大的地面沉降量。
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As to the first research topic, we present a 'Noble Brand Positioning Four Master Phases Theory': Brand Space Theory, Brand Capital Theory, Brand Value Theory and Brand Circle Theory in advance. Following based on the Principal Component Analysis of statistical theory, we implemented the quantitative research in the 'Noble Brand Positioning Four Master Phases Theory'. We used the most famous fast food brand 'McDonald' s' as the sample space. The simulation test result shows that the Overall Index Explanatory Power is 83% under the Cronbath' s a is 0.88 through the quantitative verification. This result gives a strong support in defining the Noble Four Niche Phases Theory as the important strategic factor in establishing brand positioning index. After completing the quantitative research, the Principal Weight of each Sub-Niche is positive. This also implies that the Noble Brand Positioning Four master Phases Theory represents positive affection to brand positioning index. We also created the following Sub-Niches those are rarely mentioned in the past literatures. The Sub-Niches are:'Endless Running Strategy, Business Environment Strategy, Physical Capital Strategy, Brand Logo, Brand Music, Business Life Strategy, Personnel Capital Strategy, Life Cycle Strategy, Trust Mask Strategy, Re-Positioning Strategy, Word-Power Strategy, Globalization Strategy, Network Revolution Strategy and Green Brand Strategy'. The quantitative verification model can classify the responses of the sampling space into groups. After that, we used the quantitative verification process to classify the Target Consumer. And through the Principal Component Analysis, the group that owns the biggest average value consists of the Master Target Consumers for the business. This result would become the best suggestion for the business to adjust its strategies and to upgrade the productivity efficiency and create higher profit. As to the second research topic, we focused on finding the best corresponding characteristics attributes of the Brand Music for the Brand Log.
针对第一个研究主题,本文首先提出了一种创新性的品牌定位利基理论(A New Brand Positioning Niche Phase Theory);品牌空间论,品牌资本论,品牌价值论与品牌循环论,接着本文以统计理论的主成份分析方法针对本文所提的创新性的品牌定位利基理论进行量化研究,本文以快餐业中知名品牌麦当劳作为样本空间,由量化验证的结果显示在信度分析Cronbatch's α为0.88之下其总指标解释力(Overall Index Explanatory Power)为83%,验证本文所提的创新性的品牌定位利基理论是构建品牌定位的重要策略因素,同时经由量化分析结果每项主成分权重值皆为正值更验证了本文所提的企业创新性的品牌定位利基理论与品牌定位指标呈现正相关:同时本文所提出次利基:'永续经营策略、企业环境策略、实体资本策略、企业生命策略、品牌标志策略、品牌音乐策略、人际资本策略、生命周期策略、信任标志策略、重新定位策略、文字威力策略、放眼全球策略、网络革命策略与绿色品牌策略'更是其它文献所未提及的:本文量化验证模式更可将样本空间中的responses分类群组,然后量化验证以界定目标市场,经由分析结果显示,其中具最大主成份百分位序均值者所属群组,即为企业中的主力消费群,提供企业决策者参考,进而调整其企业策略,而为企业提升生产效率创造更大的利润。
- 推荐网络例句
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We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.
索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称;三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起,称之为挽歌体诗人或者史诗诗人,他们被称为诗人,似乎只是因为遵守格律写作,而非他们作品的模仿本质。
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The relationship between communicative competence and grammar teaching should be that of the ends and the means.
交际能力和语法的关系应该是目标与途径的关系。
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This is not paper type of business,it's people business,with such huge money involved.
这不是纸上谈兵式的交易,这是人与人的业务,而且涉及金额巨大。