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In connection with the character of Boc L-Glutamic Acid and aminoacetic acid structures, the reaction of aminoacetic acid acylated via Boc Anhydride has been studied on the condition of CH3OH in the paper. The yield of the derivatives is characterized by the melting point, the content of carboxylgroup and the product purity. The results showed that the best experiment condition is followed.

本论文以甲醇作为均相反应介质,Boc酸酐与谷氨酸为原料,在碱性条件下,以产物的熔点,羧基含量以及产物纯度作为产物质量确定的指标,最终得出N-Boc-谷氨酸的合成最优条件。

Moreover,the paper discusses the exiting schemes on binning termination condition,points out their problems,and proposes a more reasonable termination condition.The experimental results show that the novel approach is effective.

1引言在高质量真实感图像渲染领域,光线跟踪技术近年来得到了长足的发展,这一方面得益于硬件性能的提高,另一方面是由于高质量的加速数据结构的提出及改进,以及基于这些加速结构的遍历算法[1-3]的应用。

This paper found the structure of hydraulic excavators condition monitoring and failure diagnosis system at first.That is a system composed of hypogynous SCM realizing on-line condition monitoring and epigynous PC realizing off-line failure diagnosis.Then the function and testing principle of hypogynous system is analyzed.The design of system hardware circuit and software formality are introduced.

本文首先构建了液压挖掘机状态监测与故障诊断系统结构,即由实现在线状态监测功能的下位单片机和实现离线故障诊断功能的上位PC机组成的系统;然后确定了下位机系统的功能,分析了测试原理,设计了硬件电路和软件程序。

It is demonstrated that existence of inflection point on velocity profile is a sufficient condition, but not a necessary condition for flow instability, for both inviscid and viscous flows.

它表明存在速度剖面拐点充分条件,但不是必要条件流不稳定,都粘和粘性流动。

For naturally cooled monobloc barrel, its thermal condition in regular regime can be evaluated by measuring the outside temperature of two arbitrary rounds;(2) During a sustained firing process, unsteady heat conduction exists in a monobloc barrel, whereas unsteady and quasi steady heat conduction exist with actively cooled composite barrels, meaning that the thermal condition changes from uncontrolled to controlled;(3) Different combinations of the convective heat transfer coefficient h and thickness of gun barrel δ have much effects on cooling the bore temperature.

利用有限元软件分析了某大口径火炮身管的温度场分布,并对自然散热条件下的单筒身管和主动冷却条件下的复合身管温度场进行了比较,其结果为(1)身管温度场分布存在初始和正规工况阶段,后者的单筒身管热状态可以通过测定任意两发身管外表面温度来评估;(2)持续射击过程中,单筒身管始终处于非稳态导热过程,主动冷却身管则包括非稳态和准稳态两个过程,实现了身管热状态由不可控向可控转变;(3)对流传热系数h和身管壁厚δ的组合对降低内膛温度具有很大影响。

Results:(1) FSN can inhibit secondary joints swelling and multi-arthritis evidently, improve the whole condition of rats; at the same time, it can also lighten the synovial inflammation and hyperplasia of lesion joints distinctly, and prevent the joint cartilage and bone from destruction; the collective efficiency of FSN is better than TWP.(2) FSN can raise AA rats low LTT of spleen to normal nearly, remedy the disorder of Th / Ts and Thl / Th2 cells balance in peripheral blood, restrain exorbitant TNF- a ? IL-1 produced by PM O , thereof exert anti-inflammatory and immunoregulation effect.(3) Inside the lesion joints, FSN can depress abnormal hyper-expression of TNF- a mRNA and NF-kB in synovial tissues, as well as advance the expression of Caspase-3 (a proteolytic enzyme of apoptosis), reduce synovial immflamination and proliferation.(4) FSN can lower the expression of VEGF in synovial tissue,reduce neogenetic veins, so inhibit the growth of pannus tissue and the damage of cartilage and bone by that.(5) The above effect of FSN are in proportion to its dosage.Conclusions: FSN has inhibitory effects on symptom and condition of experimental RA, which is better than TWP as a whole.

结果:(1)FSN有明显的抗炎作用,可显著抑制AA大鼠足跖肿胀与多关节炎,改善大鼠的全身情况,同时明显减轻病变关节滑膜炎症与增生,防止关节软骨及骨质的破坏,其综合作用优于TWP;(2)FSN还能使AA大鼠低下的脾LTT恢复至接近正常,纠正外周血中T细胞亚群Th/Ts及Th1/Th2平衡紊乱,抑制大鼠PHφ过高的TNF-α、IL-1分泌,而发挥抗炎和免疫调节作用;(3)在病变关节局部,FSN能显著抑制AA大鼠滑膜细胞异常增高的TNF-αmRNA的表达,降低滑膜组织中NF-kB表达,并增加凋亡蛋白酶Caspase-3表达,从而抑制滑膜的炎症与增殖;(4)FSN还可下调滑膜组织中VEGF表达,减少血管新生,由此抑制血管翳的形成及其对软骨和软骨下骨的侵蚀;(5)FSN的上述作用皆呈现一定的量效依赖关系,高剂量组作用优于低剂量组。

Flushing distances of both Pluvialis dominica and Calidris temminckii under the condition of one person walking were less than those under the condition of two persons walking, which indicated that two species of bird were susceptive on the disturbance type including more persons.

这说明,两种鸟类对人数较多的干扰类型更为敏感。在一人行干扰条件下和二人行干扰条件下,金斑鸻的惊飞距离均显著小于青脚鹬的惊飞距离。

The making condition for releasing cholesterol from the inclusion compound was found based on the single factor experiments. The experiments demonstrated that the releasing rate of cholesterol was reached to more than 97% in the optimum condition including pH value 9.5,regurgitant time hour,concentration of edible ethanol 96% and regurgitant temperature 80C.

利用单因素实验确定山包合物释放胆固醇的优化工艺条件:pH值为9.5,回流时间为1h,乙醇浓度为96%,回流温度为80℃,此时胆固醇的释放率达到97%以上。

A combination analysis of SIP and in situ microbiological methods was applied on the anaerobic digestion of biomass organics suffering from severe acids inhibition. The studies found that accumulated acids were degraded mainly by Methanosarcina firstly with acetoclastic pathway and then with hydrogenotrophic pathway under mesophilic condition, whereas acids were mainly degraded to methane by the tandem reactions of syntrophic acetate oxidation and hydrogenotrophic methanogenesis under thermophilic condition.

联合应用稳定同位素表征技术和微生态原位表征方法,对高浓度有机酸胁迫条件下的生物质类有机物厌氧发酵甲烷化途径的研究结果表明,面临高浓度有机酸迅速累积的环境,中温发酵条件下,优势菌种为甲烷八叠球菌,依时间次序,通过乙酸发酵和氢营养型途径利用累积的有机酸产生甲烷;而在高温条件下,有机酸则通过乙酸氧化和氢营养型甲烷化途径的串联反应被降解。

Based on two kinds of control strategies of VSR under unbalanced grid condition,the introduction of a new VSR control strategy featuring undamped -oscillation that simplifies the controller structure and effectively improves VSR"s performance under unbalanced grid condition.· A systematic description of the state switching in trilogic PWM signal generation of three-phase CSR by using the conversion between bilogic and trilogic switching functions.· Referenced to the CSR"s trilogic PWM signal generation, an approach to achieve low-stress natural commutation of switching devices by reshuffling the vector composition sequence, resulting reduced switching loss.

在研究了两类电网不平衡时的VSR控制策略基础上,提出了一种新型的基于无阻尼振荡控制器的VSR不平衡控制策略,在简化控制结构的同时,有效地改善了电网不平衡时的VSR控制性能;·通过二、三值逻辑开关函数间的转换,系统地描述了三相CSR三值逻辑PWM信号发生中的状态切换;·结合三相CSR三值逻辑PWM信号发生规律,提出了通过调整矢量合成顺序而使功率管获得自然换相的低电压应力SVPWM控制,从而有效地降低了功率管的开关损耗。

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