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The interfacial chemistry, synergistic effects and interfacial kinetics of thesynergistic extraction system D_2EHPA-MPA-Fe~(3+) have been studied, where MPA is amono-alkyl phosphate extraction with long carbon chain. D_2EHPA in the mixed extractionsystem strongly exhibits the effect on the thermodynamics of micella formation and interfaceproperties of MPA. Some thermodynamic parameters of micella formation were obtained.The interfacial adsorption behaviour of D_2EHPA is opposite to that of MPA. Theemulsification for single MPA and the mixed system was discussed. The synergistic effectswere found in this mixed extraction system. It is proved that the process of Fe~(3+) extractionfor non-mixed extraction system is controlled by chemical reaction, the controlling reactionoccurs at the interface, and the reaction rate equation is obtained.

本文研究了协同萃取体系D_2EHPA—MPA—Fe~(3+的胶团形成热力学、界面特性、协萃效应和界面动力学(动力学控制机制和反应速率方程)研究发现,混合萃取体系中的D_2EHPA强烈地影响MPA的胶团形成热力学和界面吸附行为,得到了胶团生成常数、胶团形成自由能和临界胶团浓度的热力学参数D_2EHPA和MPA具有相反的界面吸附行为研究发现D_2EHPA—MPA混合萃取剂体系对Fe~(3+)产生了协萃效应动力学和界面化学的研究结果还证实了非胶束混合萃取体系的Fe~(3+)的萃取过程是受化学反应控制的,控制反应发生在界面上

The chemical formula of the phosphor is SrMoO4:Eu. The method comprises the following concrete steps that: according to the molar ratio of 2:100:100 to 4:100:100, Eu2O3, MoO3 and SrCO3 solids are put into a mortar to be ground and fully mixed; an obtained product is placed in a crucible in a muffle furnace to be roasted for 3 to 4 hours at the temperature between 500 and 700 DEG C, and then a needed product can be obtained.

该荧光粉的化学式为:SrMoO 4 :Eu 3 ,具体步骤为:将Eu 2 O 3 ,MoO 3 和SrCO 3 固体按照摩尔比为2∶100∶100~4∶100∶100的比例置于研钵中研磨,使其充分混合;将所得产物置于坩埚内放在马弗炉中于500℃~700℃的温度下焙烧3-4h,即得所需产品。

Finally, the results obtained in the application of this method to different test waveforms are compared with the results obtained using the IEC method.

最后,取得的成果在应用这种方法,以不同的测试波形进行比较,所取得的成果运用的IEC方法。

This paper reviewed the developments in 2-D numerical model of the water flow. By means of the latest observation data of the prototype, the detailed analysis was made on the major thalweg, section, island and bottomland, the erosion and deposition of the river bed and the scour hole near the dock and the law of the fluvial process was obtained. Based on the related references, the evolution trend of the channel after the Three Gorges was finished was predicted. The 2-D mathematical model of the water flow was set up and validated using the latest data. With the model, the flow and velocity of several cases were calculated. The stability computation of the bank at the typical section under difference conditions was carried out by adopting the world widely used Geo-Slope slope stability analysis program. Finally, the synthetical evaluation on the influence of the project on the flood level, velocity, river circumstances, bank protection and flood prevention was made and the conclusion that the construction of the dock had little effect on the flood discharge was obtained.

本文介绍了平面二维水流二维模型研究进展,对河道历史演变概述,通过最新原型观测资料对河道近期主泓线、断面、洲滩、河床冲淤、码头附近冲刷坑等进行详细分析,总结近期河道演变规律,并参考有关文献,对三峡建成后河道演变趋势进行预测;建立了平面二维水流模型,并根据最新资料对模型进行率定和验证,采用模型对几种工况组合进行壅水和流速计算;采用国际上广泛应用的Geo-Slope滑坡稳定分析程序对几种工况条件下工程断典型断面岸坡进行稳定性计算;最后总结工程建设对洪水位、流速、河势、堤防及防洪抢险等方面进行综合评价,得出码头建设对行洪影响较小的结论。

A satisfactory result was obtained,the correlation coefficient of the built model based on Leave-one-out Cross-validation were 0.990 0 and 0.986 7,respectively.This model is tested by 13C NMR chemical shift of three terpenoid compounds and the excellent result with correlation coefficients R =0.977 7 was obtained.

而C原子是组成有机化合物分子骨架的重要元素,其NMR谱包含了与该分子量子化学性质直接相关的信息[2],因此,NMR谱被广泛应用于对有机化合物结构的鉴定[3-4]、动态过程和平衡及水溶液中蛋白质三维结构的研究(见2002年诺贝尔化学奖得主维特里希的成果)。

Microstructure-evolution of the silicon nitride ceramics sample during sintering process was investigated by a synchrotron radiation X-ray computed tomography technique. The projection images of the sample were obtained during the sintering process in real-time. 2-D and 3-D reconstructed images were obtained by treating the projection images of different sintering periods with filter back projection arithmetic and digital image processing methods.

利用同步辐射CT技术,在氮化硅陶瓷样品烧结过程中对其进行实时投影成像,并应用滤波反投影算法和数字图像处理技术,得到了样品在整个烧结过程中内部微结构演化的二维和三维重建图像,实现了对陶瓷固相烧结过程实时、无损的观测。

Different results were obtained by using different synergists with APP/PER system, the best results was obtained with melamine.

当体系中添加三聚氰胺时效果最好。

The obtained SWCC shows that the results obtained from the two methods can be considered as consistent.4. By using a suction-controllable oedometer for unsaturated soils, a series of wetting tests at constant net stresses and compression tests at different constant suctions are performed on compacted sand-bentonite mixtures to study the coupled hydraulic and mechanical behaviour of unsaturated expansive soil.

两种方法测到的SWCC曲线有较好的一致性。4、采用非饱和土固结仪对膨润土与砂混合物进行吸湿试验及常吸力下的压缩试验,研究了膨润土与砂混合物的水力和力学特性。

One pair of primers that amplified the gB gene of pseudorabies viruswas designed and synthesized.PCR technique detecting the DNA of PRV was established after selecting the best reaction conditions.This technique was applied to specifically amplify the 281 bp DNA fragment of the PRV strains including Fa,Fb,Bartha,BJ,GD,V2F4,S,S3,SR,Buk,Shope,Norden,Mink Ⅲ,HB,F8,F9 and F12 in cultured samples.The negative results were achieved from Vero cells,swine vesicular disease virus,hog cholera virus,Japanese encephalitis virus,porcine reproductive and respiratory syndrome virus,porcine parvovirus,foot and mouth disease virus F29 strain,O3I3 strain,T509 strain and O Ⅱ MF249 strain.The results of sequencing showed that the PCR method was of specificity.The sensitivity of PCR reached 15.8 pg of PRV Fa strain DNA.The tissue samples obtained during 1994 and 2000 were detected,and the results showed that the sensitivity of PCR was more sensitive than virus isolation and the Sandwich ELISA.The PCR was applied to detect 191 tissue samples from 31 pig farms obtained from Guangdong,Fujian,Hainan Provinces during 1999 and 2000,50 samples(26.2%)were positive and 22 pig farms(71%)were positive.

根据伪狂犬病病毒gB基因的序列,设计并合成了一对引物,以闽A株细胞培养毒为模板,筛选最佳反应条件,建立了检测PRV的PCR方法应用该方法对Fb、Bartha、BJ、GD、V2F4、S、S3、SR、Buk、Shope、Norden、MinkⅢ、HB、F8、F9、F12等毒株的细胞培养液进行基因扩增,均获得了分子量为 2 81bp的特异性目的DNA片段,而对Vero细胞与FMDV、SVDV、HCV、PRRSV、JEV、PPV等病毒进行检测,结果均为阴性,没有出现交叉反应对PRV毒株扩增的产物测序,结果序列与文献报道一致,证明PCR扩增产物和方法的特异性对 1994~ 2 0 0 0年期间送检的临床样品和保存的PRV毒种,用病毒分离、双抗体夹心ELISA和PCR等 3种方法进行检测,结果前 2种方法检测为阳性的,PCR检测均为阳性;PCR检测为阴性,前 2种方法检测也为阴性;可是,前 2种方法检测为阴性的,PCR却检测出部分阳性;经x2 检验,证明PCR检出率明显高于前 2种方法的检出率对PRV闽A株细胞毒提取物DNA进行检测,其最低检出量为 15 8pg 对 1999~ 2 0 0 0年期间广东、福建、海南等省的 31个大中型猪场送检的 191份病料进行检测。

The millimetersized tubular crystal selenium was first prepared. By studying the process of treating selenium in ethylenediamine, we proposed the mechanism of the preparation of selenides under solvothermal condition. The selenides came into being from the reaction of metal ions with Se〓, which was obtained by the amine attacking selenium. Moreover, a new precursor to prepare nanocrystalline selenides at room temperature was obtained. From this precursor, we have prepared nanocrystalline silver selenides, copper selenides, lead selenides and cadmium selenides nanorods.

首次报道了采用溶剂热处理的方法制备出厘米尺度的管状结构硒晶体;通过对硒粉在乙二胺中的溶剂热研究,初步探讨了以单质硒为硒源的溶剂热合成硒化物的反应机理应是硒受胺类的亲核进攻变成Se〓而进一步形成相应的硒化物;获得了合成硒化物纳米晶的前驱物,并在室温条件下合成了硒化银、硒化铜、硒化铅纳米晶和硒化镉纳米棒等。

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However, as the name(read-only memory)implies, CD disks cannot be written onorchanged in any way.

然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口,替代木托盘,免薰蒸,符合欧盟、北美各国对出口货物包装材料的法令要求;喷涂钢托盘适用于重载上货架之用,托盘表面根据需要制作成平板状、波纹状及间隔形式,满足不同的使用要求。

A single payment file can be uploaded from an ERP system to effect all pan-China RMB payments and overseas payments in all currencies.

付款指令文件可从您的 ERP 系统上传到我们的电子银行系统来只是国内及对海外各种币种付款。