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After the airdrop experiments of the system of the projectile and speed-down parachute, the balance velocity obtained from the optics apparatus on the ground、the balance spinning speed obtained from the gyroscope on the projectile and the image obtained from the infrared detector on the projectile are all used to simulate the six-dimension exterior trajectory of the projectile and identify the roll damping moment derivatives, and the identification can safely come to a conclusion that the absolute value of roll damping moment derivatives from the engineering calculation are on the low side.
对卷弧尾翼弹与减速伞系统进行空投试验,由地面光测系统给出平衡落速、弹上陀螺给出平衡转速、弹上红外探测器拍摄地面图像判断弹的姿态。通过六自由度弹道模拟,对弹滚转阻尼导数进行参数辨识,得到工程估算所得滚转阻尼导数绝对值偏小的结论。 5。对空投试验中出现弹姿态摆动现象,从受力分析及红外图像分析两个方面进行探讨,给出合理解释,并根据分析对弹外形进行修改,在后来的试验中收到很好的效果。
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By analyzing the molar fraction of St and MAh in the copolymers obtained from 〓C spectra, the copolymers obtained are proved to be strictly alternating structure, and sequence information obtained from DEPT experiments also verifies the copolymers with MSM sequence.
通过分析〓C NMR得到共聚物中St和MAh摩尔含量,证明共聚物具有严格交替结构,从DEPT实验中得到的结构信息表明共聚物只含有MSM序列。并且探讨了可控聚合反应的机理。
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Correctional checking formula of melt flow ratio in injection molding was obtained by introducing a correction coefficient β which reflected the complexity degree of mold cavity. The results show that, the maximum flow ratio of 486 can be obtained when injection pressure ranges from 150 MPa to 160 MPa in Archimedes spiral mold for PP, while maximum flow ratio of 419 can be obtained when injection pressure ranges from 160 MPa to 170 MPa for PE. There is a local fluctuation phenomenon for flow ratio and corresponding injection rate in square spiral mold when injection pressure of 100, 120 and 150 MPa for PP and 130, 140 MPa for PE are reached respectively,and this phenomenon is more serious for good fluidity of melt. The average flow ratio in Archimedes spiral mold is 6% larger than that in square spiral mold for PP, and 4% for PE, the average flow ratio of PP is 19% bigger than PE in Archimedes spiral mold, and 15% in square spiral mold. The influence of the cavity profiles on the melt flow ratio is more significant for good fluidity of melt.
研究结果表明:在阿基米德螺旋线模具中,PP在注射压力为150~160 MPa时取得最大流动比485,PE在注射压力为160~170 MPa时取得最大流动比419;在方形螺旋线模具中,PP在注射压力为100,120和150 MPa,PE在注射压力为130和140 MPa时流动比及所对应的注射速率出现波动,且流动性好的熔体波动更为严重;PP在阿基米德螺旋线模具中的流动比均值较其在方形螺旋线模具中大6%,而PE大4%;在阿基米德螺旋线模具中流动比均值PP比PE的流动比均值大19%,而在方形螺旋线模具中PP的流动比均值比PE的大15%;流动性好的熔体受模具型腔轮廓特征影响大。
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Methods Through the triaxial creep test, the triaxial creep curves and isochorounous stress-strain curves have been obtained, then the creep characteristics of mica-quartzose schist have been obtained by analyzing the triaxial creep curves, and the isochrounous stress-strain characteristics of mica-quartzose schist have been obtained by analyzing the isochorounous stress-strain curves. Finally, an empirical formula of creep curve is obtained by data fitting and the analysis of the relation between time and parameter of fitting formula.
通过三轴蠕变试验首先得到了云母石英片岩的蠕变曲线和应力应变等时曲线,然后对试验曲线进行分析得到云母石英片岩的蠕变特性和云母石英片岩的等时应力应变特性,最后拟合应力应变等时曲线,并分析时间和拟合公式中参数的关系,得出了蠕变经验公式。
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The different fishes which are employed in the present studies are wild-type salmon, cultured salmon of freshwater and seawater, sea perch and fat greenling. The complete CT gene sequences of salmons are obtained by PCR amplification. The partial CT sequences of sea perch and fat greenling are obtained by in vitro cloning PCR method. Alignment of obtained CT sequences with other fish CT shows that CT appears to be well conserved among the same family. And the relative in taxonomy is far away, the similarity of different fish CTs is low. On the contrary, the closer the relative in taxonomy is, the higher the similarity of different fish CTs is. The sCT is expressed in pGEX-4T-X by recombinant form . We also succeed in the research of sCT expression alone by expression PCR. In addition, sCT antiserum is obtained using GST-sCT as antigen, and the high titer is tested by double immunodiffusion. In the rat bioassay, administration of 50 μg recombinant protein evoked significant hypocalcemia at 1 h after the data are analyzed by t-test.
本文用PCR方法克隆了野生鲑鱼、养殖鲑鱼的降钙素基因,并应用体外克隆PCR的方法首次克隆出鲈鱼、六线鱼降钙素的部分基因序列,通过对克隆的降钙素序列的比较研究,结果显示同一科的鱼降钙素序列保守性较高,同时,根据降钙素的部分氨基酸序列进行了降钙素相似性的比较研究,结果显示在分类学上,分类地位较远的鱼,其降钙素相似性较低,分类地位越接近的鱼,其降钙素相似性越高;我们利用谷胱甘肽S-转移酶(Glutathions S-transferase,GST)融合表达载体pGEX-4T-X对克隆的鲑鱼降钙素基因进行了融合表达研究,应用表达PCR的方法对降钙素基因的独立表达进行了初步的研究探索,并将纯化的融合蛋白作为抗原,获得了高效价的兔抗鲑鱼降钙素免疫血清;生物活性研究表明,大肠杆菌表达的融合蛋白具有显著的降血钙作用。
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Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area;2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support;3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier;4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling;5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene PolymerizationIn this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that:1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS;2.co-mlling time had no obvious effect on the texture of support after 12 hours;3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.
XPS研究结果表明,MAO不仅仅只和乙醇作用,MAO还与MgCl_2本身有一定的作用,这是一个极为重要的发现;3、通过ICP和EDX表征,发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布;4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能,特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化,并且催化剂寿命长,表现出稳定的动力学行为,最终获得了高堆密度(大于0.35g/ml)的球形聚乙烯颗粒;5、本文选择MSPC-5为研究对象,考察了聚合反应参数对催化剂的活性及其聚合物的影响,研究发现:不同的烷基铝对催化剂具有非常重要的影响,特别足TIBA对MSPC-5的助催化活性最高,烷基铝的加入量有一个较佳值,聚合温度为80度时活性最高,H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小;、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨,制备出了一种的新型的氯化镁载体,并将该载体用于多种单活性中心催化剂的负载化研究,研究表明:1、通过BET、XRD的表征,再次证实了MAO与MgCl_2之间具有直接作用,与XPS的研究结果相一致;2、当研磨时间高于12小时时,延长研磨时间对载体的结构没有显著的影响;3、将配合物3负载于共研磨时间不同的一系列载体上,乙烯聚合结果表明,尽管共研磨时间对负载催化剂的活性具有明显的影响,但是它对聚合物的性能以及催化剂的影响不明显。
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Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area; 2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support; 3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier; 4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling; 5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene Polymerization In this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that: 1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS; 2.co-mlling time had no obvious effect on the texture of support after 12 hours; 3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.
XPS研究结果表明,MAO不仅仅只和乙醇作用,MAO还与MgCl_2本身有一定的作用,这是一个极为重要的发现; 3、通过ICP和EDX表征,发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布; 4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能,特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化,并且催化剂寿命长,表现出稳定的动力学行为,最终获得了高堆密度(大于0.35g/ml)的球形聚乙烯颗粒; 5、本文选择MSPC-5为研究对象,考察了聚合反应参数对催化剂的活性及其聚合物的影响,研究发现:不同的烷基铝对催化剂具有非常重要的影响,特别足TIBA对MSPC-5的助催化活性最高,烷基铝的加入量有一个较佳值,聚合温度为80度时活性最高,H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小;、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨,制备出了一种的新型的氯化镁载体,并将该载体用于多种单活性中心催化剂的负载化研究,研究表明: 1、通过BET、XRD的表征,再次证实了MAO与MgCl_2之间具有直接作用,与XPS的研究结果相一致; 2、当研磨时间高于12小时时,延长研磨时间对载体的结构没有显著的影响; 3、将配合物3负载于共研磨时间不同的一系列载体上,乙烯聚合结果表明,尽管共研磨时间对负载催化剂的活性具有明显的影响,但是它对聚合物的性能以及催化剂的影响不明显。
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CuS and CdS nano-particulate films were obtained with these two methods, and some interesting phenomena were observed: under the Gibbs film formed by CTAB, CuS nano-rods were obtained at the oil/water interface, and disklike aggregates of CdS nano-crystals were obtained at both the air/water and oil/water interfaces; under the Langmuir film formed by NaAOT at air/water interface, disk-like aggregates of CdS were also obtained.
利用此两种反应技术,制备了CuS和CdS颗粒膜,并研究了它们的一些光电性质;在Gibbs膜下,得到了棒状CuS纳米晶。由发现的表面活性剂形成的带状物,提出棒状CuS晶体是以带状聚集体为模板形成的;在液-液、气-液界面Gibbs膜下反应中,发现CdS纳米颗粒的盘状聚集体的形成,这是由于表面活性剂在界面上形成的二维胶束而造成的;在气-液界面上Langmuir下的反应中,也发现CdS盘状晶体的生成。
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The process comprises the subsequent steps a through e: a reacting phthalic anhydride with fluorobenzene or a derivative thereof in appropriate reaction conditions; b over reducing the product obtained in step a at the ketone moiety; c reducing the product obtained in step b with sodium dihydro-bis (2- 15 methoxyethoxy) aluminate to the corresponding alcohol ; d chlorinat ing the alcohol obtained in step c ; e inserting CO into the product obtained in step d through an appropriate Pd-containing catalytic system.
该方法包括以下步骤a~e:a使邻苯二甲酸酐与氟苯或者其衍生物在适当的反应条件中反应;b完全还原步骤a中获得的产品的酮部分;c用二氢-二(2-甲氧基乙氧基)铝酸钠将步骤b中获得的产品还原成相应的醇;d对步骤c中获得的醇进行氯化;e通过适当的含Pd的催化剂体系,将CO插入到步骤d中获得的产品中。
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The fMRI studies showed that,(1) when information obtained from self-perspective covered the information obtained from other-perspective, compared to a deductive reasoning task, the mental inference task induced increased neural activity in precuneus, decreased neural activity in ventral MPFC and enhanced functional connectivity between these two brain areas;(2) this neural activity pattern was observed in understanding human's belief, but not in understanding artificial intelligence;(3) when information obtained from other-perspective covered the information obtained from self-perspective, the mental inference task induced additional increased neural activity in dorsal MPFC and the right frontal cortex, as well as enhanced functional connectivity between these two cortical areas in addition.
EEG实验发现,额叶alpha频段神经活动在信念理解任务的早期(400-800 ms)表现为去同步化,顶叶alpha频段神经活动在信念理解任务的较晚时程(600-1000 ms)则表现为同步化。
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The absorption and distribution of chromium were studied in ryeusing nutrient culture technique and pot experiment.
采用不同浓度K2CrO4(0,0.4,0.8和1.2 mmol/L)的Hoagland营养液处理黑麦幼苗,测定铬在黑麦体内的亚细胞分布、铬化学形态及不同部位的积累。
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By analyzing theory foundation of mathematical morphology in the digital image processing, researching morphology arithmetic of the binary Image, discussing two basic forms for the least structure element: dilation and erosion.
通过分析数学形态学在图像中的理论基础,研究二值图像的形态分析算法,探讨最小结构元素的两种基本形态:膨胀和腐蚀;分析了数学形态学复杂算法的基本原理,把数学形态学的部分并行处理理念引入到家实际应用中。
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Have a good policy environment, real estate, secondary and tertiary markets can develop more rapidly and improved.
有一个良好的政策环境,房地产,二级和三级市场的发展更加迅速改善。