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The prepared PU was an elastic solid,which could dissolved in ethanol,and it exhibited strong deep purple fluorescence at the peak of 365 nm along with a shoulder at 386 nm as a thin film. Obviously,the prepared PU also was a kind of uncommon ultraviolet-emitting polymer materials.2.A novel water-soluble rod-coil block copolymer was designed and prepared successfully via the facile isocyanic acid polycondensation method using polyfluorene as rod segment and polyethylene glycol as coil segment in the main chain for the first time.
所制备的聚氨酯是一种弹性固体,可以溶解在乙醇中,同时又显示出具有半导体性质的荧光性能——最大荧光发射峰在365 nm并且在386 nm处有一个小的侧肩峰,可见它又是一种非常难得的紫外发光聚合物材料。2、首次采用了简单的异氰酸酯反应,成功地将聚芴作为刚性链段和聚乙二醇作为柔性链段,以嵌段方式连结到聚合物分子主链上,从而形成了一种新型的具有刚性链—柔性链结构的嵌段共聚物。
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The multicycle laser pulse is synthesized by a 10 fs/800 nm fundamental pulse and a 15 fs/1200 nm control pulse.
利用波长为800 nm,脉宽为10 fs的基频场和波长为1200 nm的控制场组成的双色场作用于不对称分子,发现不对称分子的高次谐波在平台区的末端呈现出光滑的超连续结构。
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The numerical simulation shows that the harmonics at the end of the plateau become continuous and form a supercontinuum with a bandwidth of about 80 eV, from which a 50 as isolated pulse in the transform limited case can be generated, when asymmetric molecules are exposed to a multicycle two-color field, which is synthesized by a 10 fs/800 nm fundamental pulse and a 15 fs/1200 nm control pulse.
通过计算机数值模拟,发现当波长为800 nm,脉宽为10 fs的基频场和波长为1200 nm的控制场组成的多光周期双色场作用于不对称分子时,不对称分子的高次谐波在平台区的末端呈现出光滑的超连续结构。超连续谱谱宽达80 eV,可以支持傅里叶极限脉宽为50 as的单个脉冲输出。
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In the UV-vis spectrum of complexes, the absorption of [CrN2O2] d -d transtion at about ~400 nm and 530~550 nm in heterometellic multinuclear complexes, which is the same to the date of some glucose tolerance factors models.
在电子光谱中,杂多核配合物中[CrN_2O_4]单元的d—d特征谱带位于~400 nm和530~550 nm处,一些葡萄糖耐量因子的模拟配合物也表现出相似的吸收。
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In this study, we investigate the effect of post-annealing on magnetization damping in sputtering deposited NiFe thin films. The film thickness is ranged from 10 nm to 100 nm. Thin films were deposited at room temperature and a subsequent post-annealing was performed in vacuum better than 10-6 torr from room temperature to 700 0C for 30 minutes.
中文摘要本研究中,我们使用改变后退火效应来观察溅镀制程镍铁薄膜(Ni84Fe16)系列的磁性阻尼行为,溅镀薄膜厚度范围为10 nm ~ 100 nm,而镍铁薄膜后退火过程在真空度约10-7 torr中进行,达到标的温度(范围由室温至700 ℃)后定温30分钟,自然冷却取出。
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The stability of GA-PBCA-NP was also studied.ResultsDue to the agglomerationg of nanoparticles with no stabilizer,it was difficult to preparate.GA-PBCA-NP produced by the two methods both had spheric and smooth outer appearance,uniform distribution,nonadherence and stability.The diameter,ebeding ratio and drug loading in GA-PBCA-NP produced by emulsification polymerization and interfacial polymerization methods were 90~600 nm and 200 nm,60.49% and 73.87%,18.15% and 22.23%,respectively.
结果未添加稳定剂的纳米球表面粘连团聚现象严重,难以成球;乳化聚合法制备的GA-PBCA-NP在透射电镜下观察表面圆整光滑,粒子之间不团聚,不黏连,粒径范围在90~600 nm,包封率为60.49%,载药量为18.15%;界面缩聚法制得的纳米粒表面圆整光滑,粒子之间不团聚,不黏连,粒径大小均匀,都在200 nm左右,包封率为73.87%,载药量为22.23%,两种方法制备的稳定性都较好。
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GA-PBCA-NP produced by the two methods both had spheric and smooth outer appearance,uniform distribution,nonadherence and stability.The diameter,ebeding ratio and drug loading in GA-PBCA-NP produced by emulsification polymerization and interfacial polymerization methods were 90~600 nm and 200 nm,60.49% and 73.87%,18.15% and 22.23%,respectively.ConclusionIt is important to add dextran 70 in preparation.
结果未添加稳定剂的纳米球表面粘连团聚现象严重,难以成球;乳化聚合法制备的GA-PBCA-NP在透射电镜下观察表面圆整光滑,粒子之间不团聚,不黏连,粒径范围在90~600 nm,包封率为60.49%,载药量为18.15%;界面缩聚法制得的纳米粒表面圆整光滑,粒子之间不团聚,不黏连,粒径大小均匀,都在200 nm左右,包封率为73.87%,载药量为22.23%,两种方法制备的稳定性都较好。
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In pH=2.0 sulfuric acid solution, 2,2′bipyridine, an almost nonluminescent compound was transformed into a highly fluorescent compound (λex=340 nm,λem=430 nm) when attacked by ·OH generated by Fenton reaction.
在酸性介质中,Fenton反应产生的羟基自由基能将几乎无荧光的2,2′-联吡啶氧化成强荧光物质,羟基化产物的最大激发和发射波长分别是340 nm和430 nm。
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While the molar ratio of WD-20 and tetraethyl orthosilicate was 0.2, the sol-fraction of the prepared nanocomposites was 6%,glass transition temperature was above 250 ℃ and the transmittance was more than 80% at the wavelength between 450 nm and 800 nm and the size of dispersed SiO2 phase was less than 100 nm.
当WD-20与四乙基原硅酸盐之比为0.2时,所制备的纳米复合材料的溶胶分数为6%、玻璃化转变温度为250 ℃以上、可见光透过率在80%以上、SiO2分散相尺寸小于100 nm。
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FeSi nanoparticles were synthesized via thermal decomposition of iron pentacarbonyl in the solution of dioctyl ether, stabilizers oleic acid and oleylamine. The TEM images showed that FeSi nanoparticles had cubic shape, but it seemed that the composition was not uniform. According to the EDS results, the Fe:Si ratio of gray-uniform nanopaiticles was almost 1:1, and blacker FeSi nanoparticles contained more Fe atoms. Although FeSi didn't have uniform structure, it still could be proved that the incorporation of Fe and Si existed in a single nanoparticle. All possible structure, lattice, binding, morphology, surface condition would be discussed. These results indicated that perhaps FeSi2 was the main structure of the new products; however, due to incompletely combination and less synthesized time, it might still contain some part of Si and Fe structure. Besides, FeSi nanoparticles preserved the optical properties from Si atoms, but the PL intensity was much lower. The maxima PL peak appeared at 388 nm with the excitation at 300 nm. Their saturation magnetization, remanent magnetization and coercivity were measured by the SQUID, exhibiting their nearly superparamagnetic behavior.
利用热裂解系统可成功将研磨矽奈米粒子及五羰铁结合,制备出铁矽奈米粒子;从穿透式显微镜照片可知其粒子呈现立方体型态,但颜色深浅及组成不均,EDS结果则显示颜色均匀之粒子铁与矽之组成大致为1:1,颜色较深之粒子则含有较高量的铁元素;尽管组成比例并不统一,但单颗粒子同时含有矽与铁两种元素,初步说明铁矽奈米粒子之形成;进行多种结构与表面分析并探讨所有可能之键结、结构及表面元素后,推测铁矽奈米粒子可能以FeSi2之结构形成,并同时包含未重组完成的矽及铁之结构;利用PL分析得知铁矽奈米粒子确实保留矽之放光特性,并在300 nm激发光源下,於波长388 nm处有一最强放光特性峰,但整体发光效益不及研磨矽奈米粒子之结果;最后,利用超导量子干涉磁化仪量测其饱和磁化量、残留磁化量、与矫顽磁力,发现磁滞现象并不明显而几乎呈超顺磁性。
- 相关中文对照歌词
- NM 156
- 推荐网络例句
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In the negative and interrogative forms, of course, this is identical to the non-emphatic forms.
。但是,在否定句或疑问句里,这种带有"do"的方法表达的效果却没有什么强调的意思。
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Go down on one's knees;kneel down
屈膝跪下。。。下跪祈祷
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Nusa lembongan : Bali's sister island, coral and sand beaches, crystal clear water, surfing.
Nusa Dua :豪华度假村,冲浪和潜水,沙滩,水晶般晶莹剔透的水,网络冲浪。