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The LUMO electron density geometry distribution of N-TPA1 is located on the cyanoacrylic group which favour electron injection,but for N-TPA2 it is mainly concentrated on the rhodanine framework,and resulting in the position of LUMO isolated from the -COOH anchoring group due to the presence of the -CH_2- group.

由于罗丹宁乙酸基团的羰基与五元环构架间隔一个亚甲基，使得LUMO电子分布距离吸附基团远，阻碍电子经由羰基注入TiO_2导带，这是N-TPA2的敏化电池效率比N-TPA1低的原因之一。

Ve schizophrenic inpatients will be enrolled into the 6-week, randomized, double-blind trial of sarcosine monotherapy (1000~3000 mg/day, N=75) vs. risperidone (2~6 mg/d, N=75). We will measure clinical efficacy and side effects biweekly during the treatment. At the beginning and the end of the trial, we will also measure cognitive function (e.g. intellect, attention, memory, executive function), serum amino acids, expressions of mRNA (by realtime quantitative RT-PCR) and protein of NMDA-related genes (such as SHMT2, AMT, PSAT1, ASCT1, and serine racemase) in peripheral blood lymphocytes.

第一部份将收案150位未曾治疗之精神分裂症住院患者，以双盲方式随机给予六周sarcosine (1000-3000 mg/day，N=75)或risperidone (2-6 mg/day，N=75)治疗，我们将每两周评估临床疗效与安全性，并在研究开始及结束时，评量认知功能(智能、注意力、记忆力、执行功能)并测定血清中glycine或D-serine浓度以及SHMT2、AMT、PSAT1、ASCT1、serine racemase等基因於周边淋巴球之mRNA (以realtime RT-PCR测定)与蛋白质表现量。

Methods Forty patients with hepatobiliary and pancreatic diseases undergoing biliojejunostomy or cystojejunostomy were randomly divided into seromuscular layer anastomosis group (n=20) and two-layer anastomosis group (n=20) before operation, which received Roux-en-Y end-to-side jejunal seromuscular layer anastomosis and two-layer anastomosis, respectively.

行胆管空肠Roux-en-Y吻合的患者随机分成2组：浆肌层吻合组(n=20)和二层吻合组(n=20)，浆肌层吻合组行Roux-en-Y袢处空肠－空肠浆肌层吻合，二层吻合组行Roux-en-Y袢处空肠－空肠二层吻合。

The results show that the zirconium sol has good spinnability when n: n= 1:3, reaction time is 6h and aging temperature is 15℃. The ZrO_2precursor fibers are made from hydrous zirconia chelated by acetylacetone. The sintercd fibers arecomposed of metastable tetragonal phase and sized about 15μm in diameter. Moreover, there aremany pores inside the fibers, but no cracks.4. ZrO_2/PVP hybrid fibers were prepared by blending the spinnable zirconium sol and 10 wt%PVP solution.

结果表明，当n(ZrOCl_2·8H_2O)：n(H_2O_2)=1：3，反应时间6h，陈化温度15℃时可得纺丝性能良好的锆溶胶，ZrO_2前驱体连续纤维的组成主要为经乙酰丙酮配位的ZrO_2水合物，热处理后的ZrO_2纤维的相结构为亚稳四方相，纤维的直径为15μm左右，纤维中存在大量的纳米级气孔，但无明显裂纹。4。

MCM-41, HMS, and MSU mesoporous silica molecular sieves were prepared via S〓I〓, S〓X〓I〓, S〓I〓, and N〓I〓 assembly pathway, in which cetylpyridium bromide, tetredecylamine, and polyoxyethylene (10) stearyl ether was used as the template, respectively. The mesostructures were characterized and confirmed by XRD, N〓 adsorption/desorption, TG, and high resolution TEM. The difference and relationship between these mesophases were also investigated.

分别以溴代十六烷基吡啶、十四胺和十八烷基聚氧乙烯基醚为模板剂，通过S〓I〓、S〓X〓I〓、S〓I〓和N〓I〓&超分子组装模式&合成了具有MCM-41、HMS和MSU结构的介孔SiO〓分子筛，用XRD、N〓吸附/脱附、TG和高分辩TEM等方法对它们的骨架和孔道结构进行了表征，并系统地比较了这几种介孔结构之间的区别与联系

Titanium incorporated mesoporous molecular sieves Ti-MCM-41, Ti-HMS, and Ti-MSU were synthesized through S〓I〓, S〓I〓, and N〓I〓 pathways using cetylpyridium bromide, tetredecylamine, and polyoxyethylene (10) stearyl ether as the structure-directing agents, respectively. The framework structure and the titanium coordination environment of these materials were characterized by XRD, N〓 adsorption/desorption, TG, TEM, FT-1R, DR UV-Vis, and ICP-AES. It was confirmed that the titanium was highly dispersed in the silica-based framework positions, and all samples were free of extra framework titanium impurities. The catalytic performance of these titanium containing mesoporous materials was investigated in the oxidation of styrene with aqueous H〓O〓 as the oxidant.

以TEOS和TBOT为硅源和钛源，分别以溴代十六烷基吡啶、十四胺和十八烷基聚氧乙烯基醚为模板剂，通过S〓I〓、S〓I〓和N〓I〓方式合成了含钛的介孔分子筛Ti-MCM-41、Ti-HMS和Ti-MSU，用XRD、N〓吸附/脱附、TEM、FT-IR、DR UV-Vis和ICP-AES等方法对它们的骨架结构、孔道结构以及钛原子的存在方式等进行了系统表征，结果表明钛原子以高分散的形式存在于以SiO〓为基本单元的介孔分子筛的骨架结构中，制备过程中未形成聚集态的骨架外金属氧化物物种。

The stereochemical structures of two new compounds, 5-(3-chlorophenyl)-2-furfur-aldehyde-N-4-methylphenyloxyacetylhydrazone and 5-(3-chlorophenyl)-2-furfuraldehyde-N-4-nitrophenyloxyacetylhydrazone, were determined by DPFGSE-NOE experiments performed in DMSO-d\-6 at 25 ℃ and variable-temperature ~1H NMR The ~1H chemical shifts of the compounds were completely assigned at 25 ℃ and 90

利用变温实验和DPFGSE NOE实验，确定了 5 (3 氯苯基) 2 呋喃甲醛 N 4 甲基苯氧乙酰腙和5 (3 氯苯基) 2 呋喃甲醛 N 4 硝基苯氧乙酰腙两个新化合物25 ℃时在二甲基亚砜中的空间构型，并对这两个新化合物在 25 ℃和 90 ℃时的质子的化学位移进行了全归属。

Under the optimum conditions of n: n=40, mass percentage of ZrO2 18%, temperature 400℃, m m=0.02 and reaction time 0.5 h, the conversion was 91.2% and the yield of liquid products was 83.6%. Compared with the results obtained by thermal pyrolysis and catalytic pyrolysis on HZSM-5, ZrO2/Ti-MCM-41 was of better catalytic activity and higher yield of liquid products, and was especially suitable for the pyrolysis of sterically hindered polymers such as PP.

结果表明，n：n=40，ZrO2负载质量分数为18%的ZrO2/Ti-MCM-41，在反应温度400℃，m(ZrO2/Ti-MCM-41)：m=0.02，反应时间30min的条件下，PP的转化率可达91.2%，液体产物的收率为83.6%，该结果优于热裂解及传统的HZSM-5小孔分子筛催化剂的催化裂解结果。

A new organic dye ,trans,trans-4-｛4-[4-(N,N-diphenylamino)styryl]styryl｝N-methylpyridinium iodide,has been synthesized and structurally investigated.

合成了一种新型有机染料，反式，反式-4-{4-[4-苯乙烯基]苯乙烯基}-N-甲基吡啶碘盐。

The electroluminescence devices (ITO/NPB/emitting layer /BCP/Mg : Ag) based on 1, 4-bis (4-N, N-methylamino styryl) naphthalene as emitting layer have been designed by the energy band matching principle.

以自制的&D-π-D&对称型有机绿色发光分子1，4-双（4'-N，N-二甲基氨基苯乙烯基）萘为发光层，在结构为ITO/NPB/BMABN/BCP/Mg： Ag的器件中，研究了空穴阻挡层厚度对器件发光性能的影响。

In the negative and interrogative forms, of course, this is identical to the non-emphatic forms.

。但是，在否定句或疑问句里，这种带有"do"的方法表达的效果却没有什么强调的意思。

Go down on one's knees;kneel down

屈膝跪下。。。下跪祈祷