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In this paper, the host-guest relationship between a general cucurbit [n=7] uril (Q[7]) or a new ellipsoid-host-symmetric tetramethyl-cucurbituril (TMeQ[6]) with hydrochloride salts of 4,4'-dipyridyl (44) or N,N'-dimethyl-4,4'-dipyridyl(dm44) was examined for confirming the interaction between cucurbituril (Q[6]) and these guests.

以七元瓜环(Q[7])和新型椭圆型改性瓜环―对称四甲基取代六元瓜环(TMeQ[6])为主体，4，4'-联吡啶的盐酸盐(44)以及N，N'-二甲基4，4'-联吡啶的盐酸盐(dm44)为客体的主客体相互作用进行了考察。

Methods The SpaA was purified by electroelution from NaOH-extracted antigen of Erysipelothrix rhusiopathiae strain C43311. The rSpaA-N was expressed in E. coli BL21 as a soluble protein by IPTG inducing,and purified with GST affinity chromatography. Mice of each group were subcutaneously immunized three times with 50μg or 100 μg of native SpaA, rSpaA-N or NaOH-extracted antigen with in complete or incomplete Freund adjuvant at 2-week intervals.

将猪丹毒丝菌C43311株SpaA-N以可溶形式表达在大肠杆菌BL21中，用GST Bind Resin纯化试剂盒纯化rSpaA-N，采用电洗脱法从猪丹毒丝菌C43311株NaOH提取抗原中纯化天然SpaA，将rSpaA-N、天然SpaA和NaOH提取抗原制成亚单位疫苗，同时设GST及生理盐水对照组，间隔2周分3次皮下免疫小鼠，第3次免疫后2周用100LD50猪丹毒丝菌C43065株进行腹腔攻毒，采用间接ELISA方法检测免疫组小鼠血清的抗体动态变化。

The HPV positivity amongst the group of women with no cervical abnormality was 43%, while that in women with cervical dysplasia and cervical cancer was 81.2% PCR products from 89 HPV positive cases were genotyped by LiPA, of which 49 cases were single HPV infected concerning 11 different HPV types and the commonest type was HPV-16, occurring in 25(51%) of all single HPV infected cases. The other 40 specimens contained multiple HPV types comprising 16 different HPV types. Although double infections(n=25) prevailed, triple(n=9),quadruple(n=3) and quintuple(n=3) infections were also found. PCR products of four HPV positive cases failed to be classified by LiPA. Sequencing analysis revealed that these 4 cases were HPV-66 which was not included in LiPA probes. Follow-up data of 12 cases confirmed the HPV genotyping results. Conclusion The LiPA for HPV genotyping is easy to perform.

结果 155例妇女子宫颈刮片中HPV DNA检出率为60%，其中在宫颈细胞学检查正常或仅有炎症病变的妇女中HPV DNA阳性率为43%，而在宫颈细胞增生不良或宫颈细胞癌的妇女其阳性率为81.2%。93例HPV阳性的标本中，89例利用LiPA成功地作出了基因分型，其中单独一型HPV感染为49例，涉及11种不同基因型HPV，最常见的型别为HPV 16，占单独感染的51%(25/49)；另40例为不同型别HPV重叠感染，涉及所有16种HPV基因型别，二重感染占主导地位(n=25)，同时也检测出其它多重感染。4例HPV阳性的标本应用LiPA未能作出基因分型，DNA序列分析显示这4例为HPV 66感染，此型别不包括在LiPA所标记的探针内。12例随诊资料显示了LiPA的物异性及高度的重复性。

METHODS: Dogs (n=16) were randomly divided into 2 groups: the control (n=7) and the CHF group (n=9) induced by rapid right ventricular pacing at 240 pulsemin^(-1) for 4 to 5 weeks. The electrophysiologic parameters were evaluated by the technique of standard electric stimulation and monophasic action potential recording.

16只犬随机分为正常对照组(n=7)和CHF组(n=9)，应用右心室快速起搏240 pulsemin^(-1 4-5周制作CHF犬模型，应用心脏电刺激和单相动作电位记录技术测定心室生理指标。

The results indicate that the high efficiency and stable performance of shortcut nitrogen removal in MBR-PBBR process is attributed to the predominance of functional microbiology Nitrosomonas eutropha during the period of operation,which occupies over 54%of total bacteria.However,large amount of organic carbon can destroy the predominance of N.eutropha,whose proportion decreased to 31%at TOC/N=0.3.The diversity of microbial community in MBR increases along with operating time.

结果发现，生物强化的MBR-PBBR工艺能实现相对稳定和高效的捷径生物脱氮，主要归功于MBR中的功能微生物Nitrosomonas eutropha在运行过程中始终保持优势地位，占全菌数的比例大于54%；然而，当外加有机碳源较高(TOC/N≥0.2)时，可动摇氨氧化菌的优势地位，N.europha占全菌数的比例在TOC/N=0.3时下降至31%。

Directed under plate tectonics theories, author applied the relationship between orogenyy belt and basin, analyzation of proto-type basin restoration of Paleo-structures etc to systematically draw the Paleo-structural maps and Paleo-sedimental photographical maps on Z, O, S, D, C, P, T, J, K, E, N〓j, N1〓k, N〓k etc in Tarim basin.

以板块构造理论为指导，运用造山带与盆地、原型盆地分析、古构造分析等分析方法，系统编制了Z、O、S、D、C、P、T、J、K、E、N〓j、N〓K，N〓K等盆地及周缘古构造岩相图，全面系统地研究和恢复了塔里木大型叠合复合盆地构造演化历史，并将塔里木盆地构造演化史划分为7个构造演化阶段。

Eight porphyrin compounds, meso-5, 10, 15, 20-Tetra [4-aminophenyl] porphine (TAPPH〓, 1), meso-5, 10, 15, 20-Tetra [4-(N-pyrrolidinyl) phenyl] porphine (TBPPH〓, 2), meso-5, 10, 15, 20-Tetra [4-(4'-ethylpiperazinyl) phenyl] porphine (TEPPH〓, 3), meso-5, 10, 15, 20-Tetra [4-(4'-butylpiperazinyl) phenyl] porphine (TUPPH〓, 4), meso-5, 10, 15, 20-Tetra [4-(4'-heptylpiperazinyl) phenyl] porphine (TEPPH〓, 5), 5- [4-(4'-ethylpiperazinyl) phenyl] -10, 15, 20-triphenylporphine (MEPPH〓, 6), 5- [4-(4'-buthylpiperazinyl) phenyl] -10, 15, 20-triphenylporphine (MUPPH〓, 7) and N, N'-di (meso-5, 10, 15, 20-tetraphenylporphinato) piperazine (DiPPH〓, 8) have been designed and synthesized. These porphyrins are never reported except TAPPH〓.

设计并合成了8种卟啉化合物，分别为meso-5，10，15，20-四（4-氨基苯基）卟啉（TAPPH〓，1），meso-5，10，15，20-四卟啉（TBPPH〓，2），meso-5，10，15，20-四[4-（4'-乙基哌嗪基）苯基]卟啉（TEPPH〓，3），meso-5，10，15，20-四[4-（4'-丁基哌嗪基）苯基]卟啉（TUPPH〓，4），meso-5，10，15，20-四[4-（4'-庚基哌嗪基）苯基]卟啉（THPPH〓，5），5，10，15-三苯基-20-[4-（4'-乙基哌嗪基）苯基]卟啉（MEPPH〓，6），5，10，15-三苯基-20-[4-（4'-丁基哌嗪基）苯基]卟啉（MUPPH〓，7）和N，N'-二（meso-5，10，15，20-四苯基卟啉基）哌嗪（DiPPH〓，8）。

An interview guide, entitled "Maternal Perception of the Onset of Lactation", was also used to obtain milk secretion data. Results found a mean onset of lactation of 78.2±18.7 hours (range=42 to 121 hours). The prevalence of delayed lactation onset was 43.6%(n=58). Slighly over half of participants (56.9%, n=33) were primiparous. Parity, total second stage of labor duration, duration of second labor stage beyond one hour, and perinea wound pain were the most significant predictors of delayed lactation onset.

研究结果发现：(1)首次泌乳时间的平均值为78.2±18.7小时（范围42至121小时）；(2)产妇自觉延迟泌乳的发生机率为43.6%(n=58)，其中初产妇占56.9%(n=33)，经产妇占43.1%(n=25)；(3)产次、第二产程时间、第二产程时间大於一小时、第一到第三天会阴伤口疼痛分数，是延迟首次泌乳时间的重要预测因子。

Methods The rat's models of the SAP was established with 5% sodium taurocholate injected retrogradely into the biliary-pancreatic duct. Eighty SD rats were randomly divided into 4 groups (n=20 in each group), including sham group, SAP group, treatment group Ⅰ and treatment group Ⅱ.

采用逆行性胰胆管注射5%牛磺胆酸钠制备SAP模型。80只SD大鼠随机分为假手术组(n=20)、SAP组(n=20)、治疗Ⅰ组(乌司他定治疗组，n=20)、治疗Ⅱ组(TNF-α抑制剂联合乌司他定治疗组，n=20)。

2Soil column leachate experiment shows, soil texture and soil section form are the main factors affecting the nitrate leaching; in soil organic fertilizer produce a nitrate leaching process, during five-month experiment, nitrate content has be increasing in leakage solution, organic fertilizer applying decrease the pH and increase the electric conduction of leakage solution, there is positive action between nitrate content in leakage solution and electric conduction, which shows that nitrate-N accumulation during organic fertilizer applying is one of the main factors for soil salification; for decrease the leaching of the nitrate-N in soil, in sandy moisture soil the best amount of organic fertilizer should be 7.5～ 15 t·hm~(-2), in Loamy moisture

在小麦-玉米轮作体系上投入化肥氮300kg·hm~(-2)N和有机肥22.3t·hm~(-2)折N261.2kg·hm~(-2，能使农田氮素收支达到平衡，在兼顾环境效益的基础上获得了较高的产量效益。并通过肥料效应函数和硝态氮累积效应函数进一步预测最佳施肥组合，即化肥氮施用量为N226.5kg·hm~(-2)，有机肥用量为39.9t·hm~(-2)折N466.8kg·hm~(-2，其中小麦季施化肥氮105.85kg·hm~(-2)N、有机肥30t·hm~(-2)折N351kg·hm~(-2，玉米季施化肥氮120kg·hm~(-2)N，有机肥9.9t·hm~(-2)折N115.8kg·hm~(-2。同时，磷素平衡分析表明，在施用有机肥的基础之上，化学磷肥的施用量应适量的减少或不施。

Do you know, i need you to come back

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。