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Ethanol was substituted for N,N-dimethyl sulfoxide as solvent of colouring agent pyrazolone and better results were obtained.

改用无水乙醇代替N,N-二甲基甲酰胺作为显色剂吡唑啉酮的溶剂,效果更好。

Both styrene conversion and epoxide selectivity can be obviously improved when a solution of N,N-dimethylformamide and dimethyl sulfoxide with an appropriate proportion is used.

使用适当比例的N,N-二甲基甲酰胺和二甲亚砜的混合溶剂能够显著提高苯乙烯的转化率和环氧化物的选择性。

Measure character: Frequency limits: CH1:dResolution of C ~ 225MHz frequency: 10 / second time-interval resolution : N/A measures speed: Can amount to 200 times measure / the second mixes in limits of the voltage on GPIB sensitivity : DC ~ 100MHz: 200MHz of ~ of 5Vac+dc 100MHz of 20mVrms ~±: 225MHz of ~ of 5Vac+dc 200MHz of 30mVrms ~±: Input of 5Vac+dc of 40mVrms ~± adjusts:(CH1 chooses) impedance, coupling: 1M Ω or 50 Ω, ac or Dc are low connect filter: 100kHz, but switch attenuation:× 1 or reference of × 10 exterior time base inputs: 1, 5, 10MHz sparks: CH1, to rising / drop the edge sparks, the percentage that uses signal n or absolutely voltage install n, setting sensitivity mixes to low, medium or tall gate start: Automatic, the hand is moved (setting gate time or resolution digit); Exterior, defer interface: Standard GP-IB(IEEE 488.1 and 488.2), take; of SCPI compatible language to say RS-232 power source only: 10 % of 100-120VAC ±, 50, 60 or 10 % of 400Hz ± 10 % of 220-240VAC ±, 50 or 10 % of 60Hz ± are suttle: 3kg dimension: 348.3mm of × of 212.6 × 88.5H

测量特征:频率规模:CH1:dc~225MHz 频率分辨率:10位/秒时候距离分辨率:N/A 测量速度:可达200次测量/秒在GPIB上电压规模和灵敏度: DC~100MHz: 20mVrms~±5Vac+dc 100MHz~200MHz:30mVrms~±5Vac+dc 200MHz~225MHz:40mVrms~±5Vac+dc 输入调节:(CH1选择)阻抗,耦合: 1MΩ或50Ω,ac或dc 低通滤波器: 100kHz,可切换衰减:×1或×10 外部时基参考输入: 1,5,10MHz 触发: CH1,对回升/回升沿触发,用信号电平的百分数或相对电压设置电平,设置灵敏度至低、中或高闸门和启动:主动,手动(设置闸门时候或分辨率位数);外部,延迟接口:尺度GP-IB(IEEE 488.1和488.2),带SCPI兼容说话;只讲RS-232 电源:100-120VAC±10%,50,60或400Hz±10% 220-240VAC±10%,50或60Hz±10%净重:3kg 尺寸:212.6×88.5×348.3mm

The properties of the basis functions, such as the weighting property, positivity, symmetry and endpoints' properties,are similar with those of the n degree Bernstein basis functions,and the generated curves are similar with the n degree Bézier curves.

基函数的权性、非负性、对称性、端点性质等均与n次Bernstein基函数类似;生成曲线也具有与n次Bézier曲线类似的几何性质。

It is also pointed out that an n-mode boson coupled quadratic Hamiltonian can be diagonalized by a "negative unitary" matrix which is an element of complex symplectic group SP(2n,c),and an n-mode fermion coupled quadratic Hamiltonian can be diagonalized by a unitary matrix which is an element of complex fermion group F(2n,c).

并且指出,对于n模玻色子耦合二次型哈密顿量,通过一个负幺正矩阵它是复辛群SP(2n,c的元素可以把它对角化;对n模费米子耦合二次型哈密顿量,通过一个幺正矩阵它是复费米群F(2n,c的元素可以把它对角化。

Based on an overall analysis of the output power performance of GaAs MESFET and its linear distortion, the optimal design of tailless double-peak n~+n carrier distribution is presented.

经过对GaAs MESFET输出功率及其线性失真的综合分析,提出了无拖尾双峰n~+n载流子浓度分布的最佳设计。

Two above methods are generalized to tensor product Bézier surfaces and triangular Bézier surfaces, we give two approaches of degree reduction for tensor product Bézier surfaces, each of which reduces a given degree n×m tensor product Bézier surface to a n〓×m〓 one, and two methods of degree reduction for triangular Bézier surfaces, which reduce a given degree n triangular Bézier surface to a degree m one. The explicit formulas of control points for reduced tensor product and triangular Bézier surfaces are obtained respectively.

张量积Bézier曲面的两种降阶方法均可把n×m阶张量积Bézier曲面一次降阶为n〓×m〓阶张量积Bézier曲面;三角Bézier曲面的两种降阶方法均可把n阶三角Bézier曲面一次降阶为m阶三角Bézier曲面,并给出降阶张量积Bézier曲面和降阶三角Bézier曲面控制顶点的显示表示式。

In the process of laboratory study, oxycodone was prepared by oxidating thebaine at 6,14-position under oxydol, hydrodeoxidizing 7,8-position double bond and 14-position ether under palladium catalyst. Furthermore, N-methyl of oxycodone was isolated byα-chloro-ethyl chloroformate under anhydrous condition and protection of 14-position hydroxyl to obtain noroxycodone, which was further converted into methylnaltrexone by N-alkylation in presence of cyclopropyl bromomethane, then by isolating 3-position methyl of methylnaltrexone under boron tribromide, becoming hydrochloride to prepare target compound, natrexone hydrochloride.

实验室工艺方面,本文首先用双氧水氧化蒂巴因的6-位和14-位、在钯炭催化下加氢还原7-8位双键和14-位醚合成羟考酮,然后提出并优化了在无水和14-位保护的情况下,用氯甲酸-α-氯乙酯脱去羟考酮的N-位甲基合成去甲羟考酮,再用环丙甲基溴将去甲羟考酮的N-位烷基化合成甲基纳曲酮,最后采用三溴化硼脱去甲基纳曲酮的3-位甲基和成盐酸盐合成盐酸纳曲酮。

Eight novel N,N′-naphthalene acyl substituted aromatic acylamino thiocarbamide s(Ⅱ1~Ⅱ8) were synthesized from aryl acylhydrazine and α-naphthalene acyl isothiocyanate, which was obtained by the reaction of potassium thiocyanate with α-naphthalene acyl chloride obtained from 2-naphthylacetic acid and thionyl chloride in anhydrous benzene.

通过α-萘乙酸和SOCl2在无水苯中反应制得α-萘乙酰氯,与硫氰酸钾反应生成α-萘乙酰基异硫氰酸酯,再与芳基酰肼进行加成反应,合成8种新型N,N′-萘乙酰基取代芳乙酰胺基硫脲类化合物(Ⅱ1~Ⅱ8)。

Naphthalene acetyl chloride was prepared firstly by the reaction between α-naphthylacetic acid and SOCl2 in anhydrous benzene,then reacted with potassium thiocyanate to obtain α-naphthalene acetyl isosulfocyanate,as taking an addition reaction with p-chloro benzoyl hydrazine the novel compound N-naphthalene acetyl-N'-p-chloro benzoylamino thiocarbamide was finally synthesized.

通过α-萘乙酸和SOC l2在无水苯中反应制得α-萘乙酰氯,然后与硫氰酸钾反应生成α-萘乙酰基异硫氰酸酯,再与对氯苯甲酰肼进行加成反应,生成新型化合物N-萘乙酰基-N'-对氯苯甲酰氨基硫脲。

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I didn't watch TV last night, because it .

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Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

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