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It,s allelchemicals were isolated through extraction, thin-layer chromatography, and column chromatograpathy. After the white clover was infused in ethanol and evaporation, the leavings was dissolved by water. The aqueous extract was extracted by petroleum,chloroform, ethyl acetate and n-Butanol successively, and the bioassay showed that the chloroform phase has obvious inhibitory effect, the inhibitory rate was 44.32%,88.08% on Abutilon theophrasti M., seedling length and root length, 82.08%,92.16% on Echinochloa crusgalli L., seedling length and root length, and the Amaranthus retroflexux L., germination rate is 0, the secondly was ethyl acetate phase.

运用萃取、薄层层析、柱层析等方法对白三叶草地上部分的化感物质进行初步分离,结果表明,白三叶草经乙醇浸提旋转蒸发后用蒸馏水溶解,依次用石油醚、氯仿、乙酸乙酯、正丁醇萃取,生物测定表明氯仿组分对杂草的抑制作用最强,对苘麻芽长和根长抑制率分别为44.32%、88.08%,对稗草芽长和根长的抑制率分别为82.08%、92.16%,反枝苋的发芽率为0;其次是乙酸乙酯相。

Methods: Based on national standard, detected n-hexane, benzene, toluene, dimethylbenzene, ethyl acetate, butyl acetate and butanone in 450 factories.

根据中华人民共和国国家标准,对昆山市的450家接触正己烷、苯、甲苯、二甲苯、乙酸乙酯、乙酸丁酯、丁酮7种有机物的企业车间空气进行采样检测。

Reductive conversion of geraniol to citronellol is adopted as a model reaction, and several factors in the reaction are discussed using gas chromatography method. The influence of n-hexane and butyl acetate, as organic solvents, on biocompatibility was studied; the influence of methanol, ethanol, glycol, n-butanol and 1-hexanol, as energy substance, on the transformation efficiency was compared, respectively; the catalysis capabilities of Baker's yeast, XST-KO yeast, LP yeast, alcohol yeast, dry yeast, Saccharomyces cerevisiae, Angel yeast and Meishan yeast were discussed. It has been proved that biocompatibility of n-hexane are much better than that of butyl acetate, and the hexane has been demonstrated the most effective in terms of the influence on biotransformation, Baker's yeast has shown the highest tranformation efficiency among the eight yeast strains.

以香叶醇转化为香茅醇作为模型反应,通过气相色谱法进行定性和定量分析研究了影响该有机相生物转化反应的几个基本因素,考察了两种有机溶剂正己烷和乙酸丁酯对生物相容性的影响,选用甲醇、乙醇、乙二醇、正丁醇和l-己醇分别作为能量物质进行实验,比较其对转化的影响并探讨了Baker's酵母、XST-KO酵母、LP酵母、酒精酵母、假丝酵母、干酵母、安琪酵母和梅山酵母八种不同酵母作为生物催化剂对模型反应的催化能力,结果表明,正己烷作为有机溶剂,其生物相容性明显好于乙酸丁酯,更加有利于该生物转化反应进行;乙二醇作为能量物质,该模型反应转化率最高;而 Baker's酵母作为生物催化剂,对该模型反应的催化能力最强,最适合作为该模型反应的催化剂。

Then, N-for-aspartame was obtained from the reaction of 3-formyl-4-carboxymethyl-1,3-oxazolidine-5-one and L-phenylalanine methylester hydrochloric acid under sodium acetate anhydrous in ethyl acetate, and the target product was prepared after removing formyl in the mixture system of hydrochloric acid, methanol and water, the yield of aspartame reaches 89.2%.

最后,用3-甲酰-4-羰基口恶唑烷-5-酮乙酸与L-苯丙氨酸甲酯盐酸盐在溶剂中进行接肽反应,然后在甲醇/盐酸混合体系中进行脱甲酰保护基,从而得到最终目标产物,产率为89.2%。

And Cucumis sativus L. were tested by bioassay-guided separation. The extracts from P. tomentosa flower with ethanol were extracted with petroleum ether, ethyl acetate and n-butanol. The inhibition rate of the ethyl acetate extract to growth of the 3 kinds of plant radicel were 99.89%, 63.53% and 32.74% respectively at 0.5 mg/mL concentration, and that of petroleum ether were 76.30%, 56.17% and 23.36%.

绒叶泡桐Paulownia tomentosa花乙醇提取物依次用石油醚、乙酸乙酯、正丁醇和水萃取后进行活性测定,结果表明,石油醚萃取物在浓度为0.5mg/mL时,对反枝苋、生菜和黄瓜种子胚根生长的抑制率分别为76.30%、56.17%和23.36%;乙酸乙酯萃取物在浓度为0.5mg/mL时,对反枝苋、生菜和黄瓜种子胚根生长的抑制率分别为99.89%、63.53%和32.74%。

The extracting ability of several organic solvents such as ethyl acetate, butyl acetate, glycerol triacetate, iso-amy lacetate, and n-butanol, was compared, and it was found that ethyl acetate was a good kind of organic solvent.

比较了几种不同的有机溶剂:正丁醇、乙酸丁酯、乙酸乙酯、三乙酸甘油酯、乙酸异戊酯等的萃取能力,发现乙酸乙酯是一种理想的提取溶剂。

Our company is mainly engaged in chemical raw materials trading, the company mainly engaged in: toluene, xylene, mesitylene, durene, 6 # 120 # 200 # solvent, ethyl acetate, butyl acetate, acetone, butanone, cyclohexanone, isophorone, MIBK, isopropyl alcohol, isobutyl alcohol, butanol, mixed alcohols, methanol, ethanol, ethylene glycol, diethylene glycol, diacetone alcohol, Anti-White Water, CAC, n-hexane, dichloromethane, trichloro-B, DMF, 5 # 10 # 15 # white mineral oil, lubricating oil, sewing machine oil, as well as high-pressure polyethylene, linear polyethylene, low-pressure polyethylene, polypropylene, rubber and other chemical raw materials.

我公司主要从事化工原料贸易,公司主要经营:甲苯、二甲苯、三甲苯、四甲苯、6# 120# 200#溶剂、醋酸乙酯、醋酸丁酯、丙酮、丁酮、环已酮、异佛尔酮、MIBK、异丙醇、异丁醇、正丁醇、混丙醇、甲醇、乙醇、乙二醇、二甘醇、二丙酮醇、防白水、CAC、正已烷、二氯甲烷、三氯乙、DMF、5# 10# 15#白矿油、润滑油、针车油以及高压聚乙烯、线性聚乙烯、低压聚乙烯、聚丙烯、橡胶等各种化工原料。

A random copolymer of poly(vinyl acetate-co-isopropenyl acetate) with number-average molecular weight of 9600 and relatively narrow molecular weight distribution (MWD, M w/ M n=2.03)was prepared by free radical copolymerization of vinyl acetate with isopropenyl acetate using AIBN as initiator.

通过自由基共聚合方法,以AIBN为引发剂引发醋酸乙烯酯和醋酸异丙烯酯共聚,得到两者的无规共聚物聚。

Results The mixing, loading and storing processes of the construction, might generate lots of occupational hazards, including toluene, dimethylbenzene, trimethylbenzene, isopropanol, butyl alcohol, propanol, methyl methacrylate, butyl acetate, methyl isobutyl ketone, methyl ethyl ketone, acetic ether, nitro-cotton, n-hexane, n-heptane, carbinol, ethanol, ethyl propionate, diisobutyl ketone, glycol ether, isoamyl acetate, 2,4-toluene diisocyanate, isophorone, noise, power frequency electric fields.

结果 该项目在混兑生产和装卸、仓储过程中,可能产生的职业病危害因素主要有甲苯、二甲苯、三甲苯、异丙醇、丁醇、丙醇、甲基丙烯酸甲酯、乙酸丁酯、甲基异丁基甲酮、丁酮、乙酸乙酯、硝化棉、正己烷、正庚烷、甲醇、乙醇、乙酸丙酯、二异丁基甲酮、乙二醇乙醚、乙酸异戊酯、2,4甲苯二异氰酸酯、异佛尔酮、噪声、工频电场。

The concents of testosterone and NO of the mouses gavaged with high dosages of Chinese chive extractiong were not significantly more than that of giving middle dosages.This indicated that Chinese chives might be more safe than traditional chinese herbals of sexual improvement function.2、The screening of sexual improvement function chemical substances of Chinese chivesThe crude extract was leached to four phases by petroleum ether, ethyl acetate,n-butanol and water.By doing animal tests to detect the contents of testosterone and NO in serum of mices,the result was showed that the extracts of petroleum ether and n-butanol have sexual improvement function,especial the n-butanol phase.

从小鼠灌喂不同剂量的韭菜提取液试验结果来(来源:ABCa539a5论文网www.abclunwen.com)看,灌胃高剂量的小鼠的睾酮含量和NO含量相对于中剂量来说并不上升,而是保持稳定,因为睾酮含量和NO含量过度上升可能会带来付作用,所以由此可以说明其食用安全性高,副作用小。2、韭菜改善性功能物质的筛选将韭菜粗提物依次通过不同溶剂萃取,分成石油醚、乙酸乙酯、正丁醇和水四个萃取相,通过小鼠灌胃的动物试验,以小鼠血液NO含量和睾酮含量为指标,发现正丁醇和石油醚萃取相中的物质有改善性功能的效果,尤其是正丁醇相效果非常显著。

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