查询词典 monobasic

Anhui Institute for Drug Control, Hefei 230051ABSTRACT Objective To establish an HPLC method for the determination of azithromycin powder.Method The chromatographic conditions were as followed: C8 column, 0.045 mol/L ammonium phosphate monobasic solution∶acetonitrile (2∶1)(adjusted to pH7.35 with triethylamine) as mobile phase, temperature: 40℃, the flow rate: 1.0 ml/min, detection wavelength: 210nm.

阿奇霉素为氮杂内酯类抗生素，日抗基和《中国药典》2005年版［1］均采用微生物检定法测定其含量，《欧洲药典》4.6版和USP26版中均采用HPLC法，专属性较强，试验周期短，但均使用的是聚合物极性柱，《欧洲药典》柱温为70℃，USP采用电化学检测器，其采用的设备在我国药检部门尚未普及［2］。

Methods The HPLC System consisted of Agilent Plus C18 column, acetonitrile-buffer(0.01mol · L-1 monobasic potassium phosphate, contained 0.1% triethyl amine, pH 6.8 )(70∶30) as mobile phase with detection wavelength 282nm.

采用 Agilent Plus C18柱；以0.01mol · L-1磷酸二氢钾溶液（含0.1%三乙胺，用磷酸调节 pH 值至6.8）-乙腈（30∶70）为流动相；检测波长：282nm 。

Methods Anhydrous acetic acid as solvent, 0.1 mol/L perchloric acid as titrant, crystal violet solution as indicator to establish non-aqueous titrations and ODS column as stationary phase, methanol and a mixture of 0.025 mol/L sodium phosphate monobasic and 0.02 mol/L sodium dedecyl sulfate (80:20) adjusted with phosphoric acid to a pH (4.8±0.1J as mobile phase, 220 nm as detective wavelength to establish HPLC-UV method for determination of piperazinylethylestrone drug substance; FMOC-CL as a derivatization reagent, FD as a detector to establish an HPLC method with derivatization and column switching for determination of piperazinylethylestrone in dog plasma.

分别采用无水冰醋酸为溶剂，0.1mol/L高氯酸为滴定液，结晶紫指示液指示终点的非水滴定法和HPLC-UV法测定哌嗪雌酚酮原料药含量；以FMOC-CL为衍生化试剂，采用柱切换柱前衍生化萤光检测的HPLC法测定狗血浆中哌嗪雌酚酮含量。

Column: Agilent C18; mobile phase 10mol.l-1 monobasic Acetate buffer, 20 molL-1triethylamine solution adjusted to pH5.5 with Acetic acid -acetonitrile ,gradient elution, flow rate: 0.6 mLmin-1; Results:The Traditional Chinese Medicines contained Acarbose, Phenformin and Glibenclamide, and can be separated completely.

色谱柱：Agilent ZORBAX ODS C18柱(5μm，4.6×250mm， Agilent)；流动相：醋酸盐缓冲液(10molL-1醋酸胺，20 molL-1三乙胺，用醋酸调节pH5.5)与乙腈，梯度洗脱，流速：0.6 mLmin-1，色谱检测波长234nm，格列吡嗪为内标物进行定量分析。

Column: Agilent C18; mobile phase 10mol.l-1 monobasic Acetate buffer, 20 mol·L-1triethylamine solution adjusted to pH5.5 with Acetic acid -acetonitrile ,gradient elution, flow rate: 0.6 mL·min-1; Results:The Traditional Chinese Medicines contained Acarbose, Phenformin and Glibenclamide, and can be separated completely.

色谱柱：Agilent ZORBAX ODS C18柱(5μm，4.6×250mm， Agilent)；流动相：醋酸盐缓冲液(10mol·L-1醋酸胺，20 mol·L-1三乙胺，用醋酸调节pH5.5)与乙腈，梯度洗脱，流速：0.6 mL·min-1，色谱检测波长234nm，格列吡嗪为内标物进行定量分析。

By the time of its fall, most of the prisoners were writers who had written against the corruptions of the government.

到它被攻陷的时候，里面多数的犯人是写了反对政府贪污文章的作家。

The most obvious variation to ovum morphological character was that the color was changed from light green to sepiaceous in embryonic development, and all the ovums were almost hatched after 96h.

在胚胎发育过程中卵的形态特征最明显的变化是颜色从淡绿到深褐色，卵在发育96h后卵基本全部孵化。