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The invention discloses a dielectric hole-microhole composite material and synthesizing method in the inorganic porous material, adsorbing material and catalytic material technical domain, which comprises the following steps: adopting zeolite molecular sieve as raw material; reacting with sodium bisilicate solution under 30-60 deg.c for 10-300 min; disintegrating particle part of zeolite molecular sieve into piece with microhole structure; adding cetyl trimethyl ammonium bromide as molder; adjusting pH value of mother liquid to 10-12; aging 1-8h; adding in the high-pressure autoclave to do water heat synthesizing reaction at 80-130 deg.c for 24-72h; separating solid; washing; drying; sintering under 500-600 deg.c for 5-10h; obtaining the Si-Al porous material with dielectric hole and microhole composite structure.
本发明属于无机多孔材料、吸附材料和催化材料技术领域,涉及具有介孔-微孔复合材料及其合成方法。其特征是以沸石分子筛为原料,用偏硅酸钠的水溶液在30~60℃反应10~300分钟,使沸石分子筛的颗粒部分解离形成具有微孔结构的碎片,加入模板剂十六烷基三甲基溴化铵,然后调节母液pH值为10~12,老化1~8小时,然后加入高压釜于80~130℃进行水热合成反应。反应24~72小时后,分离出固体,水洗、干燥,然后于500~600℃焙烧5~10小时,得到具有介孔和微孔复合结构的硅铝多孔材料。本发明的效果和益处是所发明的合成方法可用于合成多种沸石结构和介孔结构的复合材料,所合成的材料经过质子交换可以具有较强的酸性,在吸附和催化领域具有广泛应用前景。
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The factors which affect the average molecular weight of the polymer of AM and DMDAAC were investigated. The optimal reaction conditions are as follows: the concentration of monomer AM was 30%, while DMDAAC was 5%; the reaction temperature was 30℃, the amount of initiators at the low temperature stage was 0.05‰(compared to the weight of the monomers joining the polymerization), while V-50 was 0.025‰, the weight ratio of potassium persulphate to sodium bisulphite is 1:1, the amount of carbamide was 40‰, and complexing agent was 0.05‰, besides, aerate nitrogen gas for 8min, then the high molecular weight polymer (M=1.217×10^7) could be got after 16h reaction.
研究了影响AM与DMDAAC共聚物的平均分子量的因素,得到了优化条件为:单体浓度为30%,DMDAAC与AM摩尔比为5:95,聚合温度为30℃,低温段引发剂用量为0.05‰,K2S2O8与NaHSO3质量比为1:1,偶氮二异丁基脒盐酸盐(V-50)用量为0.025‰,尿素用量为40‰,乙二胺四乙酸二钠(EDTA-2Na)用量为0.05‰,在此优化条件下聚合反应16h后得到分子量为1.217×10^7的阳离子型聚丙烯酰胺。
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The molecular systematics of Bryaceae is new focus in the study on moss. RAPD has been widely used for molecular systematics, and it's an important technique in phylogeny analysis.
真藓科Bryaceae植物的分子系统学研究是藓类植物研究中的新热点,RAPD是分子系统学研究中被广泛采用的一项重要技术。
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According to molecular design, an inter-molecular-coordination borate eater containing nitrogen as coupling a-gent was synthesized. There are two reactive groups, amino and butoxy in the borate ester molecule.
中文文摘]通过分子结构设计,合成了一种氮-硼内配位结构的硼酸酯偶联剂,解决了硼酸酯水解稳定性差的问题,同时分子结构中含有氨基、丁氧基等活性基团。
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Meanwhile, the standard experiment on addition of small molecular organic arsenics revealed that the small molecular organic arsenics such as cacodylic acid, disodium methylarsonate were detected to be inorganic arsenic by the two detection methods with high recovery efficiency.
同时,试验中用小分子有机砷进行加标试验,结果表明:二甲基胂酸、甲基胂酸二钠等小分子有机砷对两种测定方法的影响很大,会把小分子有机砷作为无机砷检测出来,且检出回收率很高。
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Stannous caprylate was selected as the catalyst. Under certain vacuum, we investigate the relation of both the dose of catalyst, the temperature of reaction, the time of reaction and the molecular weight of the PLA.Furthermore we investigate how the purity of lactide and the circumstance of vacuum affect the molecular weight of the PLA.
实验中选用辛酸亚锡Sn(oct_2为催化剂,在一定的真空度下考察了催化剂用量、反应温度、反应时间与聚乳酸分子量的关系;并考察了丙交酯纯度及真空度对聚乳酸分子量的影响。
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Their adsorption rate on the molecular sieve catalysts surface and the stability of their carbonium ions were then obtained based on the molecular simulation on these molecules from their dipole moment, 2-dimensional electrostatic potential energy contours and 3-dimensional electrostatic potential energy isosurface.
采用半经验的AM1量子化学计算方法和静态理论,分别考察了噻吩、 3 甲基噻吩和 2 ,5 二甲基噻吩分子结构特性的不同,从偶极矩、各自垂直于芳香环平面的二维电势能分布曲线和整个分子周围三维电势能分布情况等方面分析了它们在分子筛催化剂表面吸附速度的快慢和生成正碳离子稳定性的高低,进一步比较了噻吩及其衍生物所生成的正碳离子进一步反应的能量变化,从而可判断噻吩及其衍生物裂化脱硫速度的快慢,噻吩及其衍生物裂化脱硫的速度由大到小分别为:2 ,5 二甲基噻吩、 3 甲基噻吩、噻吩。
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Chapter 2 Study on the preparation and application of a new electrical active-inactive switch molecular beaconWe developed a new electrical active-inactive switch molecular beacon and used carminic acid as signal molecule.
第二章:新型电化学活性-非活性转换分子信标的研制及其应用本章中,首先提出了一种基于电化学活性-非活性分子转换的新型分子信标。
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With the rapid growth in supramolecular chemistry in recent years, a great deal of effort has been devoted to the design and assembly of supramolecular compounds, for these compounds have potential applications in catalyses , molecular recognition, molecular electronics, photonic materials and so on.
近年来,超分子配合物因在催化化学、主客体-超分子化学和分子磁性材料、超导材料、非线形光学材料等方面的潜在应用价值而成为最活跃的研究领域之一。
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Then the reaction rates of IgE and IgG in asthmatic patients serum to chenopodium album pollen were counted by immunoblotting. RESULTS: Twelve bands of protein were obtained through SDS PAGE. The molecular weight of each band was 92, 63.1, 61, 52, 45, 43, 39.7, 38.9, 34, 31.6, 28.4 and 18.5~12 ku. Immunobloting identified 4 protein bands recognized by sIgE, molecular weights being 92, 34, 31.6 and 18.5~12 ku, which reacted with 70%, 50%, 80% and 90% of asthmatic patient serum.
结果: 藜草花粉经电泳后得到12条蛋白质区带,分子质量依次为92, 63.1, 61, 52, 45, 43, 39.7, 38.9, 34, 31.6, 28.4和18.5~12 ku;免疫印迹可见4条sIgE反应带,蛋白分子质量依次为92, 34, 31.6和18.5~12 ku;与患者血清反应率分别是70%, 50%, 80%和90%;与血清sIgG结合的反应带有8条,蛋白分子质量为92, 61, 52, 45, 43, 39.7, 31.6和18.5~12 ku;与患者血清反应率分别是80%, 40%, 10%, 20%, 80%, 10%, 10%和100%。
- 推荐网络例句
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The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.
此刻阴唇已经几乎完全的缝在一起了,排除多余淤血体液的管子和Foley导管从顶端冒出来。
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To get the business done, I suggest we split the difference in price.
为了做成这笔生意,我建议我们在价格上大家各让一半。
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After an hour and no pup, look for continued contractions and arching of the back with no pup as a sign of trouble.
一个小时后,并没有任何的PUP ,寻找继续收缩和拱的背面没有任何的PUP作为一个注册的麻烦。