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RESULTS:The transendothelial electrical resistance of microvessels superfused with artificial cerebrospinal fluid was about 2 500 Ω*cm2, indicating a tight barrier with extremely low ion permeability, and application of 10-4 mol*L-1 histamine in superfusate caused a rapid and reversible decrease of resistance.
结果:脑软膜微血管经灌流人工脑脊液,测得的跨内皮电阻大约为2 500 Ω*cm2,说明微血管内皮是具有较低通透性的致密屏障,在人工脑脊液中加入10-4 mol*L-1组胺引起跨内皮电阻快速的和可逆性的下降。
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Result: The transendothelial electrical resistance of microvessels superfused with artificial cerebrospinal fluid was about 2500 Ω·cm2, indicating a tight barrier with extremely low ion permeability, and application of 10-4 mol·L-1 histamine in superfusate caused a rapid and reversible decrease in transendothelial electrical resistance.
结果 :脑软膜微血管经灌流人工脑脊液,测得的跨内皮电阻大约为 2500Ω·cm2 ,说明微血管内皮是具有较低通透性的致密屏障,在人工脑脊液中加入 10-4 mol·L-1组胺引起跨内皮电阻快速的和可逆性的下降。
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Methods: As the rabbits were anesthetized and mechanically ventilated via a tracheotomies, lung injury was then induced by endotracheal instillation of 0.0225 mol/L hydrochloric acid (12 ml/kg).
新西兰大白兔麻醉后纯氧机械通气15min,经气管导管注人0.0225mol/L的盐酸12ml/kg,造成急性肺损伤。
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The products were identified by IR,NMR,MS and elemental analysis. In our method,K.OH was used in place of NaOH to synthesize benzyl ester of 3,5-dimethyl-4-hydroxybenzoic acid,2',6'-dimethyl-4'-(n-succinimidyloxycarbonyl) phenyl-acridinium-9-carboxylate was purified on a silica gel column with chloroform/ethylacetate(4:l,v/v) as eluent and further purified by triturating with hexane/acetone(2:l,v/v).The luminescence produced by DMAE-NHS is a flash light with maximumemission at 0.4s and decay half-time of 0.9s. The luminescence intensity is 6.11x10 cps/mol,which is affected by the composition of trigger and surfactant.
DMAE·NHS的合成是本论文的关键和难点,我们对文献方法进行改进:文献方法用氢氧化钠与3,5-二甲基-4-羟基苯甲酸反应制得3,5-甲基-4-羟基苯甲酸钠,再用3,5-二甲基-4-羟基苯甲酸钠与苄氯作用制备3,5-二甲基-4-羟基苯甲酸苄酯,我们用氢氧化钾代替氢氧化钠,使合成取得成功;在合成2',6'-二甲基-4'-苯基-吖啶-9-甲酸酯时,文献方法对粗产品进行两次硅胶柱层析纯化,第一次柱层析用氯仿/乙酸乙酯(4:1,Ⅴ:Ⅴ)作溶剂和淋洗剂,第二次柱层析用己烷/丙酮(2:1,Ⅴ:Ⅴ)作溶剂和淋洗剂,按照文献方法得到的不是所需要的化合物,我们只进行第一次柱层析纯化,然后用己烷/丙酮(2:1,Ⅴ:Ⅴ)进行研磨,过滤,洗涤,除去溶于己烷/丙酮(2:1,Ⅴ:Ⅴ)的部分,得到所需要的产品。
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This article discussed the influence factors of productivity of formic acid such as the mol ratio of sodium formate and phosphoric acid, the addition of phosphorus pentoxide, vapouring temperature.
对原料配比、五氧化二磷加入量、蒸馏温度对甲酸产品浓度、产率的影响进行了实验。
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The results showed that the ultimately productive rate of formic acid reached 95.75% when the mol ratio of sodium formate and phosphoric acid was 1:1.30, the quantity of phosphorus pentoxide was 35.73 g, vapouring temperature was 115℃.
实验结果表明:在一定实验体系中,甲酸钠与磷酸摩尔比为1:1.03、五氧化二磷加入量为35.73 g、蒸馏温度为115℃时,甲酸最终浓度可达到95.75%。
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According to the change of the kinds of elements content in slag, F in slag volatilizes in the form of KF and NaF, KF volatilizes much more easily than NaF, KF plays a leading role in the F volatilization, theoretical analysis shows that the saturation vapour pressure of KF in the test slag is 31. 4 times of NaF; when F content is far more than K, KF volatilization is first order grade reaction, it is dominated by K content, the apparent activate energy is 275. 30KJ/mol.
4依据对含氟熔渣中高温条件下(1450℃、1505℃)的各种元素含量的变化情况,发现氟在熔渣中是以碱金属氟化物挥发,并且,KF比NaF具有更好的挥发性,在氟的挥发中占主导地位,理论研究也证明,在1505℃试验组成的熔渣中,KF的饱和蒸气压是NaF的31.4倍;在含氟量远大于钾含量的情况下,KF挥发为一级反应,受钾浓度控制,其表观活化能为275.30KJ/mol。
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The phenyl acetate was synthesized from phenyl hydroxide and acetyl chloride by direct esterification and the factors influencing the synthesis were studied.Results showed that the optimal conditions were:n(C6H6O):n(C2H3OCl)=1:1.2,the amount of solvent cyclohexane was 40 mL(compared to 0.15 mol C6H6O),the reaction temperature was 20℃,and the reaction time was 5 h.
乙酸苯酯(分子式C8H8O2)是重要的药物中间体,它可以转化得到邻羟基苯乙酮和对羟基苯乙酮的混合物,可用于治疗急慢性黄疸型肝炎、胆囊炎等疾病,其中邻羟基苯乙酮是合成抗心律失常药盐酸普罗帕酮的重要中间体。
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It was found that the content of γ-amino butyric acid in brown rice reached the maximum value after soaking for 4 hours at the ratio of brown rice and sodium glutamate 1 200 g/mol, and under the soaking!conditions of pH 5~6, Ca~ 2+ Conceutritio...
发现糙米在浸泡温度40~50℃,Ca2+浓度为0.5mmol/L,pH值为5~6,糙米与谷氨酸钠的比值为1200g/mol的浸泡液中浸泡4h后,其γ-氨基丁酸含量分别达最高。
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In the measurement of the hydroxyproline in the collagen,the traditional acid hydrolysis method is that under 110 ℃ the animal organism is hydrolyzed with 6 mol/L HCl,for 24 h.
在胶原的羟脯氨酸测定中,传统的酸法水解是在110℃下使用6 mol/L的HCl消解24 h,其操作步骤繁琐且所花时间较长。
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It is suggested that TDS can be used as a new method for the analysis of pedogenesis and climatic change.
总之,热处理过程中磁化率的变化能非常灵敏地反映磁性矿物的转化情况,而且,这种转化往往与样品所经历的土壤化作用强度密切相关,因此,TDS可做为分析成土作用强度和古气候变化的一种新方法。
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Therefore, in this chapter, I will research into the conflict and contradiction of the paternity. Also, in this novel, the father's behavior of "He who loves well chastises well." is quite suspicious, one of the reasons is that the father thought his son belonged to him. And then, this thesis quoted Lacan's theory to touch upon that someone who has accepted the concept of patriarchal society, he will be influenced for his whole life. That also reveals that human being has no choice sometimes in this society.
因此本章会先就父子关系的冲突与矛盾做深入的探讨,小说中的父亲似有对儿子爱之深责之切的行为,其原因可能在於父亲将儿子视为所有物所致;其次,论文将引用拉冈相关理论,讨论在父权社会中,不论身分为何,只要是已受父权社会观念根深蒂固影响的人物,终生都将受其所苦,此也揭示出人生存於社会上的无奈。
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But these days, because of everybody's attention,"Super Marie " track begins suddenly to become eccentric, see a chess do not go out only action, be in it seems that sedulous and evasive what.
但这几天,因为大家的关注,"超级玛丽"的行踪突然开始变得古怪,只看棋不出招,似乎在刻意回避着什么。