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We have developed a simple and easy-handling procedure for copper-catalyzed cyanation of aryl halides using K4[Fe_6] as the cyanide source. The present procedure has ligand- and base-free advantages, and was accomplished under the conditions of exposure to the air without degassing of the solvent.4. We carried out the selective control of preparation for phenyl ether and phenol from iodobenzene with 10 mol% of Cu_2·H_2O as the catalyst under the condition of exposure to air.

这个程序有无配体无碱的好处，并能够在暴露于空气的条件下进行，溶剂也不用脱气。4、空气气氛下，用10 mol%的Cu_2·H_2O催化碘苯偶联，实现了制备二苯醚和苯酚的选择性控制：即在有(来源：Aa955BC55论文网www.abclunwen.com)机溶剂NMP中实现了碘苯直接制备二苯醚的Ullmann反应，在H2O中实现了碘苯直接制备苯酚。

In combination of oxygen nonstoichiometry data determined using the iodometric titration, the oxygen chemical diffusion coefficient D〓 for YBa〓Cu〓O〓 is calculated. D〓 takes a value of 7. 8×10〓 at 650℃ and 2. 0×l0〓cm〓s〓 at 800℃, and the associated apparent activation energy is 51±0.9 kJ·mol〓.

根据Fick第一定律，结合氧渗透率数据及氧非化学计量数据，可计算出YBa〓Cu〓O〓的氧化学扩散系数D〓在650～800℃，D〓为7.8×10〓～2.0×10〓cm〓，D〓的表观活化能为51±〓0.9 kJ·mol〓。

It is found that UIFR with softening point of 90℃, OH value of 32mg KOH/g andM of 377 g/mol is synthesized when molar ratio of isobutyraldehyde to formaldehyde is 1.5, molar ratio of aldehyde to urea is 6, vacuum distillation temperature and time is 140℃ and 1 h respectively. The terpolycondensate is soluble in most solvents, of paints and exhibits excellent yellowing-resistance.

结果表明，在异丁醛、甲醛摩尔比为1.5，醛、脲摩尔比为6，真空蒸馏温度为140℃、时间为1h的条件下，合成出的UIFR软化点为90℃，羟基值为32mgKOH/g，M为377g/mol，且树脂具有良好的溶解性和杭黄变性。

All of them were labeled with [32P] orthophosphate (2.03×10^5 Bq/mL) for 2 h and then stimulated with CCK8 l0^(-7 mol/L and DMEM respectively for different time. Reactions were terminated by freezing neurons in liquid nitrogen. The 32P-labeled lysates isoelectrically focused on IPG Drystrip pH 4~7 linear gels and subsequently separated by second-dimensional SDS-PAGE.

培养乳小鼠神经元，随机分为CCK8刺激组和对照组，32P-NaH2PO4标记后分别给予CCK810^(-7 mol/L和等量无磷培养基，作用不同时间后液氮终止反应，经双向电泳、放射自显影，获得磷酸化蛋白质的电泳图谱。

6Fe_2O_3. 1.81 (CaO.2Fe_2O_3) The apparent activation energy of barite decomposition in air is 119.9 kJ/mol and the order of reaction is 1.3—1.4 obtained by kinetical calculation.

动力学计算表明，在空气中重晶石分解的表观活化能E~*=119.9kJ/mol，反应级数n=1.3—1.4。

A 30 min exposure to peroxynitrite (10〓μmol/L) followed by incubation in fresh medium induced apoptosis in cultured cerebellar granule cells, which was confirmed by DNA laddering, chromatin condensation, nuclei fragmentation, and the formation of apoptotic bodies.

原代小脑颗粒细胞经10μmol/L过氧化亚硝基处理30min，并继续培养一定时间后逐渐发生细胞凋亡，主要表现为DNA链断裂、染色质凝缩、核破裂、形成凋亡小体。

We may well explain why ricin-induced apoptosis showed no typical DNA ladder. The presence of laddering in DNA gels implies an apoptosis process, but its absence does not rule out the apoptosis. The ricin 0.05μmol〓 had no effect on the 〓 phase of cell cycle, but induced 〓 arrest. The ricin may affect the balance of synthesis and destruction of proteins that controlling the cell cycle.

检测到DNA梯度表明细胞发生了细胞凋亡，未检测到DNA梯度不能否认凋亡的存在。0.05μmol.L〓的蓖麻毒素对HeLa细胞周期的G〓/G〓期无影响，而诱导了G〓/M期阻滞，蓖麻毒素可能引起一些控制细胞周期蛋白的合成与降解发生紊乱。

Five new bacterial diseases of Ligularia fischeri, Vigna angularis , Brassica juncea var.japonica, Aconitum coreanum and Silybum marianum in Jilin province were firstly reported in the world; and their sympotoms of the diseases were described in detail. According to the configuration of the pathogens observed by electrical microscope, Gram staination, pathogenicity, cultural characters, physiological and biochemical characters, as well as G+C mol%, the pathogens were identified respectively .

首次报道了马蹄叶腐烂病、红小豆溃疡病、黄花乌头顶枯病、江户菜软腐病和水飞蓟软腐病在吉林省的发生，详细描述了该五种病害症状及危害情况；通过对分离的病原菌的电镜形态观察、革兰氏染色、致病性、培养性状、生理生化性状、G+C mol％等方面的测定，依据《Bergey's Manual of determinative Bacteriology》9th ed相关部分，初步确定了其病原菌的分类地位并对病原菌进行了室内药剂筛选。

The different Melilotus varieties under the condition of the low content (1ower than 0.10 mol/L) salt stress showed certain degree of adaptability, but with the increase of salt content, the inhibitory concentration level also increased.

各草木樨品种对低浓度(≤0.10 mol/L)盐胁迫有一定的适应性，但随盐浓度的增加其受抑制程度加剧。

In different NaCl salt stress solution concentrations (which were 0.05, 0.1, 0.15, 0.2, 0.25, 0.3, 0.35 mol/L), the seven salt tolerance of Melilotus varieties of the germination percentage was calculated, including the relative germination percentage, seed potentiality, germination index, the sprouts length, the relative sprouts length and the salt index.

以7个耐盐草木樨品种种子为材料，用不同浓度NaCl（NaCl浓度分别为0.05， 0.10， 0.15， 0.20， 0.25， 0.30和0.35 mol/L）胁迫处理后，测算其种子的发芽率、相对发芽率、发芽势、发芽指数、胚芽长度、相对胚芽长度和耐盐指数。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。