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Under technological conditions such as: room temperature, current density 200 A/m^2, anolyte acidity 0.5 mol/L chlorhydric acid, acidity of catholyte 1.5 mol/L chlorhydric acid, circulation of anolyte and catholyte 40 L/h, Ni(superscript 2+) concertration 0.85 mol/L, and the average cell voltage 1.3 V, the electricity consumption of dissolving a ton of nickel base alloy is 813 kWh, and the Ni(superscript 2+) retention rate of the ion exchange membrane is more than 99.5%.

在电流密度200 A/平方公尺、阳极酸度0.5 mol/L、阴极酸度1.5 mol/L、循环量40 L/h、Ni(上标 2+)浓度0.85 mol/L左右和室温的条件下电解,平均槽电压1.3 V,电溶1 t镍合金板耗电813 kWh,阴离子交换膜对镍的截留率大於99.5%。

The ventilatory responses of peripheral chemoreflex following 0.1 m l microinjection within the NTS of either PTK inhibitor genistein(10 mol/L), AMPA glutamate receptor inhibitor CNQX (10 mol/L),or inactive PTK inhibitor daidzein (10 mol/L) were recorded.

在孤束核处分别微量注射蛋白酪氨酸激酶的抑制剂genistein和其非活动性抑制剂daidzein 以及 AMPA受体阻断剂CNQX,观察这些药物对外周化学感受性反射的影响。

Self-assembly of PEO-b-PB (M〓of PEO=5100 g/mol and M〓 of PB=5100 g/mol) and poly (PAA, M〓=2000 g/mol) was obtained in THF/dodecane mixtures via PEO/PAA complex. The effect of ratio of PEO-b-PB: PAA was investigated.

通过PEO-b-PB(PEO和PB分子量均为5100g/mol)中PEO链段和聚丙烯酸(PAA,分子量为2000g/mol)的氢键相互作用,我们在THF/正十二烷混合溶剂中获得了PEO-b-PB/PAA的自组装体,并研究了PAA用量对自组装行为的影响。

Further, at concentrationssimilar to the maximum therapeutic plasma concentrations (10–7 mol/L olprinone; 10–6 mol/L milrinone; 10–5 mol/Lamrinone) olprinone and milrinone were more potent at inducingrelaxations than amrinone in gastroepiploic arteries and radialarteries, whereas in internal mammary arteries milrinone wasmore potent than the others.

此外,在与最大治疗血浆浓度相近似的浓度中(10–7 mol/L 的奥普力农、10–6 mol/L 的米力农、10–5 mol/L 的氨力农)时,奥普力农和米力农对胃网膜和挠动脉的舒张作用比氨力农强;而对乳内动脉,米力农的舒张作用比其它两者更强。

The kinetic behaviors of ethylene homo- olymerization and ethylene / l-hexene co-polymerization , catalyzed by the metallocene catalyst PS-DVB-MC in an 0.5 L stainless steel reactor , were studied. The effects of polymerization conditions on ethylene polymerization , such as concentration of catalyst , temperature of polymerization , pressure of ethylene , molar ratio of AI / Z r , etc ., were also investigated . Some leading results were as follows : the activity of the catalyst PS–DVB- MC for ethylene homo-polymerization was high ( 1.053 x 107 gPE / mol Zr·h ), but the molar ratio of AI / Zr was low ( 350:1 ); the catalytic ability for ethyleneα-olefin ( such as l hexene etc .) co-olymerization was great , and the corresponding activity come up to a maximum of 1.753 x 107 gPE / mol Zr·h while concenlration of l-hexene was 0.080 mol / L ; the molecular weight of polyethylene was about 180,000 , meanwhile the molecular weight distribution was narrow ( 2.19 ); the bulk density of polyethylene and ethylene / l-hexene co -polymer were 0.25 and 0.34 respectively .

采用0.5L高压不锈钢反应釜,对催化剂PS–DVB-MC催化乙烯均聚和乙烯/ l-己烯共聚合的动力学行为进行了研究,详细考察了催化剂浓度、反应温度、压力、Al/ Zr比、1-己烯浓度等因素对乙烯聚合反应的影响,得到如下主要结论:催化剂PS-DVB-MC具有催化乙烯均聚的高活性(1.053×107g PE / mo1 zr.hr),低Al / Zr比( 350:1 );具有良好的催化乙烯与α-烯烃(如1-己烯等)共聚的能力,在1-己烯浓度为0.080 mol / L时,催化活性达到最大(1.783×107 g PE / molZr.hr);乙烯均聚产物的分子量在18万左右,分子量分布窄( 2.19 )。

The results calculated by the Elovich rate equation showed that K release rates from 1 mol.L-1 HNO3 extraction >those from 2 mol.L-1 HNO3 extraction >those from H-resin extraction. Elovich equations combining with the data of H-resin and 2 mol.L-1 HNO3 successive extraction could well described the release characteristics of soil K. The correlation coefficients of the equations reached most significant levels (r=0.956**—0.999**), and standard errors of specific K release capacities between the vaules calculated by the equations and those measured by both successive extractions were smaller(s=1.61 and 3.52). The specific release rates of soil K calculated by the Elovich rate equations were significantly correlated with the indices of soil K availability (the amounts of easily available K, nonexchangeable K, total available K in soils and K absorbed by ryegrass).

研究结果表明:1 mol.L-1 HNO3提取法的释K速率>2 mol.L-1 HNO3提取法的释K速率>氢饱和交换树脂提取法的释K速率;氢质交换树脂和2 mol.L-1 HNO3提取法结合Elovich模型较理想地描述了土壤K素的释放特性,拟合方程的相关系数均达极显著水平(r=0.956**-0.999**),土壤特征累积释K量的计算值与实测值的标准差较小(s=1.61和3.52),且通过速率方程计算的土壤特征释K速率与K素有效性指标(速效K、缓效 K、有效K及黑麦草总吸K量)的相关性也较为密切。

Methods Anhydrous acetic acid as solvent, 0.1 mol/L perchloric acid as titrant, crystal violet solution as indicator to establish non-aqueous titrations and ODS column as stationary phase, methanol and a mixture of 0.025 mol/L sodium phosphate monobasic and 0.02 mol/L sodium dedecyl sulfate (80:20) adjusted with phosphoric acid to a pH (4.8±0.1J as mobile phase, 220 nm as detective wavelength to establish HPLC-UV method for determination of piperazinylethylestrone drug substance; FMOC-CL as a derivatization reagent, FD as a detector to establish an HPLC method with derivatization and column switching for determination of piperazinylethylestrone in dog plasma.

分别采用无水冰醋酸为溶剂,0.1mol/L高氯酸为滴定液,结晶紫指示液指示终点的非水滴定法和HPLC-UV法测定哌嗪雌酚酮原料药含量;以FMOC-CL为衍生化试剂,采用柱切换柱前衍生化萤光检测的HPLC法测定狗血浆中哌嗪雌酚酮含量。

The calculated results with B3LYP/6-31G-DFT show:(1)the molecular total energy of benzofuroxan is lower than that of o-dinitrosobenzene;(2)the activation energy(Ea+=51.0kJ/mol)of forward reaction that benzofuroxan isomerises into o-dinitrosobenzene,is in agreement with the experimental(58.6kJ/mol)provided by reference,and the activation energy(Ea-=4.6kJ/mol)of back-ward reaction is very small.It is concluded thereby that benzofuroxan is more stable than o-dinitrosobenzene.In addition,the corresponding ab initio calculations at the level of HF/3-21G,HF/6-31Gand MP2/6-31G//6-31G were completed,and it was found that the calculated results by B3LYP-DFT method are superior to those from ab initio calculation.

结果表明,苯并氧化呋咱的分子总能量比邻二亚硝基苯的低;由苯并氧化呋咱异构为邻二亚硝基苯的正向反应活化能(Ea+=51.0kJ/mol),与文献实测值(58.6kJ/mol)较接近,而其逆向反应活化能(Ea-=4.6kJ/mol)很小,从而揭示了苯并氧化呋咱比邻二亚硝基苯更稳定·此外,进行了HF/3-21G、HF/6-31G和MP2/6-31G//6-31G水平下相应的计算,发现B3LYP-DFT的结果较abinitio为优。

From the potential energy profile, it can be predicted that, the dominant channel of this reaction consists of three steps: the two reactants first form a three-membered ring intermediate (INT1) through a barrier-free exothermic reaction of 19.2 kJ/mol; three-membered ring intermediate (INT1) isomerizes to a four-membered ring silylene(P2) via the transition state (TS2) with an energy barrier of 22.8 kJ/mol; four-membered ring silylene(P2) further reacts with ethene(R2) to form a silicic bis-heterocyclic compound (P3), which is also a barrier-free exothermic reaction of 132.2 kJ/mol.

用CCSD//MP2/6-31G*方法研究了单重态二甲基亚烷基硅烯与乙烯生成硅杂双环化合物环加成反应的机理,根据该反应的势能面可以预言,该反应的主反应通道有三步组成:第一步是两反应物(R1, R2)首先生成了一三元环中间体(INT1),它是一无势垒的放热反应,放出的能量为19.2 kJ/mol;第二步是三元环中间体(INT1)经过渡态TS2异构化为了四元环硅烯(P2),其势垒为22.8 kJ/mol;第三步是四元环硅烯(P2)进一步与乙烯(R2)反应生成了硅杂双环化合物(P3),该反应也是一无势垒的放热反应,放出的能量为132.2 kJ/mol。

The calibration curve is linearly proportional to the concentration of chlorpyrifos over the range 2.0×10~(-4) mol·L~(-1)—7.25×10~(-7) mol·L~(-1) with a regression coefficient 0.99948 and a detect limit 9.0×10~(-8) mol·L~(-1). Part 4. Determination of Thiram hangover in Mushroom by B-Z chemical oscillating Reaction.

第四部分蘑菇中福美双残留的快速检测依靠B-Z化学振荡反应体系,建立了蘑菇中福美双含量的快速测定方法。

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As of Tuesday, Google's results were still censored in China.

截至周二,谷歌的搜索结果仍受中国审查。

In order to make the positive action increase and negative one decrease, the sub-forces of the social factors must be adjusted to form a centripetal force.

在这一过程中,人的主体性发挥是社会有机体健康发展的灵魂。

Objective To investigate the relationship between the telomer ase activity and apoptosis in gastric cancer.

目的为了探讨胃癌组织中端粒酶与细胞凋亡的关系。