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The flow stress increases with increasing the strain rate, and decreases with increasing the deforming temperature, which can be described by a constitutive equation in hyperbolic sine function with the hot deformation activation energy of 209.84 kJ/mol, and can also be described by a Zener-Hollomon parameter.

该合金热压缩变形的流变应力行为可用双曲正弦形式的本构方程来描述,也可用Zener-Hollomon参数来描述,其变形激活能为209.84 kJ/mol。

The material parameters in the hyperbolic sine constitutive equation were determined with regression analysis, and the DRX activation energy was thus obtained to be 269 kJ/mol. The relationship between critical strain, peak strain/stress and the dimensionless parameter Z/A were established by linear regression.

采用回归法确定了双曲线本构方程中的材料常数和动态再结晶激活能(269kJ/mol),并建立了临界应变、峰值应变和峰值应力与无量纲参数Z/A之间的关系。

The results indicate that the flow stress of the alloy increases with increasing strain rate and decreasing deformation temperature. The flow stress increases with increasing strain until the stress reaches the peak value, then the flow stress remains constant, which indicates that dynamic recrystallization happens during deformation. The flow behaviors are described by the hyperbolic sine constitutive equation, and the activation energy calculated is 337.75 kJ/mol. The as-forged microstructure consists of refined α2/γ and γ grains, and the grains are much homogeneous than before. The B2 phase distributes uniformly at the grain boundary of α2/γ and γ grains. The B2 phase decreases with increasing deformation temperature.

结果表明:流变应力随着应变速率提高和变形温度降低而增大;在变形过程中,流变应力随着变形量增大而增大,当流变应力达到峰值后趋于平稳,表明合金在变形过程中发生了动态再结晶;热变形过程的流变应力可采用双曲正弦本构关系来描述,平均激活能为337.75 kJ/mol;从合金的组织演化过程中可以看出,合金中不均匀的原始组织得到明显均匀化,变形后的组织是由α2/γ层片晶团和γ晶粒组成的双态组织,在α2/γ层片晶团和γ晶粒的晶界交界处发现分布均匀的B2相,并且随着变形温度升高B2相数量逐渐减少。

Methods There were 268 patients with severe icteric hepatitis(TBiL≥170.1μmol/L,PTA≥40%) who were divided into the treating group(136 cases) and the control group(132 cases).

2 6 8例重度黄疸肝炎(TBiL≥ 170 1μmol/L ,PTA≥ 4 0 %)病人分治疗组(136例)和对照组(132例),在同样对症治疗的基础上,治疗组加用蝮蛇抗栓酶 0 5~ 0 75U静滴,4周为 1个疗程。

The rats in group C were raised without any special interposal as control group. On the 14th day of the experiment, all rats in 3 groups received esophageal acid perfusion with 0.1 mol/L HCl, the drops was kept at 37℃ and 10 mL/h, the total duration lasted 50 min.

实验第14天,对A、B、C组动物分别进行食管酸灌注,使用0.1 mol/L盐酸滴注,滴注液保持37℃,速度10 mL/h,共50 min。

The results show that the calculated cell parameters are in agreement with the experimental ones. The interactions between Li—N and Al—N are strong ionic bonds in Li3AlN2. The interaction between N and H is strong covalent bond and the interaction between Li and N is strong ionic bond in LiNH2. The calculated reaction enthalpies are 23.7 and 55.3 kJ/mol, respectively, which are in agreement with the experimental ones.

结果表明:Li3AlN2的Li—N、Al—N键主要为离子键,LiNH2的N—H键主要为共价键,Li—N键主要为离子键;298 K时贮氢反应的反应焓计算值分别为23.7和55.3 kJ/mol,与实验值均符合得较好;反应中各固态、气态物质的晶胞的结构优化后的晶格常数、键长与键角等与相应的实验值均符合较好。

However, only β-ionone replaced the bis-ANS of MmedCSP1 by 50%, and the binding constant was 16.89 μmol/L.

但只有脂类化合物β-紫罗兰酮能在浓度为1mmol/L下将bis-ANS从MmedCSP1中替换50%,β-紫罗兰酮与MmedCSP1的结合常数为16.89μmol/L。

The present paper covers a simple method for preparing urease from jack bean. In terms of the method, the total yield was 37. 1% and the specific activity was 43. 6 μmol ?min-1/ mg protein.

报道了以刀豆为原料制备脲酶的一种简便方法,其总收率为37.1%,比活达43.6μmol·min~(-1)/mg蛋白。

And adsorption of jack bean proteins onto the amphoteric resin was studied in this paper. The amphoteric resin was in innersalt form. The results of adsorption experiments show that when the proteins are adsorpted into the amphoteric resin in the neutral phosphate buffer solution, the diffusion coefficient of protein is near twofold in 0.4 mol/L NaCl phosphate buffer solution than that in solution without salt, and the adsorption capacity of protein also rises at the same ti...

通过盐浓度对吸附的动力学和热力学影响的研究,结果表明,在中性磷酸盐缓冲液中,两性树脂吸附刀豆蛋白,有盐( 0 。4mol/L Na Cl)的比无盐的扩散系数提高将近一半,且吸附量增加,其吸附等温线的效率在最初始部分高于无 Na Cl时的;随着盐浓度( 0~ 1 mol/L Na Cl)的提高,树脂对蛋白的吸附量也变大,盐浓度提高时树脂膨胀体积的增大与蛋白吸附量的增加呈线性关系,内盐型两性树脂对大分子蛋白质的吸附作用与小分子高价离子的相似,同样是通过内盐键破裂吸附。

The results show that when the mass ratio of sodium jarosite residue to anthracite is 5∶1, reduction roast lasts at 800℃for 0.5 h, leaching is carried out at 70℃for 40 min by 0. 5 mol/L H2SO4 with liquid-solid ratio of 7∶1, 93% of both iron and nickel can be leached out.

研究结果表明:当黄钠铁矾渣与无烟煤按质量比为5∶1均匀混合,在800℃还原焙烧0.5 h,焙烧渣用0.5 mol/L硫酸溶液按液固比7∶1在70℃浸出40 min时,渣中93%的铁和镍进入浸出液中。

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