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The optimum conditions are 0.2 mol chlorobenzene, and 0.7 g catalyst, and 0.07 mol glycine, and 0.08 mol nitric acid, and reaction time of 3 hours, and reaction temperature of 45℃.

最宜工艺条件：氯苯为0.2 mol，催化剂为0.7 g，氨基乙酸为0.07 mol，硝酸为0.08 mol，反应温度为45℃，反应时间为3 h。

The profile distributions of silicate, phosphate and nitrate suggest that the organic material decomposition in area is mainly through nitrification during early diagenesis. Based on benthic fluxes of nutrients calculated using Fick's first law, benthic fluxes of silicate, phosphate and nitrate are -886.45~42.62 mol/(m^2d),-3.04~5.83 mol/(m^2d) and -189.43~21.05 mol-(m^2d), respectively, and perhaps silicate and nitrate are one of the major sources of nutrients for bottom water. Our results also reveal temporal and spatial variations of benthic fluxes for silicate, phosphate and nitrate, which may be related to sedimentation environment changes caused by global climatologic change.

在水－沉积物介面附近矽酸盐、磷酸盐和硝酸盐都存在著极陡的浓度梯度，Fick扩散定理的计算结果表明，研究区内矽酸盐、磷酸盐和硝酸盐的海底扩散通量分别为-886.45～42.62mol/、-3.04～5.83mol/和-189.43～21.05mol/，且矽酸盐和硝酸盐主要是从沉积物向底层水体扩散，是底层水体营养盐的来源之一；研究区内矽酸盐、磷酸盐和硝酸盐的海底扩散通量存在著一定的时间和空间变化，这可能与因全球气候变化而导致的沉积环境的改变有关。

Collector current is proportional to concentration of dopamine in the range over 5.0×10〓mol/L to 5.0× 10〓mol/L and remains independent of ascorbic acid concentration to approximately 5. 0×10〓mol/L.

由于在收集电极上消除了由电位变化引起的充电电流和阴极-阳极工作时的反馈作用，多巴胺的检测限可达7.5×10〓mol/L，线性范围为5.0×10〓～5.0×10〓mol/L。

Optimum extraction conditions were selected by the condition experiments and the concentration of Cu, Pb, Zn in main components were also determined for revealing the distribution of the heavy metals in the suspended particulate matters. It was found that hydroxylamine hydrochloride (0.006 mol/L NH2OH·HCl+0.01 mol/L HNO3) can remove most of Mn oxides, and sodium dithionite 0.8 mol/L Na2S2O4

结果表明，0.006 mol/L NH2OH·HCl+0.01 mol/L HNO3萃取30 min可以单独萃取悬浮颗粒物中大部分的锰氧化物，0.8 mol/L Na2S2O4（pH=6.0）萃取40 min可以同时萃取铁、锰氧化物，而对非目的组分的影响较小；悬浮颗粒物对Cu、Pb、Zn重金属有明显的富集作用，其中Cu主要结合在悬浮颗粒物的有机质组分中，Pb主要富集在铁、锰氧化物中，锰氧化物和有机质对Zn的分布起主要的富集作用。

METHODS: The rabbit hindlimb normothermic tourniquet ischemia model was employed. The tendon on the dorsum of the foot was exposed for observation of microvessels. The responses of arterioles on tendon surface to topical application of 10(-6) mol/L noradrenaline, 10(-6) mol/l acetylcholine (an endothelium-dependent vasodilator) and 10(-4) mol/L nitroglycerin (an endothelium-independent vasodilator) were observed at the period of ischemia and following 30 minutes of reperfusion after 2 hours and 5 hours of ischemia by use of intravital microscopy.

应用兔后肢止血带常温缺血模型及足背肌腱表面微循环观察法，观察肢体缺血 2小时及 5小时再灌注后微动脉对局部滴注血管收缩剂 [去甲肾上腺素(10 - 6 mol/ L ) ]、内皮依赖性血管舒张剂 [乙酰胆碱(10 - 6 mol/ L ) ]及内皮非依赖性血管舒张剂 [硝酸甘油(10 - 4 mol/ L) ]的反应性变化。

The present invention adopts the technical proposal of adopting ZSM-5 mesoporous molecular sieve raw powder with a silicon-aluminum mol ratio SiO2Al2O3 of 20 to 1000 and a weight percentage of 20 to 100 percent as well as at least one caking agent selected from SiO2, clay and Al2O3 to extrude, tablet or spray into shape; then treating for 1 to 8 hours by 0.1 to 3 mol/l of at least one ammonium liquor from ammonium nitrate, ammonium chloride or ammonium sulphate or 0.1 to 8.5 mol/l of at least one acid liquor from muriatic acid, nitric acid, vitriol or acetic acid under a temperature of 20 to 90 DEG C; then using steam to treat for 2 to 15 hours under the temperature condition of 400 to 700 DEG C; using a liquor of 0.1 to 3mol/l selected from at least one of oxalic acid, citric acid or maleic acid under a temperature condition of 20 to 90 DEG C to dip for 2 to 5 hours to obtain the modified molecular sieve catalyst, thus better solving the problems.

本发明通过采用硅铝比SiO2/Al2O3为20～1000重量百分比计20～100％的ZSM-5介孔分子筛原粉与余量的选自SiO2、粘土或Al2O3中至少一种粘结剂挤条、压片或喷球成型；再经过0.1～3摩尔/升选自硝酸铵、氯化铵或硫酸铵中的至少一种铵溶液或0.1～8.5摩尔/升选自盐酸、硝酸、硫酸或乙酸中的至少一种酸溶液在温度20～90℃下处理1～8小时；然后在温度为400～700℃条件下水蒸汽处理2～15小时；再用0.1～3摩尔/升选自草酸、柠檬酸或马来酸中至少一种在温度为20～90℃条件下浸渍2～5小时得所需改性分子筛催化剂的技术方案较好地解决了该问题，可用于甲醇转化制丙烯的工业生产中。

The linear range for resorcinol is 5.0×10^(-9)~1.0×10^(-4) mol/L with the detection limit of 3.0×10^(-9) mol/L. The relative standard deviation is 3.5% for 1.0×10^(-6) mol/L resorcinol in 11 repeated measurements.

该法测定间苯二酚的线性范围为5.0×10^(-9)~1.0×10^(-4)mol/L，检出限为3.0×10^(-9)mol/L，相对标准偏差为35%（1.0×10^(-6)mol/L间苯二酚，n=11。

Results: The satisfactory separation was achieved on optimization of electrophoretic condition: 0.08 mol·L-1 heptane-10% isopropanol - 0.01 mol·L-1 sodium tetraborate buffer - 0.12 mol·L-1 SDS (pH 9.0) as microemulsion with on - column UV monitoring at 214 nm,25 kV applied voltage, 30 ℃ column temperature.

微乳毛细管电泳在吉他霉素组分分离方面的成功应用，为结构相似的中性物质的分离提供了一种新方法，也为日后的定量测定提供了依据。

Chelator-assisted hydrothermal method for growing ZnO nanopricks ZnO nanopricks were formed while 0.3 mol/L diaminoethane, 3 mol/L butylamine and 0.25 mol/L EDTA were used as chalators to react with zinc foil at 100℃ for 12 h.

络合物水解法制备ZnO球形颗粒利用酒石酸锌的水解反应，在水溶液中制备了由超细颗粒组装的ZnO球形颗粒，XRD、HRTEM检测结果表明颗粒为纤锌矿ZnO多晶结构，在溶液中添加乙二醇，产物的尺寸和分散性得到了改善。

Molecular beacon coupled with carminic acid was electrochemical inactivity,but after hybridized with complementary sequence, electrochemistry signal was greatly enhanced,and it was linear related with the concentration of complementary sequence in the range of 6.0×10~(-8)mol/L～1.4×10~(-6) mol/L,with the detective limit of 1×10~(-8)mol/L.

此类分子信标本身在实验选定条件下无电化学信号，与完全互补序列杂交后产生电化学信号，论文采用碳纳米管修饰电极对杂交前后的电化学信号进行检测。

The circulation, consumption and reproduction of the trilogy have not only testified to its historical significance and literariness, but also invested it with new meanings.

该三部曲的流通、消费与再生产不仅验证了其历史意义及文学性，而切还赋予它以新的意义。

If he thought that he could buy me off, he would be wrong.

如果他认为他可以收买我，那他就大错特错了。