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Under the optimal conditions 1.5×10~(-3 mol/L of 22, 1.0 MPa of O_2, 120℃, 20 h, the conversion of ethylbenzene was 37.8%, and the selectivity for acetophenone and 1-phenylethynol was 82.5% and 13.5% respectively.

在22浓度为1.5×10~(-3)mol／L，氧气压力为1.0 MPa，120℃反应20 h，乙苯转化率为37.8％，苯乙酮的选择性为82.5％，1-苯基乙醇的选择性为13.5％，锰配合物23次之。

Under optimal conditions, oxidation of ethylbenzene into acetophenone under 1 atm O2 and 1 mol% NHPI reach to 64% yield.

在最佳的催化状态下，苯乙烷能在1 atm的氧气、1 mol% NHPI与轴向配位基为吡啶的紫质修饰二氧化钛共催化下，氧化成苯乙酮，并得到64%的产率。

The mobile phase was a mixture of acetonitrile 0.378 mol/L acetum (30∶70) and in a flow rate of 0.8 mL/min; The detective wavelength was 321 nm; Column temperature was room temperature and the injection quantity was 10 μ L.

色谱柱 Lichrospher C 18 (4.6 mm ×250 mm，5 μm)，C 18 保护柱；流动相：乙腈 0.378 mol/L冰醋酸水溶液(30∶70)；检测波长321 nm；流速0.8 mL/min；柱温：室温；进样量10 μL。

The effect of different calcium chloride concentration, reaction time and neutralized acid on yield of tagatose was investigated by single factor tests. Results showed that the condition, such as calcium chloride (0.01～0.03 mol/L), reaction time(20～40 min), acetum, carbon dioxide, phosphate acid to synthesize tagatose was suitable.

通过单因素实验，确定了以D-半乳糖为原料进行化学法合成D-塔格糖的工艺条件为：CaCl2的添加量在0.01～0.03 mol/L，反应时间在20～40 min，并用醋酸、CO2、磷酸中和时D-塔格糖产率较高。

Through the orthogonal experiment, the optimum condition for tagatose synthesization was determined to be 0.02 mol/L calcium chloride, 30 min, acetum neutralization.

通过正交设计实验优化反应条件，最终确定以0.02 mol/L的CaCl2为催化剂，反应时间30 min，用醋酸中和金属氢氧化物D-塔格糖复合物时，D-塔格糖的产率最高，可达到49.05%。

The activation energy was calculated to be 406 kJ/mol and the rate constants were determined.

测定了各反应条件下的反应速率常数并测得其活化能为406kJ/mol。

When the concentration of Mn(superscript 2+) in the nutrient solution was 1.0×10^(-5) mol/L, the root activity and the content of aloin and aloe-emodin were the highest. The content of Mn(superscript 2+) in the Aloe barbadensis Mill. increased as the concentration of Mn(superscript 2+) supplied improved.

当营养液中Mn(上标 2+)浓度为1.0×10^(-5) mol/L时，芦荟根活力最高，芦荟苷和芦荟大黄素含量也最高；随着供Mn(上标 2+)浓度的提高，芦荟体内Mn(上标 2+)含量不断增加。

RESULTS: Both HPC and treatment with ruthenium red (5 μmol/L) during the first 10 min reoxygenation improved recovery of LVDP,±dp/dtmax and decreased LVEDP, which was associated with reduced infarct size and lactate dyhydrogenase release.

用TTC染色法测心肌梗死面积。结果：低氧预处理和低氧后复氧期的前10 min用钌红（5 μmol/L）处理均可促进LVDP、±dp/dtmax和LVEDP的恢复，减小心肌梗死面积，减少LDH释放。复氧期的前10 min用精胺(20 μmol/L)处理可减弱低氧预处理的心脏作用。

Kcal/mol and one between 32 and 49℃ with Ea=2. 44 Kcal/mol.

在13-32℃，反应的活化能为7.23 Kcal／mol。

The sensor show Nernst response for 20× 10〓～50×10〓mol/L nicotinic acid with detective limit of 2.0×10〓mol/L, other advantages of the sensor include resistance to poison、 fast response et al..

用电化学方法制备的烟酸-PPy化学传感器对2.0×10〓～5.0×10〓mol/L浓度范围内的烟酸有良好的Nernst响应，传感器具有选择性好、响应快、制备容易等优点。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。