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The mobile phase was a mixture of acetonitrile 0.378 mol/L acetum (30∶70) and in a flow rate of 0.8 mL/min; The detective wavelength was 321 nm; Column temperature was room temperature and the injection quantity was 10 μ L.

色谱柱 Lichrospher C 18 (4.6 mm ×250 mm，5 μm)，C 18 保护柱；流动相：乙腈 0.378 mol/L冰醋酸水溶液(30∶70)；检测波长321 nm；流速0.8 mL/min；柱温：室温；进样量10 μL。

The effect of different calcium chloride concentration, reaction time and neutralized acid on yield of tagatose was investigated by single factor tests. Results showed that the condition, such as calcium chloride (0.01～0.03 mol/L), reaction time(20～40 min), acetum, carbon dioxide, phosphate acid to synthesize tagatose was suitable.

通过单因素实验，确定了以D-半乳糖为原料进行化学法合成D-塔格糖的工艺条件为：CaCl2的添加量在0.01～0.03 mol/L，反应时间在20～40 min，并用醋酸、CO2、磷酸中和时D-塔格糖产率较高。

Through the orthogonal experiment, the optimum condition for tagatose synthesization was determined to be 0.02 mol/L calcium chloride, 30 min, acetum neutralization.

通过正交设计实验优化反应条件，最终确定以0.02 mol/L的CaCl2为催化剂，反应时间30 min，用醋酸中和金属氢氧化物D-塔格糖复合物时，D-塔格糖的产率最高，可达到49.05%。

In order to investigate the capabilities of zircon as waste forms for immobilizing simulated trivalent actinides, trivalent europium (Eu3+) was used as the simulacrum for trivalent actinides, the waste forms containing 20 mol% Eu3+ were successfully synthesized by high temperature solid reaction and using ZrO2, SiO2 and Eu2O3 powders as starting materials.

中文摘要：为研究锆英石基三价锕系模拟核素固化体的性能，利用Eu3+作为三价锕系核素模拟替代物质，以ZrO2、SiO2和Eu2O3粉体为原料采用高温固相法制备了包容Eu3+为20mol%的锆英石基固化体。

This model was finely fitted by theexperimental results and was used to calculate the activation area,which was 0.127 〓/mol with little dependence of subphasetemperature. The positive activation area indicate that there is anincrease in area when the activated complex is formed, increasingthe surface pressure should decrease the rate constant and that theactivated complex is unimolecular in nature.

在一系列实验曲线的基础上，我们提出测量的面积变化应该由聚合中分子结构变化引起的急剧的瞬时面积变化与随后的与此面积变化相反的弛豫过程两部分组成，并据此提出一种反应动力学模型，此模型与实验结果相当吻合，此模型用于处理聚合速率的紫外光强依赖性，得到聚合速率常数近似与光强成二次幂指数关系；此模型也被用于计算活化面积，发现活化面积为〓，几乎与温度无关。

The activation energy was calculated to be 406 kJ/mol and the rate constants were determined.

测定了各反应条件下的反应速率常数并测得其活化能为406kJ/mol。

To decrease maufacture costs and improve the ratio of efficiency and outlay.The not exensive emulsifier, hydrophobe and other adminicle were mixed with self-made polyesters, siloxane-polyester copolymers to obtain defoamers which be better than imported.And the factors in the process of compound were studied particularly and systemically.the prime project is as follows:the siloxane-polyester copolymer is synthesized with PPG2000,PEG400,1% hydrogen-containing Polyhydrosiloxanes, hexane diacid,which mol ratio of materials is 7:3:6:5.emulsifying agents are SP-60 and tw-60,the value of HLB is 8.5.its dosage is 5%.the concentration of control- bubble resin is 5%. the concentration of liquid hydrocarbon A is 20%.

为进一步降低消泡剂的生产成本，提高其使用时的效费比，采用价格低廉的乳化剂、疏水剂及其他助剂与所制聚醚酯、有机硅改性聚醚酯进行复配，制取了性能优于进口产品的优质消泡剂；并对复配工艺各要素进行了详细、系统的研究；最佳配方为：PPG2000、PEG400、含氢量1%的硅油，己二酸以物质的量之比为7：3：6：5制成的有机硅改性聚醚酯，乳化剂选择SP-60/TW-60组合、HLB值为8.5、用量5%，抑泡树脂用量5%，液态烃A用量20%，液态烃B用量10%，疏水剂用量15%～20%。

In general, the amidation provides the desired amides in high yields using the insoluble base CaCO 3 , TBHP as an oxidant, and a mixture of CuI and AgIO 3 (1 mol %).

一般而言，提供酰胺酰胺在高收益预期使用中亚基地溶性三日tBHP作为氧化剂、混合、崔贴水3(1克分子%)。

The catalytic efficiency of 7a was the best when acetone was used as Aldol donor, and the Aldol products were obtained with up to 78% ee in the presence of 10 mol% 7a.

对丙酮与醛的反应，7a的催化效果最好，在10％催化剂存在下产物ee值高达78％。

When the mol quantity of Cu2+ dissolved was 5% of those of AlCl3 in ionic liquids, alkylation results from ionic liquids is comparable with those obtained with concentrated sulfur acid: the yield of alkylate reaching 178% of the volume of butene inputted, the selectivity of C8 reaching 75% and the octane number of alkylate reaching 92.2.

溶入Cu2+和Cu+后，离子液体的催化性能有显著的改善，当Cu2+的摩尔加入量为三氯化铝的5%时，烷基化油收率达到丁烯体积的178%，对C8的选择性为75%，烷基化油辛烷值为92.2，并且离子液体可以重复使用。

Putt your way through 36 fun-filled holes of minigolf on 3D designed courses with elevated greens, bunkers, bridges and water hazards, among other crazy obstacles.

您的推杆方式，通过36个有趣的填孔迷你的三维设计的课程，以提升绿党，掩体，桥梁和水的危害，除其他疯狂的障碍。

Some participles can be used either as attributes or as predicatives.

有些分词既可当定语用，也可当表语用。