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Results ICD (0.5,5 and 50 μmol/L) caused dose-dependent reduction in the number of osteoclastic bone resorbing lacunae. The inhibitory effect ICD (5 μmol/L) was more remarkable than that of aminopropanediphosphonate. Both ICD and APD reduced the surface area of osteoclastic bone resorbing lacunae.

结果 ICD(0.5，5与50 μmol/L)使体外破骨细胞性骨吸收陷窝数目呈剂量依赖性减少，中等浓度(5 μmol/L)的抑制作用明显高于阳性对照药帕屈磷酸钠，两药均可使吸收陷窝表面积明显降低，而且ICD作用更明显。

Both 200 μmol/L and 100 μmol/L of nicorandil can arrest the dogs heart, which can be resuscitated by reperfusion.

200 μmol/L和100 μmol/L的尼可地尔均可使犬心停跳，再灌注后可复跳。

When the concentrations of tetrabutyl ammonium bromide and KI in solution were 5.0×10^(-4) mol/L and 3.0×10^(-3)mol/L at pH 3.0, Bi(superscript 3+) could be quantitatively separated from Mo, Ga(superscript 3+), Co(superscript 2+), Mn(superscript 2+), Zn(superscript 2+), Rh(superscript 3+), Al(superscript 3+), Cr, V, Ni(superscript 2+), Sn, W and Fe(superscript 2+).

当溶液中溴化四丁基铵和碘化钾的浓度分别为5.0×10^(-4) mol/L和3.0×10^(-3)mol/L和在PH3时，Bi(上标 3+)可与Mo，Ga(上标 3+)，Co(上标 2+)，Mn(上标 2+)，Zn(上标 2+)，Rh(上标 3+)，Al(上标 3+)，Cr，V，Ni(上标 2+)，Sn，W和Fe(上标 2+)定量分离。

Seven biogenic amines were extracted from a sample with 6% perchloric acid, then derivatized with benzoyl chloride. 0.02 mol/L borate buffer (pH 9.2) containing 0.06 mol/L sodium deoxycholate-methanol （95∶5, v/v）was used as a running buffer. The detection wavelength was set at 214 nm. The separation was achieved within 12 min. Good linearities were observed from the calibration plots in the concentration ranges.

样品经6%过氯酸萃取后，由苯甲酰氯衍生化，以含0.06 mol/L脱氧胆酸钠的0.02 mol/L硼酸(pH 9.2)-甲醇(体积比为95∶5)混合液为电泳介质，电泳电压25 kV，温度25 ℃，检测波长214 nm，在12 min内实现了7种生物胺的完全分离。7种生物胺的浓度与其峰面积在一定的范围呈良好的线性关系，检出限除组胺为15 μg/g外，其余均为5 μg/g。

In addition, the constant-volume combustion heat of MPC was determined as -25432.72 J·g~(-1) by a oxygen bomb calorimeter at 298.15 K, and its standard molar combustion enthalpy and standard molar enthalpy of formation were calculated as -3868.92 kJ·mol~(-1) and -422.33 kJ·mol~(-1), respectively.

同时本文测定了MPC的恒容燃烧热为-25432.72 J·g~(-1)，并计算出MPC的标准摩尔燃烧焓为-3868.92 kJ·mol~(-1)及标准摩尔生成焓为-422.33 kJ·mol~(-1)。

To elucidate the biological structure basis of transgenic rice plants expressing maize PEPC gene with high photosynthesis efficiency, PEPC transgenic rice and its wild type with at 3 leaves seedling stage were treated under 1000 μmol/(m^2s) light intensity for 100 min, respectively, and those under 200 μmol/(m^2s) light as the control. The structure of mesophyll cells, bundle sheath and thylakoids of the second blade were observed with a transmission electron microscope.

为了阐明转玉米PEPC基因水稻高光效的结构基础，以转玉米PEPC基因水稻和未转基因原种为试验材料，在水稻的三叶期，施以100min，1000μmol/的高光强处理，以200μmol下的水稻为对照，运用透射电镜观察叶肉细胞、维管束鞘以及叶绿体内类囊体片层结构。

METHODS: The bile was treated with 3 different methods, including the 2D-Clean-up kit group: the bile sample was dissolved with lysis buffer (contains: 7 mol/L carbamide, 2 mol/L thiourea, ammonium persulfate with mass concentration of 0.4 g/L, 65 mmol/L dithiothreitol, carrier ampholytes with mass concentration of 0.2 g/L).

将标本分别按3种不同方法进行处理：①2D-Clean-up试剂盒处理胆汁标本：用裂解液，7 mol/L尿素，2 mol/L硫脲，质量浓度为0.4 g/L的过硫酸铵，65 mmol/L二硫苏糖醇，质量浓度为0.2 g/L的载体两性电解质溶解沉淀过夜。

For the oxidation channel from OH group migration to O atom insertion,the activation energy barriers for OH migration are 58.4,65.3, and 79.2 kcal/mol,respectively,whereas those for O atom insertions beginning with directly destroying Si_a-Si_s backbonds by a foreign H_2O molecule are much lower,the respective values are 19.0,16.7,and 24.8 kcal/mol.

对于先经过OH迁移致使O原子插入Si_a-Si_s backbond的氧化途径，OH迁移所克服的能垒依次为58.4、65.3和79.2 kcal/mol，而H_2O以O原子进攻Si_a位来打开Si_a-Si_s键进而使O原子插入的能垒则相对较低，仅为19.0、16.7和24.8 kcal/mol。

Department of Chemical Pharmacology, Capital University of Medical Science, Beijing 100054, ChinaAbstract: A reversedphase high performance liquid chromatographic method was developed for the simultaneous quantitative determination of caffeine, dapsone and chlorzoxazone. The operation was carried out on a C18 column (250 mmX4.6 mm i.d., 5.0 μm) with the mobile phase of acetonitrilephosphate buffer including 0.02 mol/L KH2PO4 and 0.02 mol/L (C2H53N, pH 6.5(25:75 in volume ratio).

用反相高效液相色谱同时测定血清中咖啡因、氨苯砜、氯唑沙宗探针药物的质量浓度，以乙腈磷酸盐缓冲体系(含 0.02 mol/L的磷酸二氢钾和0.02 mol/L的三乙胺，pH 6.5)(体积比为25：75)为流动相，以安替比林为内标，经C18柱(250 mmX4.6 mm i.d。， 5.0 μm)分离，紫外检测器检测，使3种探针药物得到较好的分离，并且在有效血药浓度范围内线性良好。

Adduct G is isomerized by F. The isomerization energies are relatively high (in the gas phase: 244.77 kJ/mol; in solvent of water: 234.83 kJ/mol), which is consistent with the experiment that adduct F is the primary alkylation product.

加合物G由F异构形成，且有相对高的异构化能（气相：244.77 kJ/mol；水溶剂中：234.83 kJ/mol），这与实验上得到加合物G是主要癌变物的结果一致。

The concept of equivalent rotationally rigidity is offered and the formula of rotationally rigidity is obtained.

主要做了如下几个方面的工作：对伸臂位于顶部的单层框架—筒体模型进行分析，提出了等效转动约束的概念和转动约束刚度的表达式。

Male cats normally do not need aftercare with the exception of the night after the anesthetic.

男猫通常不需要善后除了晚上的麻醉。