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The linear ranges of determination for pyrogallol, phloroglucinol, pyrocatechol, resorcinol and parodioxybenzene were 1.0×10〓~2.0 ×10〓mol l〓, 1.0×10〓~1.0×10〓mol l〓, 1.0×10〓~6.0×10〓mol l〓, 1.0 ×10〓~2.0×10〓mol l〓 and 1.0×10〓~6.0×10〓mol l〓 respectively, and their detection limits were 7.2×10〓mol l〓, 6.8×10〓mol l-1, 2.1 × 10〓mol l〓, 7.1×10〓 mol l〓 and 2.2×10〓mol l〓 respectively.

该方法测定连苯三酚、间苯三酚、邻苯二酚、间苯二酚和对苯二酚的线性范围分别为1.0×10〓~2.0×10〓mol l〓,1.0×10〓~1.0×10〓 mol l〓,1.0×10〓~6.0×10〓mol l〓,1.0×10〓~2.0×10〓mol l〓和1.0×10〓~6.0×10〓mol l〓;检出限分别为7.2×10〓mol l〓、6.8×10〓 mol l〓、2.1×10〓 mol l〓、7.1×10〓mol l〓和2.2×10〓mol l〓。

Differently, the ethanol-precipitates from HWE (HWE-EtOH ppt) were mainly composed of galactose (~38 mol%), followed by arabinose (28 mol%), glucose (~13 mol%), rhamnose (~13 mol%), mannose (~6 mol%), and fucose (~3 mol%).

不同地,HWE经乙醇沉淀物(HWE-EtOH ppt)之单糖组成以半乳糖(37.5 mol%)为主,其次为阿拉伯糖(28 mol%)、葡萄糖(~13 mol%)、鼠李糖(~13 mol%)、甘露糖(~6 mol%)、及岩藻糖(~3 mol%)。

The concentrations of insulin are 0,10~(-9)mol/L, 10~(-8)mol/L, 10~(-7)mol/L; the concentrations of Sodium vandate are 0,10μmol/L,25μmol/L,50μmol/L; the concentrations of AG1024 are 0,1μmol/L, 10μmol/L, 100μmol/L; the concentrations of ursolic acid are 0, 10~(-7)mol/L,10~(-8)mol/L,10~(-9)mol/L.

胰岛素的浓度为0、10~(-9)mol/L、10~(-8)mol/L、10~(-7)mol/L;钒酸钠的浓度为0、10μmol/L、25μmol/L、50μmol/L;AG1024的浓度为0、1μmol/L、10μmol/L、100μmol/L;熊果酸的浓度为0、10~(-7)mol/L、10~(8)mol/L、10~(-9)mol/L。

In addition, when the modified PVA resins fulfilled requirements in the following: 1 the acetalization degree varied from 60 mol% to 80 mol%, 2 the esterification degree varied from 10 mol% to 20 mol%, 3 the amount of hydroxyl group was 5-25 mol%, 4 the range of value of B/P(the mass ratio of the binder to diazo resin) was from 4 to 4.5,5 the range of its molecular weight was from 4×10^5 to 8×10^5, the negative PS plate obtained had excellent sensitivity, hydrophobic property, good developability, good ink receptivity and good scratch resistance.

因此其分子量、酯化度和缩醛度的确定,必须综合考虑各项性能之间的平衡。缩醛度为60-80 mol%,酯化度10-15mol%,羟基5-25 mol%,分子量约为4-8万,B/P为4-4.5时,制得的阴图PS版的感度、显影性、着墨性和耐磨性都较好。

The isopiestic molalities and water activities have been determined for the systems Li_2SO_4-H_2O and Li_2B_4O_7-H_2O at 273.15K in the ion strength ranges of 0.6063~ 1.7640 mol · kg~(-1),and 0.1069—0.6478 mol· kg~(-1) respectively and for the systems Li_2SO_4-H_2O, Li_2B_4O_7-H_2O and Li_2SO_4-Li_2B_4O_7-H_2O at 298.15K in the ion strength ranges of 0.3577—5.6378 mol·kg~(-1), 0.1747—2.4497 mol·kg~(-1), 0.2394—5.5399 mol · kg~(-1) respectively by the isopiestic method using an improved equipment.

本论文利用改进的等压设备和实验方法测定了273.15K下纯盐水溶液Li_2SO_4和Li_2B_4O_7离子强度范围分别为0.6063~1.7640mol·kg~(-1,0.1069~0.6478mol·kg~(-1)以及298.15K下纯盐水溶液Li_2SO_4和Li_2B_4O_7离子强度范围分别为0.3577~5.6378mol·kg~(-1,0.1747~2.4497mol·kg~(-1)和Li_2SO_4-Li_2B_4O_7-H_2O体系混合盐水溶液离子强度范围为0.2394~5.5399mol·kg~(-1的等压平衡浓度和水活度。

The results showed that when 0.3 g of divinyl benzene was used as crosslinking agent, the crosslinking degree increased significantly from 28.26% to 90.95% with the increase of MAA amount from 4.0 mol% to 10.0 mol%, and this increase became slowly as MAA amount was more than 10.0 mol%; the particle volume expansion was increased gradually as MAA amount increased, and reached a maximum of 42.1% when 12.0 mol% of MAA was used, and perfect porous morphology inside particles was observed even when the crosslinking degree reached 95.4% at 14.0 mol% of MAA.

结果表明:在交联剂二乙烯基苯用量一定(0.3 g)的条件下,随着MAA用量从4.0 mol%增加到 10.0 mol%,聚合物交联程度从28.26%迅速增大至90.95%,当其用量超过10.0 mol%后 P x增大趋势变缓;随着MAA用量的增加,处理后胶粒体积膨胀百分率逐渐增大,在MAA用量为12.0 mol%时Δ V 达到42.1%的最大值,当MAA用量增大到14.0 mol%时,尽管 P x高达95.44%,胶粒仍具有完好的孔状结构。

METHODS: While hypoxia-reoxygenation groups were not given any medicine intervention as control, the treatment of xionggui diwan 1×10-6mol/L was subdivided into xionggui diwan 1 × 10-6 mol/L + non-hypoxia and xionggui diwan 1 × 10-6 mol/L + hypoxia groups, and the treatment of xionggui diwan 10 × 10-6 mol/L was subdivided into xionggui diwan 10 × 10-6 mol/L + non-hypoxia and xionggui diwan 10 × 10-6 mol/L + hypoxia groups.

缺氧-复氧前后组分为两个亚组(即缺氧-复氧前、缺氧-复氧后),均不进行药物干预;芎归滴丸1×10-6 mol/L组分为两个亚组(即芎归滴丸1.0×10-6mol/L+不缺氧组、芎归滴丸1×10-6mol/L+缺氧组);芎归滴丸10×10-6mol/L组分为两个亚组(即芎归滴丸10×10-6 mol/L+不缺氧组、芎归滴丸10×10-6mol/L+缺氧组)。

The concentrations of catechol and hydroquinone are linear with the intensity of synchronous fluorescence in the concentration range of 1.0×10^(-6)-9.0×10^(-5) mol/L and 1.0×10^(-6)-1.0×10^(-4) mol/L, with correlation coefficients of 0.998 6 and 0.999 1 and detection limits of 8.2×10^(-7) mol/L and 5.4×10^(-7) mol/L.

邻苯二酚和对苯二酚在1.0×10^(-6)~9.0×10^(-5)mol/L和1.0×10^(-6)~1.0×10^(-4)mol/L浓度范围内与同步荧光强度呈线性关系,相关系数分别为0.9986和0.9991,检出限分别为8.2×10^(-7)mol/L和5.4×10^(-7)mol/L。

The apparent degradation reaction activity energy of PET and PC are evaluated to be 27. 19kJ. mol〓 and 35. 75kJ. mol〓 in system noncritical region respectively. The mass transfer and scatter, which are the controlling factors of degradation in system noncritical region, change into chemical reaction in system critical region, where the activity energy of PET and PC are evaluated to be 89. 79kJ. mol〓 and 80.61kJ. mol〓 respectively.

在系统的非临界区域,PET、PC的降解为液固相反应,反应速率很低,其降解反应表观活化能分别为为27.19KJ.mol〓和35.75KJ.mol〓,为传质、扩散控制;在系统的临界区域,PET、PC的降解为液态均相反应,降解反应速率显著提高,其降解反应表观活化能分别为89.79KJ.mol〓和80.61KJ.mol〓,为化学反应控制。

Diffusion coefficients for metol and p-benzenediol were 2.1×10 cm^2/s and 2.7×10^6 cm^2/s, respectively. The electrocatalysis mechanism has been studied. ATR-FTIR was used for the characterization of the ME/Au SAMs. The oxidation currents were linear in the range of 1.0×10^(-7)~1.0×10^(-4)mol/L for metol and 6.0×10^(-6)~6.0×10^(-4)mol/L for p-benzenediol, with the correlation coefficients of 0. 9992 and 0.9996 by differential pulse voltammetry, and detection limit 2.0×10^(-8)mol/L and 1.2×10^(-6) mol/L for metol and p-benzenediol, respectively.

采用水平衰减全反射-傅立叶变换红外光谱技术对ME/Au SAMs进行了表征,示差脉冲伏安法同时测定米吐尔和对苯二酚,不产生干扰,其氧化峰电流与相应物质的浓度分别在1.0×10^(-7)~1.0×10^(-4)mol/L和6.0×10^(-6)~6.0×10^(-4)mol/L范围内呈良好的线性关系,相关系数分别为0.9992和0.9996,检测限分别为2.0×10^(-8)和1.2×10^(-6)mol/L。

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