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Two new kind of energy transfer donor-acceptor dyads consisting of α-naphthoic acid moiety and 9-aminoacridine units linked by tetraethylene glycol or triethylene glycol flexible chain have been synthesized.

本工作分别用聚三乙二醇及聚四乙二醇柔性链将α-萘甲酸酯与9-氨基吖啶连接起来，合成了两种新型二元发色团分子体系，在两个体系中，选择激发α-萘甲酸酯，都可以发生从α-萘甲酸酯到9-氨基吖啶的高效率的单重态-单重态能量传递。

Heterocyclic compounds contianing oxazole or thiazole moiety are also an important organic fluorescent compounds,which extensively exist in nature compounds and have superior biological activities.

含有噻唑和噁唑母体的杂环化合物广泛存在于天然化合物中，具有很好的生物活性，而且还是一类很重要的有机荧光材料，因而受到广大科学研究者的广泛关注。

Objective Some pentacyclic steroidal analogues with 3-hydroxy-5-ene moiety have been synthesized to evaluate inhibition of VEGF in breast cancer cells.

目的 设计合成一系列具有3-羟基－5-烯骨架的五环甾体骨架衍生物，并测试其抑制乳腺癌细胞新血管生成的活性的抑制作用。

In order to study novel polyquinolines for their applications in the fields of electroluminescent devices and chemosensors, we synthesize polyquinolines containing phenylamine moiety for single-layer LEDs; moreover, we synthesize polyquinolines with different molecular structures to investigate their properties as fluorescent chemosensors.

本论文是以研究新型聚喹啉材料在电致发光和荧光传感器方面的应用为目的，将芳胺基元引入到聚喹啉主链上，以期使聚喹啉可用于单层电致发光器件中；同时通过合成不同分子结构的聚喹啉来考察其作为荧光传感器的性能和规律。

A novel bis (o-aminobenzophenone) s monomer is synthesized, and is used to get three different polyquinolines containing phenylamine moiety through Frieldlander reaction. The solubilities, thermal stabilities and luminescent properties of the polymers were evaluated. All the polymers are thermal-stable, and are soluble in common organic solvents. The emission of their thin film is from excimer emission.

合成了一种新型的二邻氨基二苯酮单体，通过Frieldlander反应，可以构造出不同结构的含有类三芳胺基元的发光聚喹啉，对其溶解性、热性能进行了研究，结果表明这类聚喹啉在常用有机溶剂中的溶解性有了很大提高，同时保持了聚喹啉较高的热稳定性；研究了它们在溶液态和薄膜态的紫外可见吸收光谱和荧光发射光谱，发现它们在薄膜态下的荧光发射主要来自于分子间激基复合物发射。

In order to study novel polyquinolines for their applications in the fields of electroluminescent devices and chemosensors, we synthesize polyquinolines containing phenylamine moiety for single-layer LEDs; moreover, we synthesize polyquinolines with different molecular structures to investigate their properties as fluorescent chemosensors.

中文题名聚喹啉的合成与表征副题名外文题名 Synthesis and characterization of novel polyquinolines 论文作者童辉导师王利祥学科专业高分子化学与物理研究领域\研究方向学位级别博士学位授予单位中国科学院长春应用化学研究所学位授予日期2002 论文页码总数152页关键词发光材料共轭聚合物荧光传感器电致发光聚合物聚喹啉馆藏号BSLW /2003 /O633 /17 本论文是以研究新型聚喹啉材料在电致发光和荧光传感器方面的应用为目的，将芳胺基元引入到聚喹啉主链上，以期使聚喹啉可用于单层电致发光器件中；同时通过合成不同分子结构的聚喹啉来考察其作为荧光传感器的性能和规律。

Thus, the phosphonate moiety is remainedin the products and this methodology can be used in the synthesis of substituted vinylphosphonates.

因此在本烯化反应中保留了膦酸酯基团，可用来合成取代的烯基膦酸酯。

A range of oligoaryls having alternating para- or meta-benzene-furan rings is synthesized by rapid convergent/divergent method from the annlation of a propargylic dithioacetal and an aldehyde having a propargylic dithioacetal moiety as the substituent.

中文摘要结合分流法/汇集法，利用炔丙基硫缩酮单体和另一具有醛基的单体进行环化反应，可以迅速合成对位及间位取代苯环呋喃交错寡聚物。

It can be proposed that when the substituent is an electron donor, the twisted configuration between pyrazoline ring and the moiety attached on N1 is the fluorescence-emitted configuration of 2-pyrazoline, and the configuration where two moieties are placed in a co-plane is the best non-radiative decay configuration of these compounds.

这表明，对于C3位取代基为推电子基或弱的拉电子基团的化合物，N1所联取代基与吡唑啉环相扭曲的构象是化合物的发光构象，两者处于同一平面的构象是化合物的最佳非辐射衰变构象，与C3所联取代基的旋转扭曲无关。

In the third chapter, the synthesis of5-[(1"S)-1",2"-diacetyl-oxyethyl]-1-phenylpyrazol-3-carboxaldehyde oxime(2) from5-[(1"S)-1",2"-diacetyl-oxyethyl]-1-phenylpyrazol-3-carboxaldehyde(1) and phenyl-hydrazine were introduced firstly. The synthesis of nine dioxapyrrolino[3,4-c]pyrazoles containing chiral pyrazolyl moiety(6a-i) from 2 with N-substituted-phenylmaleimide by nonmetal oxidant IBD-initiated intermolecular 1,3-dipolarcycloaddition was described in detail.

第三章首先以5-[(1′S)-1′，2′-二乙酰氧基乙基]-1-苯基吡唑-3-醛(1)和苯肼为原料，合成了化合物5-(1′S)-1′，2′-二乙酰氧基乙基1-1-苯基吡唑-3-醛-苯腙(2)；再用化合物(2)与N-取代苯基马来酰亚胺反应，利用无金属氧化剂—IBD引发1，3-偶极反应，发生分子间的环加成，合成了9种新型手性吡唑连二氧代吡咯啉并

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。