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RESULTS AND CONCLUSION: The course of treatment was 10.4 months, and the velocity of mandibular second molar mesializing was 0.8 mm per month, with 8.5 mm in mesiodistal direction, there was no changes in the vertical direction.

结果与结论:疗程10.4个月,下颌第二磨牙平均移动速度为0.8 mm/月;平均近中移动8.5 mm,垂直向没有变化;磨牙长轴向远中倾斜角度为2.5°,下颌中切牙位置无改变。

Methods HPLC was applied in this study. Kromasil KR100-5C18 (4.6 mm×250 mm, 5μm) column and DAD detector were used with a mixture of methanol and 0.1% methanoic acid as mobile phase in a gradient mode.

采用高效液相色语法,以DAD为检测器,Kromasil KR100-5C18 (4.6 mm×250 mm, 5μm)为分析用色谱柱,甲醇-0.1%甲酸溶液为流动相进行梯度洗脱,建立了玄参药材的指纹图谱。

The separation was achieved within 4 min using a BEH Shield RP18 column (100 mm 2.1 mm, 1.7 μm) with 50 mmol/L monoammonium phosphate solution (pH 6.5) and acetonitrile as the mobile phase.

以BEH Shield RP18柱(100 mm 2.1 mm,1.7 μm)为分析柱,以50 mmol/L的磷酸二氢铵(pH 6.5)和乙腈为流动相进行梯度洗脱,3种磷酸腺苷在4 min内实现了较好的分离。

Methods The HPLC was performed on Lichrospher C18 (200 mm × 4.6 mm, 5μm) column. The mobile phase consisted of methanol and 0.02 molL^(-1) monobasic potassium phosphate buffer (60:40). The flow rate was 1.0 mlmin^(-1). The detection wavelength was set at 333 nm.

以汉邦Lichrospher C18 (200 mm×4.6 mm,5μm)为色谱柱,以甲醇-0.02 molL^(-1)磷酸二氢钾溶液(用磷酸调节pH值至4.2)60:40)为流动相,UV检测波长333 nm,流速1.0mlmin^

Inosine -5'- monophosphate (5'-IMP) and guanosine-5'-monophosphate (5'-GMP) in samples were separated successfully using an Inertsil ODS-3 column (250 mm×4.6 mm, 5 μm) when 0.02 mol/L monopotassium phosphate (pH 4.5) was employed as the mobile phase with a flow rate of 1.0 ml/min at 250 nm and 25℃.

采用Inertsil ODS-3色谱柱(250 mm×4.6 mm, 5μm);以0.02 moL/L磷酸二氢钾溶液(pH 4.5)为流动相,流速1.0 mL/min,柱温25℃,检测波长250 nm,同时分离了样品中5'-鸟苷酸二钠和5'-肌苷酸二钠。

[Objective] To analyze the outcome of internal fixation for occipitalization with atlantoaxial joint dislocation by posterior decompression and occipitocervical fusion [Method] From December 2005 to June 2007,8 patients with occipitalization and atlantoaxial joint dislocation received removal of the posterior arcus of atlas and the enlargement of the posterior edge of the foramen magnum after skull traction performing for an average of 135 daysAll patients were operated on by posterior craniocervical fusion using cervifix internal fixation system and autologous ilium graftsThe clinical efficacy after operation was analyzed by Japanese Orthopaedic Associationneural function score [Result] All the patients were followed up from 6 months to 2 years, average of 15 monthsNo complication was foundAtlantodental interval was 5~9 mm before and 4~6 mm after skull tractionAtlantoaxial joint dislocation didn't completely reducedThe neurological defects were improved to some extents according to the JOA scoreImageology showed all patients had full decompression and bony fusionThe loosening or broken internal fixation was not found [Conclusion] Posterior decompression and fusion is a feasible method for the treatment of occipitalization with atlantoaxial joint dislocation,and the clinical effect is satisfactory

分析后路减压枕颈融合内固定术治疗合并寰枢关节脱位的寰椎枕骨化临床疗效。[方法]2005年12月至2007年6月间,对8例合并寰枢关节脱位的寰椎枕骨化患者在行颅骨牵引治疗一段时间(12~16 d,平均135 d)后采用枕骨大孔后缘扩大,寰椎后弓切除减压取自体髂骨枕颈融合Cervifix系统内固定术,手术后采用日本骨科学会神经功能评分分析临床疗效。[结果]8例患者随访6个月~2年,平均为15个月。8例患者无一例出现术后并发症,术前寰齿前间隙为5~9 mm,经颅骨牵引后为5~7 mm,寰枢关节脱位未能完全复位。手术前后JOA评分示神经症状均有不同程度恢复,影像学检查示枕颈区减压充分植骨区获得骨性融合,无一例出现内固定松动或断裂。[结论]合并寰枢关节脱位的寰椎枕骨化患者术前仔细评估影像学改变,采用颅骨牵引一段时间后行后路减压枕颈融合内固定术的治疗方案是合理可行的,且临床效果满意。

The separation was performed with a DiamonsilTM ODS C18 4.6 mm×200 mm, 5 ?

反相高效液相色谱法,采用DiamonsilTM ODS C18 4.6 mm×200 mm, 5 ?

The mean outer diameter of the cup was 52 mm (range, 48 to 62 mm). Osteolysis progressed in sixteen (53%) of the thirty hips.

臼杯的平均外径是52 mm(48 ~62 mm)。30例中有16例骨溶解加重。

Methods Rhizoma Gastrodiae, Pellis Ovis, and Calculus Bovis Sativus in Tianhuang Houzao powder were identified by TLC. The content of Gastrodin in the powder was determined by HPLC. The HPLC condition was as follows: column was Phenomenex C18 (4.60 mm×250 mm, 4 m), the mobile phase consisted of methanol-0.05% phosphoric acid (3:97), the UV detection wavelength was at 220 nm, the flow rate was 1.0 ml/min with column temperature at 25℃.

用薄层色语法鉴别天黄猴枣散中天麻、猴枣、体外培育牛黄;用高效液相色谱法对制剂中天麻素进行定量分析,Phenomenex C18 (4.60 mm×250 mm, 4 m)色谱柱,流动相为甲醇-0.05%磷酸溶液(3:97);检测波长220 nm,流速1.0 ml/min,柱温25 ℃。

METHODS: Puncture with the needle retaining in the cavity of knee of normal adult corpse without effusion or pneumatosis was performed, and 1, 5, 10, 15, 20, 30, 40 mL contrast-medium was injected into the cavity. Coronal section, vertical plane and transect were scanned with T2WI, 4 mm thickness and 1 mm interval by MRI.

对10件无积液、积气、结构正常的成人尸体膝关节腔内穿刺留针,通过穿刺针向关节腔内依次注入1,5,10,15,20,30,40 mL对比剂,分别于每次注射后行冠状面、矢状面、横断面T2WI,厚度4 mm,间距1 mm,MRI扫描。

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