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The optimum condition of preparing process were obtained: the amount - of - substance ratio of sodium hydroxide and eerie sulfate tetrahydrate was 4.8:1 ,the quantity of PEG was 8 mL in reaction and 7 mL in washing, absolute alcohol was 10 mL in washing, irradiation time was 6 min, constant microwave irradiation pressure was 0.14 MPa, microwave power was 232 W, the ultrasonic wave dispersing time was 10 min and the microwave drying time was 10 min.
通过考察制备过程中的各个影响因素,得到了制备纳米二氧化铈的最佳工艺条件:氢氧化钠与四水硫酸高铈物质的量比为4.8:1;聚乙二醇的反应用量为8mL,洗涤用量为7mL;无水乙醇的洗涤用量为10mL;微波恒压时间为6min;微波压力为0.14MPa;微波功率为232W;超声波分散时间为10min;微波干燥时间为10min。
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The optimal chromatographic conditions as following: velocity of nitrogen, hydrogen and air is 35ml/min,25 ml/min, and 300 ml/min respectively; temperature of column and vaporing chamber is 45,100 respectively; temperature of detector is 120℃.
对所制柱子的色谱条件进行系统研究表明,该柱使用温度低,使用温度范围20℃-48℃,可进行常温分析。
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Optimal reaction conditions were as follows: PAAS and SMA at weight ratio of 4:1, stirring for emulsifying at speed of 1500 rpm and last 60 min, acidifying for 90 min, and the curing temperature under 50℃for 90 min.
优化配方及工艺条件为:聚丙烯酸钠和苯乙烯-马来酸酐按4:1混合作乳化剂,1500rpm搅拌,分散乳化60min,酸化90min,50℃固化90min作为制备二甲戊乐灵微胶囊的优化工艺条件,在此条件下可以得到平均粒径为9.6μm、粒度分布均匀、包封率在99%以上的球形微胶囊。
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After dialyzing for 10~20 min, SNP at a concentration of 1 μmol/L increased the induced responses to innocuous mechanical stimulation and decreased those to noxoius mechanical stimulation. The induced responses to both innocuous and noxious mechanical stimulations were all decreased after dialyzing the same dose of SNP for 20~30 min. The decrease was shown within 7~15 min dialysis when SNP was used at a concentration of 20 μmol/L.
脊髓深层神经元透析1 μmol/L SNP, 10~20 min后,非伤害性机械刺激诱发的反应增强,伤害性机械刺激诱发的反应减弱;透析20~30 min后,伤害性和非伤害性机械刺激诱发的反应均减弱;透析20 μmol/L SNP 7~15 min内伤害性和非伤害性机械刺激诱发的反应均降低。
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The organic layer was evaporated and the residue was redissolved by mobile phase.The concentrations of propofol and lidocaine were assayed on a hypersil BDS C18 column with a mobile phase consisting of acetonitrile-methanol-water(10∶60∶30)(including 0.14%n-butyamine 0.1%acetic acid)at a flow rate of 1 mL*min-1 and detected at 220 nm during 1~7 min and at 273 nm during 7~16 min.
氮气吹干有机层,残留物用流动相重新溶解后,用Hypersil BDS C18柱分析,流动相为乙腈-甲醇-水(10∶60∶30),内含正丁胺0.14%和冰醋酸0.1%,流速为1 mL*min-1,检测波长:1~7 min用220 nm,7~16 min用273 nm。
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Helium was used as the carrier gas under a constant pressure of 206 kPa. The oven was programmed at a rate of 5 ℃/min from 90 ℃(held for 5 min) to 280 ℃(held for 5 min).
载气为氦气,恒压,柱前压206 kPa;进样器温度250 ℃;柱箱初始温度为90 ℃,保持5 min,以5℃/min的升温速率升至280 ℃,保持5 min。
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The TEO was 7.5 ± 5.0 min in Group 1,8.2 ± 5.0 min in Group 2, and 9.8 ± 4.0 min inGroup 3.
组1的 TEO 是7.5±5.0分钟,组2的为8.2±5.0 min ,组3的为9.8±4.0min。
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Objective To investigate the effect of 17β-estrogen(E2), simvastatin and verapamil-nitrogtycerin solution on the synthesise of NO in human umbilical vein cells. Methods HUVECs were treated with 17β-E2, simvastatin and V-G solution for 30 min, 60 min and 120 min, respectively.
目的 观察17β雌二醇(E2)、辛伐他汀和异搏定一硝酸甘油复合溶液在短时间内对体外培养的人脐带静脉内皮细胞合成一氧化氮功能的影响。
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By using TG analysis, the combustion characteristics of cooking oil tar in pipes were studied under heating rates of 5℃/min, 15℃/min and 25℃/min respectively.
采用热重分析法对餐饮业油烟道油垢的燃烧过程进行实验研究和理论分析,分别在5,15,25℃/min升温速率空气气氛中,研究油烟道油垢的燃烧特性以及升温速率对着火温度、可燃性指数的影响。
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Results showed that, the specific refining energy consumption is decreased with increment of rotation speed of the primary refiner. At freeness level of about 670 mL CSF, for example, the specific refining energy consumptions is 363 kWh/t o.d. at 3000 r/min, and 305 kWh/t o.d. at 3500 r/min, which is equivalent to 16% energy saving, furthermore the specific energy consumption is only 265 kWh/t o.d. at 4000 r/min, which means 27% less refining energy required. At the same time, pulps produced at higher refiner speed have higher strength properties and lower shives contents. There is little change of optical properties of the pulps.
结果表明:小叶桉物料在相同条件下进行汽蒸、挤压和化学预浸渍后,分别采用3500 r/min和4000 r/min的盘磨转速进行第一段磨浆,浆料磨至游离度670 mL时所需磨浆电耗与3000 r/min时的相比,分别下降16%和27%;浆料中纤维束含量分别降低20%和35%;第一段磨后浆料再分别经相同盘磨转速(3000 r/min)的后续磨浆后,与相近游离度的浆料性能比较可知,随第一段磨浆盘磨转速的提高,浆料的细小组分含量略有增加,纤维束含量显著降低,强度性能有不同程度的改善,但光学性能变化不显著。
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- 推荐网络例句
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The circulation, consumption and reproduction of the trilogy have not only testified to its historical significance and literariness, but also invested it with new meanings.
该三部曲的流通、消费与再生产不仅验证了其历史意义及文学性,而切还赋予它以新的意义。
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If he thought that he could buy me off, he would be wrong.
如果他认为他可以收买我,那他就大错特错了。
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Can I be excused today's lesson?
我可以不上今天的课吗?