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The conditions was as follows: Maxima 820 workstation,Hypersil column ODSC_(18)(4.6mm×200mm 5μm),UV detective wavelength 247nm,Flow rate 1.0ml/min,sensitivity 0.01 AUFS Mobile phase is composed of acetonitrile,H_2O,methanol(45:55:1).By which the inerference of impurity may be avoided and there is a good linear relationship between concentration and peak area.

本文建立了体内外氟比洛芬样品的HPLC测定方法:色谱柱:4.6mm×200mm Hypersil ODSC_(18)(4.6mm×200mm 5μm,)紫外检测波长247nm;流动相为乙腈:水:甲醇=45:55:1,流速:1.0ml/min;柱温:室温;灵敏度:0.01AUFS,进样量:20μL,该法可将氟比洛芬与杂质分离,浓度与峰面积之间呈良好的线性关系,满足分析要求。

Methods A gastric barostat was used to study, in healthy subjects, the effect of motilin (300 ng/kg/30 min I) or saline on fasting gastric fundus tone and on post-prandial relaxation.

使用胃恒压器研究正常对象中胃动素(300 ng/kg/30 min I)或盐水对空腹胃底张力和餐后舒张的影响。

BP, SpO2, EKG, PETCO2, cerrical contraction , fetal cardiac sounds were monitored continuously in the perinatal analgesia pe riod. The analgesia effects were determined by giving a mark for pain by VAPS, motor nerve blockings were given amark by Bromage scale; Apgar scale were conduc ted 1-5 min after neonates were labored out.

围分娩镇痛期连续监测血压、脉氧饱和度(SpO2)、EKG、PETCO2、宫缩及胎心音,记录产程时间;镇痛效果采用 VAPS 评分法进行疼痛评分,运动神经阻滞以 Bromage分级评分;新生儿出生后1~5 min进行 Apg ar评分,分娩后24 h新生儿 NACS评分。

Methods: Twenty ASA Ⅱ~Ⅲ patients aged 28~69 years were randomly divided into 2 groups:(1)3-mins group (n=10).(2)8 deep breathings group (8DB). Arterial blood samples were drawn with a fraction of inspired oxygen of 0.21for arterial blood gas analysis. Before induction of anesthesia, patients in 3 mills group were asked to breathe normally for 3 mins during which 100% oxygen at 10 L/min through an anesthesia mask attached to a circle system with soda lime was adopted, and adjustable pressure limiting valve was kept open.

20例气管插管患者随机分为吸氧去氮组(3MIN组)与60s深呼吸8次组(8DB组),入手术室后在呼吸空气情况下采集动脉血气标本测定血气分析,并记录SpO2值。3MIN组采用完全密闭面罩,氧流量10L,麻醉机活瓣旋开以15次/min频率自然呼吸3min.8DB组在相同条件下在60s内深呼吸8次。

The results indicated that water soluble curcuma colourant can be used in silk dyeing and the better dyeing condition was as follows: pH=3, 80℃, 50~60 min, the dosage of colourant was 8%, and the colourant has good building up property for silk.

试验结果表明,水溶性姜黄色素可用于真丝染色,较佳的工艺条件为pH=3、80℃、50~60 min、色素用量8%,色素对真丝具有较好的提升性。

Experimental results showed that AB-8 resin possesses higher absorption and desorption capacity. The appropriate adsorption conditions were: the range of the sample concentration was 0.6~1.0mg/ml, pH was 4.28 or so and velocity of flow was 3ml/min. When 95% ethanol was used as eluant, the desorption capacity was 97%, and 4 BV eluant could desorb FSPV basically.

结果表明:AB-8树脂对FSPV有较好的吸附和解吸效果;其吸附FSPV适宜的条件为:上样液浓度0 6~1.0mg/mL,pH值在4.28左右,上样流速3ml/min;用95%乙醇洗脱时,解吸率达96.78%,4BV洗脱液基本上能将FSPV洗脱下来。

ResultsThe results showed that the best separating conditions were 150 times of 1% ammonia hydrate as eluant, and the elution velocity was 5.0ml/min.

结果在考察范围内,最佳分离条件为:150倍量1%氨水,洗脱速度5.0 ml/min。

D., 5 μm. The flow rate was set at 0.8mL/min and the eluent was detected at 340 nm for the four flavonoids.

选择Venusil ASB C18色谱柱(150 mm×4.6 mm,5μm),流速为0.8 mL/min,检测波长为360 nm,柱温为35℃。

Detection was carried out at the wavelength of 230 nm. Different composition mixtures of methanol and water were used as eluents with a mobile phase flow rate of 0.8mL/min.

紫外检测波长230nm,流动相为甲醇和水混合物,流速为0.8mL/min,采用梯度洗脱方式进行分析。

The results showed that DPPH eluted as a sharp peak at 3 min or so.

实验结果表明:DPPH自由基在3 min左右出峰。

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However, as the name(read-only memory)implies, CD disks cannot be written onorchanged in any way.

然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口,替代木托盘,免薰蒸,符合欧盟、北美各国对出口货物包装材料的法令要求;喷涂钢托盘适用于重载上货架之用,托盘表面根据需要制作成平板状、波纹状及间隔形式,满足不同的使用要求。

A single payment file can be uploaded from an ERP system to effect all pan-China RMB payments and overseas payments in all currencies.

付款指令文件可从您的 ERP 系统上传到我们的电子银行系统来只是国内及对海外各种币种付款。