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The optimum extraction conditions were summed up as follows through orthogonal test: 60 % methanol solution as solvent, lixiviating temperature at 60 ℃ and 40 min lixiviating time, the ratio of raw materials to liquid as 1∶40, and lixiviating twice.

正交试验表明,采用60 %甲醇溶液作为溶剂,最佳提取条件为浸提温度60 ℃,浸提时间40 min,料液比为1∶40,浸提2次。

However, the centralized CFAR detection and Min-OS are heavily influenced by the variation and mismatching of .

然而集中式 CFAR 检测和 Min-OS 受变化或失配的影响非常严重。

Methods by using a broad pH range column(Gemini NX C18,4.6mm×150mm,5μm),basic mobile phase which was[H_2O-ammonia-glacial acetic acid] (96:3.6:0.4)-methanol,the related substances in etimicinsulfate were separated and detected by electrospray ionization and positive ion monitoring,the ESI ion source condition was following: temperature is 350℃,nebulizing pressure is 50 psi,dry gas flow is 10 L /min.some related substances in etimicinsulfate were identified by comparing the retention time in chromatography,~+ spectrum and MS~2 spectrum with reference substances\',the others which haven\'t reference substances were identified or speculated by analyzing their MS~2 fragmentation with the help of a rule summarized from the MS~2 fragmentation of gentamicin C1a,micronomicin and etimicin.Results nineteen related substances in etimicinsulfate were separated and detected.

方法利用宽pH范围的Gemini NX C18(4.6mm×150mm,5μm)色谱柱,在碱性条件下,以[水-氨水-冰醋酸(96:3.6:0.4)]-甲醇(70:30)为流动相,直接分离各组分;并用HPLC-ESI-MS~2检测样品中各组分,质谱条件:ESI离子源,离子源温度350□,雾化室压力50 psi,干燥气流速10 L/min,正离子检测方式;对有对照品的有关物质采用比对有关物质与对照品的色谱保留时间、准分子离子的质荷比及二级质谱方法进行鉴定,无对照品的有关物质,则是先通过解析庆大霉素Cla、小诺霉素、依替米星的二级质谱,对该类化合物的二级质谱裂解规律进行归纳,并以此推测未知新化合物进行结构,再用推测的结构对二级质谱进行解析,如所有的碎片离子均合理解释,表明推测合理。

HCRT potentiates NMDAR-mediated somatic release from LC neuronsApplication of 100μM NMDA evoked a pronounced secretion.This response to NMDA was subsequently enhanced by treatment with 100 nM HCRT for 5 min.

HCRT增强LC神经元NMDA受体介导的胞体递质分泌给予100μM NMDA可以显著引起分泌信号,随后用100 nM HCRT处理5 min,再次给予100μM NMDA可引起更大的分泌信号(增加大约40%)。

Result: 7 examples : normal electrocardiogram,3 examples : mostly normal electrocardiogram( namely the sinus moves soon: Heart rate 101 ~ 120 times/ min),1 many hairs building pulsates to lack the blood with 1 myocardial early.

结果:正常心电图7例,大致正常心电图3例(即窦性心动过速:心率101~120次/min),1例频发房性早搏和1例心肌缺血。

For the determination of five carbamate pesticide residues by high performance liquid chromatography with gel permeation chromatography purification, sample was extracted with acetonitrile and purified with gel permeation chromatography. Methanol-water was used as the mobile phase by gradient elution, flow rate of 1.0mL/min, using a fluorescence detector and quantitating with external standard method.

凝胶渗透色谱-液相色谱法测定5种氨基甲酸酯类农药残留中,实验采用乙腈提取,凝胶渗透色谱柱对样品进行净化,以甲醇-水为流动相,进行梯度洗脱,流速1.0mL/min,荧光检测器检测,外标定量测定。

For the extraction process, selecting 50% ethanol as solvent, controlling the solid-liquid ratio 1:15, reflexing twice in 80℃ water bath and each time for 120 min, the yield of total saponins reached 12.17 mg/g raw material.

在提取过程中,优化的工艺参数为:以50%乙醇为溶剂,控制固液比1:15, 80℃水浴提取2次,每次120 min,此条件下总皂苷得率1.217%。

Skin gelatin hydrolysate from tilapia was produced by thermal hydrolysis with a retorting treatment (at 121℃ for 30 min) and the SGH showed noticeable α,α-diphenyl-β-picrylhydrazyl free radical scavenging and lipid peroxidation inhibition.

高温热水解(121℃, 30 min)所生成的吴郭鱼之鱼皮明胶水解物(skin gelatin hydrolysate, SGH),我们发现具有清除α,α-diphenyl-β-picrylhydrazyl自由基与抑制油脂自氧化的能力。

Peltophorum dubium seeds provided by Anhembi, SP were scarified in 98% H2SO4 for 15 min to overcome mechanical dormancy.

实验所用巴西盾柱木种子由圣保罗州Anhembi公司提供,种子经由98%的浓硫酸预处理15 min,以打破物理休眠。

The optimal gas flow rate was from 25 to 50 mL/min. The solvent flux increased linearly with transmembrane pressure and the separation factor was almost constant under experimental conditions with gas sparging.

适宜的空气流量为25~50 mL/min;在气体鼓泡的情况下,溶剂透过率随操作压强线性地增加,而分离因数不受操作压强影响。

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However, as the name(read-only memory)implies, CD disks cannot be written onorchanged in any way.

然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口,替代木托盘,免薰蒸,符合欧盟、北美各国对出口货物包装材料的法令要求;喷涂钢托盘适用于重载上货架之用,托盘表面根据需要制作成平板状、波纹状及间隔形式,满足不同的使用要求。

A single payment file can be uploaded from an ERP system to effect all pan-China RMB payments and overseas payments in all currencies.

付款指令文件可从您的 ERP 系统上传到我们的电子银行系统来只是国内及对海外各种币种付款。