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With common pakchoi as the material, they were soaked in mixed solution with 1000 times of methyl parathion, dimethoate, dichlorvos, pyralid treat phosphorus, poison-to-death barnyard grass and fenvalerate for 1 min, and then they were saved in CW(25℃, humidity 55%RH), LC(4 ℃, humidity 60%RH) and DW (-24 ℃, humidity 70%RH) after air dried. After saved for 0, 24, 48 and 72 h, the samples from which were taken to determine the residual quantity of pesticides in pakchoi of different treatments.
方法]以普通小白菜为材料,将其在1000倍甲基对硫磷、乐果、敌敌畏、治螟磷、毒死稗和氰戊菊酯的混合稀释液中浸泡1 min,取出晾干后分别在CW(25℃,湿度55%RH)、LC(4℃,湿度60%RH)和DW(-24℃、70%RH)条件下保存,0、24、48、72 h后分别取样,测定各处理小白菜中农药的残留量。
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Methods: A Diamonsil C18 column was used with the mobile phase of 0.1% ammonium acetate solution-methanol (10:90) at the detection wavelength of 240 nm. The flow rate was 1.0 mL/min. Benzyl benzoate was used as internal standard.
采用Diamonsil C18柱,流动相为0.1%乙酸铵溶液:甲醇(10:90),流速1.0 mL/min,检测波长240 nm,以苯甲酸苄酯为内标。
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The HPLC finger print of TGDGBX was set up by HPLC-DAD: the chromatographic column,Diamonsil C18(250 mm×4.6 mm, 5μm, 30℃)and bidimensional gradient elution using methyl cyanide-water (flowing speed 1.0 mL·min-1,λ=203 nm). 180 Wistar rats were randomly divided into normal control group, model group, cortisone group, and TGDGBX (16,32 and 64 mg·kg-1) groups respectively.
采用HPLC-DAD,Diamonsil C18色谱柱(250 mm×4.6 mm, 5μm),乙腈―水二元梯度洗脱,流速1.0 mL·min-1,(λ=203 nm),柱温为30℃,建立了当归补血总苷的HPLC指纹图谱。180只Wistar大鼠随机分为正常对照组、模型对照组、强的松组和当归补血总苷大、中、小剂量组,每组30只。
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The Michaelis-Menten constant of xylanases in the enzymatic hydrolysis of birchwood xylan is 5.37g/L, and the maximal reaction velocity is 0.94μmol/min.
该木聚糖酶作用于Birchwood木聚糖的米氏常数为5.37g/L,最大反应速率为0.94μmol/min。
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The results showed that the liquid medium supplemented with sucrose 150 g· L-1+ 20 mg·L-1 boracic acid + 30 mg· L-1 chloridize calcic and TTC and the dyeing time of 30~35 min were suitable for the pollen germination.
结果表明:金娃娃萱草花粉萌发的适宜液体培养基为蔗糖150 g.L-1+硼酸20 mg.L-1+氯化钙30 mg.L-1;适宜的染色剂为TTC,染色时间为30~35 min。
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Ultra-clean air flow rate of 24 ~ 30m/min, which are adequate to prevent possible harassment in the vicinity of air pollution caused by such a flow will not impede the use of alcohol lamp or Bunsen burner burning disinfection of equipment and so on.
超净空气的流速为24~30m/min,这已足够防止附近空气可能袭扰而引起的污染,这样的流速也不会妨碍采用酒精灯或本生灯对器械等的灼烧消毒。
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The effects of acidity, reaction temperature, feeding mode, and rotational speed of the stirrer on the particle size of AC blowing agent were studied. The optimal conditions were obtained as follows: the catalyst composed with m:m(V2O5)=1:1 equal to 1%-2% ratio of the reagent''s mass,reagent reacts at 50℃ under pH=3-4 for 25min with 350~360r/min of the stirrer speed, and the NaClO3 solution must be added from burette.
研究了酸度、反应温度、加料方式、搅拌器的转速对AC发泡剂粒径的影响,最佳工艺条件为:催化剂m:m(V2O5)=1:1的质量约为反应物质量的1%~2%,反应体系的pH值3~4,反应温度控制在50℃左右,氯酸钠溶液(质量分数20%)采用通管滴加的方法加入,整个反应时间约为25min,搅拌器的转速一般控制在350~360r/min。
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The quantity of catalyst was equal to 0.6% of feedstocks,the reaction temperature was 78~110 ℃,and the reaction time was 45 min. The test results have shown that H_4SiW_(12-O_(40)/MCM-48 is an excellent catalyst for synthesizing butanone 1,2-propanediol ketal with its yield reaching over 91.9%.
实验表明:H4SiW12O40/MCM-48是合成丁酮-1,2-丙二醇缩酮的良好催化剂,在n∶n(1,2-丙二醇)=1∶1.6,催化剂用量为反应物料总质量的0.6%,环己烷为带水剂,反应时间45 min的优化条件下,丁酮-1,2-丙二醇缩酮的收率可达91.9%。
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The optimum conditions were determined as follows:the molar ratio of butyraldehyde to glycol was 1∶1.6,the mass ratio of catalyst to reactants was 0.4%,the volume of cyclohexane as the water-carrying agent was 10 mL,and the reaction time was 60 min.
结果表明,磷钨钼杂多酸对合成丁醛乙二醇缩醛有较好的催化活性,适宜的反应条件如下:n∶n=1∶1.6、催化剂用量为反应物料总质量的0.4%、带水剂环己烷用量为10 mL、反应时间为60 min。
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When pH is 10, adsorption time is 30 min, dosage of bone char is 0.6 g/L, the original concentration of As in drinking water is 0.5 mg/L, As removal can reach 95.2%. The adsorption behavior is fitted both with Langmuir and Freundlich isotherm. The adsorption mechanism is supposed to be Ca—OH functional groups combined with anion. And there may occur the co-precipitation between calcium hydrogen arsenate and hydroxylapatite in the aqueous solution, and ions also exchange. The saturation adsorption capacity of As reaches 4.688 mg/g. Indexes of effluent are in good agreement with the WHO stringent drinking water standards (0.01 mg/L).
研究结果表明:在pH=10,吸附时间为30 min和骨炭加入量为0.6 g/L,饮用水砷初始质量浓度为0.5 mg/L时其砷去除率可达95.2%;骨炭吸附砷的行为同时符合Langmuir和Freundlich等温吸附模型;其吸附机理可能是Ca—OH官能团结合HASO4阴离子,并产生砷酸氢钙和羟基磷灰石的共沉淀,另外还存在离子交换作用;吸附柱的饱和吸附容量为4.688 mg/g;出水砷浓度符合世界卫生组织规定饮水砷标准(0.01 mg/L)。
- 推荐网络例句
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On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.
另一方面,更重要的是由于城市住房是一种异质性产品。
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Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.
气候直方图是将所收集的降水量测定值,分为几个相等的区间作为横轴,并将各区间内所测定值依所出现的次数累积而成的面积,用柱子排起来的图形,也叫做柱状图。
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You rap, you know we are not so good at rapping, huh?
你唱吧,你也知道我们并不那么擅长说唱,对吧?