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The results show that optimum technological parameter of preparing Fe304 magnetic particles is reactive temperature 60℃,mixing speed 700r/min and reactive time 2.5h.when the reactant ratio and molarity remain constant.

实验结果表明,在反应物料配比及摩尔浓度一定的条件下,制备Fe_3O_4磁粒子理想的工艺参数为:反应温度60℃、搅拌速度700r/min、反应时间2.5h。

It was found that introducing 15 g/L additive containing 1.5 g saccharin helped to well retard electropolishing-induced corrosion of the electropolished improve the quality of the electropolished moldboard surfaces. At the same time, it was feasible to realize satisfactory precision electropolished of the laser moldboard made of stainless steel at a current density of 20~25 A/dm^2, duration of 1 min, and temperature of 60~65 ℃. The resulting polished moldboard had smooth walls and bright surface, while the corrosion was less than 0.005 mm.

结果表明,添加剂含量在15 g/L时能有效抑制抛光的腐蚀量,提高抛光质量;在精抛光的参数电流密度为20~25 A/dm^2,温度60~65℃,时间1 min条件下,钢片经去毛刺处理和精抛光处理能达到孔壁光滑、腐饮量小于0.005 mm的要求。

Monosaccharide Ca+, mobile phase of degassing water;flow rate of 1.0 ml/min.

Monosaccharide Ca+;流动相:脱气水;流速:1.0 ml/min。

A549 cell line was stimulated with LPS (10 μg/mL) and then treated with Rs504393 (10 μg/mL) for 6 hours. ALI model was established with intranasal administration of LPS (5 mg/kg) in C57BL/6J mice. RS504393 (5 mg/kg) was administered 30 min before LPS dripped nasally. IL-8, IL-1β, plasminogen activator inhibitor-1, monocyte chemoattractant protein-2, and the expressions of CCR1 and CCR2b were studied by using Realtime-RT-PCR, ELISA and cyto-flowmetry.

体外实验选用A549细胞系,应用LPS(10μg/mL)刺激合并RS504393(10μg/mL)治疗6 h后,流式细胞仪技术检测CCR1和CCR2的表达,ELISA法检测细胞培养上清液内白介素-8的浓度;体内实验选用C57BL/6J小鼠,腹腔注射RS504393(5 mg/kg)预处理30 min后经鼻滴入JPS(5 mg/kg),LPS刺激4 h后收集BALF和肺脏标本,计数BALF内细胞总数,应用BCA法检测BALF内蛋白浓度,Realtime-RT PCR和ELISA法检测BALF和肺脏IL-1β、凝血酶原激活物抑制物-1和单核细胞趋化蛋白-2的表达。

While the rotational speed of cylinder in the range of 15~25r/min,the optimum negative differential pressure and suction angle are in the range of 2.8~3.0kPa and 25.5~36.5° and the single pickup ratio can reach 94~97%.

滚筒转速在15~25r/min范围内,排种器合理负压差和吸种角范围分别为2.8~3.0kPa、25.5~36.5°,合格指数能达到94~97%。

Min-1.ConclusionIt has good effect to separate total alkaloids from embryo of Nelumbo nucifera gaertn seed by macroporous resin DA201 which can be used for a long time. There is preferable industrialized foreground.

min-1。结论DA201大孔吸附树脂对莲心总碱的分离纯化效果良好,树脂使用寿命长,具有较好的工业化前景。

Net tonnage is 2,200 tons. The twin screw propellers are inward. The revolutions at full speed are 106 r/min.

总吨12000吨,净吨2200吨,双螺旋桨推进时内旋,全速前进为106 r/min 。

The contact time after adding neutralizer was 10 min.

加中和剂后作用10 min。

The conclusions were as follows: theνO-H andνC=O IR absorption maxima shifted towards higher wave numbers after imprinting 17β-estradiol on TFMAA-co-TRIM copolymer with the red shift of theνO-H groups being apparent after precipitation polymerization for 16h while that forνC=O groups being observed after polymerization for 24h. A strong interaction between TFMAA and 17β-estradiol was confirmed by the high selectivity for 17β-estradiol, as indicted by the values of the separation factor of isomers of 17β-estradiol/17α-estradiol (2.28) and the imprinted factor (3.01). Particle diameter of TFMAA-co-TRIM polymer was between 300 nm and 1.5μm, which suited well for solid phase sorbent throughout at low column pressure. The recognition of imprinting TFMAA-co-TRIM polymer for sterol molecules was driven by enthalpy eluted with acetronitile, and low temperature was in favor of the separation of sterol structure analogues on imprinting column. TFMAA-co-TRIM polymer possessed of determinate anti-heat stability, with melting point beginning at 255.84℃, Tp=257.40℃, control TFMAA-co-TRIM polymer and imprinting TFMAA-co-TRIM polymer were respectively decompounded at 267.79℃and 343.11℃, and solid micro-extraction noddle prepared by the special polymerization also showed definite recognition for 17β-estradiol by GC/MS detecting at 270℃. By selection of various washing and elution solvents, elution reagents of close polymerization system were of more advantage in template molecules retention and recognition on molecularly imprinted solid phase extraction column. At a certain extent, progesterone, 17α-estradiol, 17β-estradiol and 4-androstene-3, 17-dione could be intercepted on the MISPE column. Especially, MISPE had high selectivity for progesterone, and imprinting TFMAA-co-TRIM polymer could achieve adsorption balance within 50 min by absorption kinetics test for 17β-estradiol. However, MISPE column showed better selectivity and enrichment property for 17β-estradiol than C18 and CSPE columns according to the data from HPLC and GC/MS analyses. Recovery of 17β-estradiol on MISPE column was up to 85.5% while when prime extracting solution of milk powder was sampled, the recovery of CSPE and C18 columns were 43.7% and 30.7%, respectively.

通过研究阐明:紫外聚合产物TFMAA-co-TRIM中的νO-H振动吸收峰在聚合16h后红移,νC=O振动吸收峰在聚合24h后红移;TFMAA-co-TRIM对雌二醇异构体的印迹因子达到了3.01,α为2.28,优于其它功能单体参与得到的聚合物识别特性;TFMAA-co-TRIM聚合物粒径介于300 nm至1.5μm之间,作为色谱固定相具有良好的通量和低的柱压;在乙腈流动相中,TFMAA-co-TRIM分子印迹固定相的分离过程主要被焓驱动,低温有利于分子印迹固定相分离甾醇结构类似物;TFMAA-co-TRIM分子印迹聚合物在255.84℃时开始熔融,Tp=257.40℃,聚合物CP的降解温度在267.79℃,MIP降解温度在343.11℃,制备的固相微萃取头初步经GC/MS 270℃的耐热性测定;不同的洗提溶剂筛选证明了选择接近聚合溶剂的洗脱体系更有利于MISPE发挥识别效应;分子印迹固相萃取柱对孕酮、17α-雌二醇、17β-雌二醇和雄烯二酮都具有不同程度的保留特性,可作为此类化合物的吸附材料,特别对孕酮强保留的富集特性,可作为孕酮的选择性识别吸附剂,其分子印迹聚合物对17β-雌二醇的吸附动力学测定显示在50 min内基本达到吸附平衡,具有作为传感器核心敏感材料的潜力;对比萃取奶粉中17β-雌二醇性能,MISPE柱比非分子印迹固相萃取柱和C18柱具有更高的保留,回收率依次为85.5%,43.7%和30.7%。

The aim of this study was to evaluate the relative impact of genetic versus nongenetic factors on muscle GS activation and regulation in young and elderly twins examined with a 2-h euglycemic-hyperinsulinemic (40 mU · m–2 · min���1) clamp combined with indirect calorimetry and excision of muscle biopsies.

这个研究的目的是采用2小时正常血糖-高血浆胰岛素钳夹技术(40 mU · m–2 · min–1)结合间接测热法和肌肉活组织切片技术探索遗传因素和非遗传因素两方面对幼年和成年双胞胎肌肉糖原合成酶调节之间的关系。

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The concept of equivalent rotationally rigidity is offered and the formula of rotationally rigidity is obtained.

主要做了如下几个方面的工作:对伸臂位于顶部的单层框架—筒体模型进行分析,提出了等效转动约束的概念和转动约束刚度的表达式。

Male cats normally do not need aftercare with the exception of the night after the anesthetic.

男猫通常不需要善后除了晚上的麻醉。

Its advantage is that it can be used in smaller units.

其优点在于可以在较小的单位中应用。